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GA/T 1322-2016: GC-MS examination methods for ten benzodiazepines including diazepam in blood in forensic science
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| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GA/T 1322-2016 | English | 299 |
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GC-MS examination methods for ten benzodiazepines including diazepam in blood in forensic science
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GA/T 1322-2016
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Basic data | Standard ID | GA/T 1322-2016 (GA/T1322-2016) | | Description (Translated English) | GC-MS examination methods for ten benzodiazepines including diazepam in blood in forensic science | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Word Count Estimation | 13,147 | | Date of Issue | 2016-07-11 | | Date of Implementation | 2016-07-11 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1322-2016: GC-MS examination methods for ten benzodiazepines including diazepam in blood in forensic science
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(Forensic science in the blood of diazepam and other ten kinds of benzodiazepines drug gas chromatography - mass spectrometry test method)
ICS 13.310
A92
People 's Republic of China Public Security Industry Standard
Court science blood diazepam and other ten kinds of benzo
Test Method for Gas Chromatography - Mass Spectrometry of Diazepine Drugs
2016-07-11 released
2016-07-11 implementation
Issued by the Ministry of Public Security of the People 's Republic of China
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents.
This standard is proposed by the National Committee for the Standardization of Pharmaceutical Technology Standardization of Substances (SAC/TC179/SC1) and
Go back.
The drafting of this standard. Shanghai Municipal Public Security Bureau Material Identification Center, the Ministry of Public Security evidence center.
The main drafters of this standard. Liang Chen, Zhang Yurong, Wang Rong, Wang Fanglin, Yu Zhong Shan.
Court science blood diazepam and other ten kinds of benzo
Test Method for Gas Chromatography - Mass Spectrometry of Diazepine Drugs
1 Scope
This standard specifies the method of gas chromatography-mass spectrometry (GC-MS) for the determination of benzodiazepines in the scientific blood of the court.
This standard applies to forensic science in the blood of diazepam, osamazepam, clonazepine, triazolam, alprazolam, nitrazepam, estazolam, chlorine
Qualitative and Quantitative Analysis of 10 Kinds of Benzodiazepines in Nitrazepam, Lorazepam and Midazolam.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Analysis of laboratory water specifications and test methods GB/T 6682-2008
Glossary of Terminology for Poison Analysis
3 terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principle
The samples were taken as blank and the samples were taken as control. According to the requirements of parallel operation, the blood samples were extracted, purified and concentrated.
(TR), mass spectral characteristics of ion fragment peaks and relative abundance as the basis for qualitative judgment; and parallel operation
For the comparison of the added standard material response values, according to the ratio of peak area, with the internal standard method for quantitative analysis.
5 reagents and materials
The reagents used in this standard are of analytical grade and test water is tertiary water (see GB/T 6682-2008).
a) Methanol.
b) benzene
c) ethyl acetate.
d) ether.
e) n-hexane.
f) dichloromethane.
g) Ammonia.
h) 1.0mol/L NaOH solution. Weigh 20.0g sodium hydroxide, add a certain amount of water to dissolve and dilute the volume to 500mL.
i) 2% Ammonia 5% methanol solution. 2.0 mL of aqueous ammonia and 5.0 mL of methanol were removed in a 100 mL volumetric flask and diluted with water
Degree, mix.
j) 5% methanol solution. remove the methanol 5.0mL in a 100mL volumetric flask, add water diluted to the mark, mix.
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