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GA/T 2129-2024 English PDF

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GA/T 2129-2024: Forensic sciences - Examination methods for glyphosate and glufosinate in biological samples - GC-MS
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Basic data

Standard ID GA/T 2129-2024 (GA/T2129-2024)
Description (Translated English) Forensic sciences - Examination methods for glyphosate and glufosinate in biological samples - GC-MS
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Classification of International Standard 07.140
Word Count Estimation 14,121
Date of Issue 2024-02-23
Date of Implementation 2024-06-01
Issuing agency(ies) Ministry of Public Security

GA/T 2129-2024: Forensic sciences - Examination methods for glyphosate and glufosinate in biological samples - GC-MS


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ICS 07.140 CCSA92 Public Security Industry Standard of the People's Republic of China Glyphosate and Glufosinate-ammonium test gas chromatography-mass spectrometry Released on 2024-02-23 2024-06-01 Implementation The Ministry of Public Security of the People’s Republic of China issued

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents" Drafting. Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents. This document was proposed and coordinated by the National Technical Committee for Criminal Technology Standardization (SAC/TC179). This document was drafted by. Beijing Public Security Judicial Appraisal Center, Ministry of Public Security Appraisal Center, Guangdong Provincial Public Security Department, Jiangsu Provincial Public Security Department, Hubei Provincial Public Security Department, Provincial Public Security Department. The main drafters of this document are. Qiao Jing, Zhang Wenfang, Yang Shiyun, Liu Yongtao, Li Mengmeng, Qin Shiyang, Zhang Ying, Xu Zizhen, Zhu Kongwen, Wang Ruihua, Pei Maoqing, Zhang Yinhua, Chang Jing, Wang Fanglin, Yu Zhongshan, and Wang Xuehu. Glyphosate and Glufosinate-ammonium test gas chromatography-mass spectrometry

1 Scope

This document specifies the gas chromatography-mass spectrometry (GC-MS) method for the determination of glyphosate and glufosinate in biological samples (blood and urine) for forensic science applications. Inspection method. This document applies to the qualitative and quantitative analysis of glyphosate and glufosinate in biological samples (blood and urine) in the field of forensic science. Other samples may be used for reference.

2 Normative references

The contents of the following documents constitute essential clauses of this document through normative references in this document. For referenced documents without a date, only the version corresponding to that date applies to this document; for referenced documents without a date, the latest version (including all amendments) applies to This document. GB/T 6682 Specifications and test methods for water used in analytical laboratories GA/T 122 Terminology for Toxicological Analysis

3 Terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 Principle

Using blank samples and spiked samples as controls, the glyphosate and glufosinate ammonium (compounds) in blood and urine were measured in parallel. Basic information is shown in Appendix A) for extraction and derivatization, and gas chromatography-mass spectrometry detection is used to determine the retention time, mass spectrometry characteristic ions and ion abundance. The concentration ratio was used as the qualitative basis, and the chromatographic peak area was used as the quantitative basis, and the external standard method was used for quantification.

5 Reagents and Materials

5.1 Reagents The experimental water should comply with the third-grade water specified in GB/T 6682.The reagents used in the analysis are all analytical grade or above. include. a) methanol; b) Acetonitrile (newly opened or dehydrated with anhydrous sodium sulfate before use); c) Acetonitrile solution (for example, 90 mL). measure 60 mL of acetonitrile and 30 mL of water and mix well; d) 20% methanol-acetonitrile solution (taking 100 mL as an example). measure 20 mL of methanol and 80 mL of acetonitrile and mix well; e) Ammonia solution (taking 100 mL as an example). Take 97 mL of water and 3 mL of concentrated ammonia solution (mass fraction 25%~28%), Mix well;

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