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National Food Safety Standard -- Food Additives -- White orchid oil
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Basic data
| Standard ID | GB 1886.275-2016 (GB1886.275-2016) |
| Description (Translated English) | National Food Safety Standard -- Food Additives -- White orchid oil |
| Sector / Industry | National Standard |
| Classification of Chinese Standard | X40 |
| Word Count Estimation | 8,899 |
| Date of Issue | 2016-08-31 |
| Date of Implementation | 2017-01-01 |
| Regulation (derived from) | Announcement of the State Administration of Public Health and Family Planning 2016 No.11 |
| Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration |
GB 1886.275-2016: National Food Safety Standard -- Food Additives -- White orchid oil
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - White orchid oil)
National Standards of People's Republic of China
National Food Safety Standard
Food additive white orchid oil
Published 2016-08-31
2017-01-01 implementation
People's Republic of China
National Health and Family Planning Commission issued
National Food Safety Standard
Food additive white orchid oil
1 Scope
This standard applies to steam distillation from the Magnoliaceae Bai Lan (Micheliaalba) prepared in flower food additive white orchid oil.
2 Technical Requirements
2.1 Sensory requirements
Sensory requirements shall comply with the requirements in Table 1.
Table 1 Sensory requirements
Project requires test methods
Pale yellow to amber color
Liquid state
The sample was placed in a cuvette, were visually observed
White Orchid characteristic aroma of aroma GB/T 14454.2
2.2 Physical and Chemical Indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Relative density (20 ℃/20 ℃) 0.870 ~ 0.910 GB/T 11540
Refractive index (20 ℃) 1.460 ~ 1.490 GB/T 14454.4
Optical rotation (20 ℃) -15 ° ~ -2 ° GB/T 14454.5
Miscibility of (20 ℃)
1 volume of the sample is miscible in 95% by volume 1 (by volume
Score) in ethanol, a clear solution
GB/T 14455.3
Acid number (as KOH)/(mg/g) ≤ 10 GB/T 14455.5
Linalool content, w /% ≥ 50 Appendix A
Appendix A
Determination of linalool content
A.1 instruments and equipment
A.1.1 Chromatography. in GB/T 11538-2006 specified in Chapter 5.
A.1.2 Column. capillary column.
A.1.3 Detector. hydrogen flame ionization detector.
A.2 Determination
Area normalization method. Press the GB/T 11538-2006 Determination 10.4.
A.3 repeatability and results are expressed
11538-2006 carried out in accordance with the provisions of 11.4 GB/T , should meet the requirements.
Food Additive White Orchid oil gas chromatography and the operating conditions of FIG see Appendix B.
Appendix B
Food Additive White Orchid oil gas chromatography and the operating conditions of FIG.
(Area normalization method)
B.1 food additive white orchid oil gas chromatography FIG.
Food Additive White Orchid oil gas chromatography is shown in Figure B.1.
Description.
. 1 --- 2-methylbutyrate;
2 --- 1,8 cineole;
3 --- cis -β- ocimene;
4 --- trans -β- ocimene;
5 --- α- Cuba alkenyl;
6 --- β- Bi Litseae alkenyl;
7 --- linalool;
8 --- (-) - β--elemene;
--- trans -β-. 9 caryophyllene;
10 --- α- terpineol;
11 --- α- Cnidium alkenyl;
12 --- δ- cadinene;
13 is --- nerol;
14 --- geraniol;
15 --- methyl eugenol;
16 --- nerolidol;
. 17 --- methyl iso-eugenol;
18 is --- 9,12-octadecadienoic acid methyl ester.
Figure B.1 food additive white orchid oil gas chromatography FIG.
B.2 operating conditions
B.2.1 Column. capillary column, length 30m, an inner diameter of about 0.32mm.
B.2.2 stationary phase. polyethylene glycol 20000.
B.2.3 film thickness. 0.50μm.
B.2.4 chromatographic oven temperature. 80 ℃ thermostat 8min, then linear temperature programmed from 80 deg.] C to 100 ℃, a rate of 2 ℃/min; 100 ℃ thermostat
8min, then deg.] C from 100 to 200 ℃, a rate of 5 ℃/min, 200 ℃ thermostat 10min; and from 200 ℃ to 220 ℃, a rate of 10 ℃/min,
Finally, at 220 deg.] C thermostat 8min.
B.2.5 Inlet temperature. 250 ℃.
B.2.6 Detector temperature. 280 ℃.
B.2.7 Detector. hydrogen flame ionization detector.
B.2.8 Carrier gas. nitrogen.
B.2.9 carrier gas flow rate. 1mL/min.
B.2.10 Injection volume. about 0.2μL.
B.2.11 split ratio. 80.1.
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