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Forensic sciences--Examination methods for dolantin in suspected drugs--GC and GC-MS
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Basic data
| Standard ID | GA/T 2030-2023 (GA/T2030-2023) |
| Description (Translated English) | Forensic sciences--Examination methods for dolantin in suspected drugs--GC and GC-MS |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | A92 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 15,141 |
| Date of Issue | 2023-03-01 |
| Date of Implementation | 2023-12-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 2030-2023: Forensic sciences--Examination methods for dolantin in suspected drugs--GC and GC-MS
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13:310
CCSA92
People's Republic of China Public Security Industry Standards
Forensic Science Suspected Drug Test for Demerol
Gas Chromatography and Gas Chromatography-Mass Spectrometry
GC and GC-MS
Released on 2023-03-01
2023-12-01 implementation
Released by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1:1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules for Standardization Documents"
drafting:
Please note that some contents of this document may refer to patents: The issuing agency of this document assumes no responsibility for identifying patents:
This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted
Focus on:
This document was drafted by: Qingdao Municipal Public Security Bureau, Appraisal Center of the Ministry of Public Security, China Criminal Police College, Tianjin Municipal Public Security Bureau, Yunnan Provincial Public Security
Judicial Appraisal Center, Jilin Provincial Public Security Bureau Physical Evidence Appraisal Center:
The main drafters of this document: Guo Jie, Lu Jinghan, Shi Huili, Jiang Huayu, Shang Jinlei, Zheng Hui, Zhu Yu, Wang Qun, Zhao Wensong, Sun Jilai:
Forensic Science Suspected Drug Test for Demerol
Gas Chromatography and Gas Chromatography-Mass Spectrometry
1 Scope
This document specifies the gas chromatography-mass spectrometry (GC-MS) qualitative test method and gas chromatography for pethidine in suspected drugs in the field of forensic science:
Spectrum (GC) quantitative test method:
This document applies to the qualitative and quantitative analysis of pethidine in suspected drugs in the field of forensic science:
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text: Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document:
GB/T 6682 Analytical laboratory water specifications and test methods
GB/T 27418 Evaluation and Expression of Measurement Uncertainty
GA/T 122 Toxicological Analysis Terminology
3 Terms and Definitions
The terms and definitions defined in GA/T 122 apply to this document:
4 principles
Extract the pethidine (see Appendix A for compound information) in suspected drug solid or liquid samples: gas chromatography-mass spectrometry
For detection, the retention time, mass spectrometry characteristic ions and ion abundance ratio were used as the basis for qualitative judgment; for gas chromatography detection, the peak area
As a quantitative basis, the solid sample is quantitatively analyzed by the external standard single point method or the internal standard standard curve method, and the liquid sample is analyzed by the external standard single point method or the internal standard curve method:
Quantitative analysis by single point method:
5 Reagents and materials
5:1 Reagents
The experimental water should meet the third-grade water specified in GB/T 6682: All reagents used in the analysis were of analytical grade: Reagents include:
a) Methanol;
b) ethyl acetate;
c) saturated sodium carbonate solution;
d) 10% sodium hydroxide solution (take the preparation of 100mL as an example): weigh 10g of sodium hydroxide, dissolve it in water and set the volume to 100mL;
e) Standard solution:
...
