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GA/T 2132-2024: Forensic sciences - Examination methods for 36 fentanyl analogs including fentanyl in human hair samples - LC-MS
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Forensic sciences - Examination methods for 36 fentanyl analogs including fentanyl in human hair samples - LC-MS
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GA/T 2132-2024
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Basic data | Standard ID | GA/T 2132-2024 (GA/T2132-2024) | | Description (Translated English) | Forensic sciences - Examination methods for 36 fentanyl analogs including fentanyl in human hair samples - LC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 07.140 | | Word Count Estimation | 54,533 | | Date of Issue | 2024-04-09 | | Date of Implementation | 2024-07-01 | | Issuing agency(ies) | Ministry of Public Security | GA/T 2132-2024: Forensic sciences - Examination methods for 36 fentanyl analogs including fentanyl in human hair samples - LC-MS
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ICS 07.140
CCSA92
Public Security Industry Standard of the People's Republic of China
Forensic science. fentanyl and 36 other substances in hair
Fentanyl-like substances test liquid chromatography-mass spectrometry
Released on 2024-04-09
2024-07-01 Implementation
The Ministry of Public Security of the People’s Republic of China issued
Table of Contents
Preface III
1 Scope 1
2 Normative references 1
3 Terms and Definitions 1
4 Principle 1
5 Reagents and Materials 1
6 Instruments and equipment 2
7 Operation Method 2
8 Results Evaluation 7
Appendix A (Informative) Basic information of compounds 8
Appendix B (Informative) Spectra of fentanyl and 36 other fentanyl-like substances 13
Foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents"
Drafting.
Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents.
This document was proposed and coordinated by the National Technical Committee for Criminal Technology Standardization (SAC/TC179).
This document was drafted by. the Anti-Drug Intelligence Technology Center of the Ministry of Public Security, the Institute of Forensic Science, the Zhejiang Branch of the National Narcotics Laboratory,
Narcotics Control Brigade of the Public Security Department of Inner Mongolia Autonomous Region.
The main drafters of this document are. Wu Jianmei, Zhang Tingting, Qiao Hongwei, Chen Jie, Qiao Yanling, Shi Yan, Yan Hui, Jin Jiabin, Liu Yong, Xu Yu, Qi Haitao,
Zhang Yuzi.
Forensic science. fentanyl and 36 other substances in hair
Fentanyl-like substances test liquid chromatography-mass spectrometry
1 Scope
This document specifies the liquid chromatography-mass spectrometry (LC-MS) test for fentanyl and 36 other fentanyl-like substances in hair in the field of forensic science.
method.
This document applies to the qualitative and quantitative analysis of fentanyl and 36 other fentanyl-like substances in hair in the field of forensic science.
2 Normative references
The contents of the following documents constitute essential clauses of this document through normative references in this document.
For referenced documents without a date, only the version corresponding to that date applies to this document; for referenced documents without a date, the latest version (including all amendments) applies to
This document.
GB/T 6682 Specifications and test methods for water used in analytical laboratories
GB/T 27418 Evaluation and expression of measurement uncertainty
GA/T 122 Terminology for Toxicological Analysis
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principle
Blank samples and spiked samples were used as controls. According to the requirements of parallel operation, 36 fentanyl-like substances (compounds
The basic information is shown in Appendix A) for extraction. Liquid chromatography-mass spectrometry was used for detection, and retention time, mass spectrometry characteristic ion pairs and ion pair abundance were used to determine the
The ratio was used as the qualitative basis, and the chromatographic peak area was used as the quantitative basis, and the external standard calibration curve method was used for quantitative analysis.
5 Reagents and Materials
5.1 Reagents
The experimental water should comply with the first-grade water specified in GB/T 6682.The reagents used in the analysis are all chromatographically pure, including the following reagents.
content.
a) Methanol.
b) Formic acid. LC-MS grade.
c) 0.1% formic acid solution (taking 1000 mL as an example). take 1.0 mL of formic acid, dilute with water and make up to 1000 mL, mix
Homogenize and ultrasonicate.
d) Standard solution.
1) Standard substance stock solution. After conversion based on the purity and salt form of fentanyl and other 36 fentanyl-like substances, each stock solution is weighed
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