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| GB/T 23228-2008 | English | 209 |
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Cigarette -- Determination of tobacco specific N-Nitrosamines in total particulate matter of mainstream cigarette smoke -- GC-TEA method
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GB/T 23228-2008
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Basic data | Standard ID | GB/T 23228-2008 (GB/T23228-2008) | | Description (Translated English) | Cigarette -- Determination of tobacco specific N-Nitrosamines in total particulate matter of mainstream cigarette smoke -- GC-TEA method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | X87 | | Classification of International Standard | 65.160 | | Word Count Estimation | 9,942 | | Date of Issue | 2008-12-31 | | Date of Implementation | 2009-06-01 | | Quoted Standard | GB/T 5606.1; GB/T 19609 | | Regulation (derived from) | National Standard Approval Announcement 2008 No.27 (Total No.140) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the mainstream cigarette smoke total particulate matter in the N-nitroso nornicotine (NNN), N- nitroso neonicotinoid (NAT), N- nitroso anabasine (NAB) and 4-(methylnitrosamino) -1-(3-pyridyl) -1-butanone (NNK) Determination of tobacco-specific nitrosamines four. This standard applies to cigarette smoke total particulate matter in the determination of these four tobacco-specific nitrosamines. |
GB/T 23228-2008: Cigarette -- Determination of tobacco specific N-Nitrosamines in total particulate matter of mainstream cigarette smoke -- GC-TEA method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Cigarette. Determination of tobacco specific N-Nitrosamines in total particulate matter of mainstream cigarette smoke. GC-TEA method
ICS 65.160
X87
National Standards of People's Republic of China
Cigarette mainstream smoke total particulate matter
Determination of tobacco specific nitrosamines N-
GC - TEA associated usage
Posted 2008-12-31
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The Standard Appendix A, Appendix B is an informative annex.
This standard was proposed by the State Tobacco Monopoly Bureau.
This standard by the National Standardization Technical Committee on Tobacco (SAC/TC144) centralized.
This standard drafting units. China Tobacco Corporation, Zhengzhou Tobacco Research Institute, Shanghai Tobacco (Group) Company.
The main drafters of this standard. Xie Wei complex, JIN Yong-ming, Zhao moon, Wang hate, Liu Jian, Wu Ming.
Cigarette mainstream smoke total particulate matter
Determination of tobacco specific nitrosamines N-
GC - TEA associated usage
1 Scope
This standard specifies the cigarette mainstream smoke total particulate matter in the N- nitroso Nornicotine (NNN), N- nitroso neonicotinoid (NAT), N- Asia
Nitro anabasine (NAB) and 4- (DMN-yl) -1- (3-pyridyl) -1-butanone (NNK) Determination of four kinds of tobacco-specific nitrosamines
method.
This standard applies to cigarette smoke total particulate matter measured in these four tobacco specific nitrosamines.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 5606.1 cigarette - Part 1. Sampling
GB/T 19609 cigarettes by conventional analytical determination of total particulate matter and tar (GB/T 19609-2004 smoking machine, ISO 4387.
2000, MOD)
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
Only present in tobacco and tobacco products in the N- nitrosamines.
Principle 4
Glass fiber filters trap cigarette mainstream smoke total particulate matter, particulate matter was extracted with dichloromethane in TSNAs, concentrated extract
And using basic alumina was purified by column chromatography. By gas chromatography - Thermal analysis spectrometer (GC-TEA) detector extracts Central Glass
Amine concentration of the mainstream smoke total particulate matter TSNAs quantitative analysis.
5 Reagents and materials
In addition to special requirements, should use analytical grade reagents. Water should be distilled water or water of equivalent purity.
5.1 dichloromethane chromatography (or analytical redistilled after use).
5.2 Methanol, HPLC grade (or analytical redistilled after use).
5.3 over anhydrous sodium sulfate.
5.4 basic alumina, 200 mesh and 300 mesh.
5.5 N- pentyl - (3-pyridyl) nitrosamines, NNN, NAT, NAB, NNK, should be greater than 97% purity.
5.6 Internal standard solution
5.6.1 internal standard stock solution
Weighed accurately 10mgN- pentyl - (3-pyridyl) nitrosamine, after about 50mL methylene chloride (5.1) was added to completely dissolve, transfer
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