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GA/T 1332-2016English229 Add to Cart 3 days [Need to translate] GC-MS examination methods for five actamide herbicides including alachlor in blood in forensic science Valid GA/T 1332-2016


BASIC DATA
Standard ID GA/T 1332-2016 (GA/T1332-2016)
Description (Translated English) GC-MS examination methods for five actamide herbicides including alachlor in blood in forensic science
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Classification of International Standard 13.310
Word Count Estimation 10,131
Date of Issue 2016-09-14
Date of Implementation 2016-09-14
Issuing agency(ies) Ministry of Public Security of the People's Republic of China


GA/T 1332-2016 GC-MS examination methods for five actamide herbicides including alachlor in blood in forensic science ICS 13.310 A92 People 's Republic of China Public Security Industry Standard Forensic science in the blood of aldehydes and other five amides Standard Test Method for Herbicides by Gas Chromatography - Mass Spectrometry 2016-09-14 release 2016-09-14 implementation Issued by the Ministry of Public Security of the People 's Republic of China Preface This standard is drafted in accordance with the rules given in GB/T 1.1-2009. Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents. This standard is proposed by the National Committee for the Standardization of Pharmaceutical Technology Standardization of Substances (SAC/TC179/SC1) and Go back. The drafting of this standard. Beijing Public Security Bureau Criminal Investigation Corps, the Ministry of Public Security evidence center. The main drafters of this standard. Yang Shiyun, Qiao Jing, Yuan Zengping, Zhang Wenfang, He Yi, Yu Zhongshan, Wang Fanglin. Forensic science in the blood of aldehydes and other five amides Standard Test Method for Herbicides by Gas Chromatography - Mass Spectrometry 1 Scope This standard provides for the use of five amide herbicides in the forensic scientific blood of alachlor, acetochlor, metolachlor, butachlor, Chromatography-Mass Spectrometry (GC-MS) test method. This standard applies to the qualitative and quantitative analysis of alachlor, acetochlor, metolachlor, butachlor and propachlor in the scientific blood of the court. 2 normative reference documents The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article Pieces. For undated references, the latest edition (including all modifications) applies to this document. Analysis of laboratory water specifications and test methods GB/T 6682-2008 Glossary of Terminology for Poison Analysis 3 terms and definitions The terms and definitions defined in GA/T 122 apply to this document. 4 principle With the blank sample and add samples for the control, according to the requirements of parallel operation, the blood extraction, purification and concentration, the use of gas phase color (TR), mass spectral characteristics of ion fragmentation peaks and relative abundance as a qualitative basis for the determination; with the parallel operation of the Tim Plus standard material response value comparison, according to the peak area ratio, with external standard method for quantitative analysis. 5 reagents and materials Unless otherwise stated, the reagents used in this standard are of analytical grade and test water is tertiary water (see GB/T 6682-2008). a) cyclohexane; b) Ethanol; c) Standard solution. 1) 1.0mg/mL Reference substance solution. Weigh alachlor, acetochlor, metolachlor, butachlor, propachlor standards Quality 50.0mg in 50mL volumetric flask, add a certain amount of ethanol dissolved and diluted to the mark, mix. Were prepared 1.0mg/mL alachlor, acetochlor, metolachlor, butachlor, propanamine standard substance solution. Sealed, placed on ice Frozen in the box. Save time for 12 months; 2) 0.1mg/mL Standard working solution. Remove 1.0mg/mL amide herbicide standard solution 1.0mL 10mL volumetric flask, add ethanol diluted to the mark, mix. Were prepared into 0.1mg/mL of alachlor, grass Amine, metolachlor, butachlor, propanamine standard working solution. Sealed, placed in the refrigerator in the cold storage. save time 6 months. ......

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