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GA/T 2021-2023 English PDF

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GA/T 2021-2023: Forensic sciences - Examination methods for 2′-chlorodiazepam and 4′-chlorodiazepam in suspected drugs - GC and GC-MS
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GA/T 2021-2023319 Add to Cart 4 days Forensic sciences - Examination methods for 2′-chlorodiazepam and 4′-chlorodiazepam in suspected drugs - GC and GC-MS Valid

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GA/T 1788.2   GA/T 1711   GA/T 424   GA/T 2012   GA/T 2013   GA/T 2011   

Basic data

Standard ID: GA/T 2021-2023 (GA/T2021-2023)
Description (Translated English): Forensic sciences - Examination methods for 2��-chlorodiazepam and 4��-chlorodiazepam in suspected drugs - GC and GC-MS
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.310
Word Count Estimation: 16,154
Date of Issue: 2023-03-01
Date of Implementation: 2023-12-01
Issuing agency(ies): Ministry of Public Security

GA/T 2021-2023: Forensic sciences - Examination methods for 2′-chlorodiazepam and 4′-chlorodiazepam in suspected drugs - GC and GC-MS


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310 CCSA92 Public safety industry standards of the People's Republic of China Forensic Science Suspected Drugs 2'-Clodiazepam and 4'-Clodiazepam test gas chromatography and Gas Chromatography-Mass Spectrometry Published on 2023-03-01 Implemented on 2023-12-01 Released by the Ministry of Public Security of the People's Republic of China

Foreword

This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents. This document is submitted by the Criminal Investigation Bureau of the Ministry of Public Security. This document is under the jurisdiction of the Toxicology Analysis Sub-Technical Committee of the National Technical Committee for Standardization of Criminal Technology (SAC/TC179/SC1). This document was drafted by. Beijing Municipal Public Security Bureau Criminal Investigation Corps, Shanghai Municipal Public Security Bureau Criminal Science and Technology Management Center, Guangdong Provincial Public Security Bureau Department Criminal Technology Center, Guangxi Zhuang Autonomous Region Public Security Department Criminal Investigation Corps, Zibo Municipal Public Security Bureau, Hangzhou Municipal Public Security Bureau, Hefei Municipal Public Security Bureau, Hunan Provincial Public Security Department Physical Evidence Identification Center, Ministry of Public Security Anti-Narcotics Intelligence Technology Center, Hohhot Municipal Public Security Bureau, Shanxi Provincial Public Security Department Science and Technology Department, Datong Municipal Public Security Bureau Security Bureau, Nanjing Anti-Narcotics Detachment. The main drafters of this document. Liu Hua, Yang Shiyun, Zhang Ying, Qiao Jing, Wang Yanyan, Xin Guobin, Liu Yongtao, Wei Juanna, Zhang Wenfang, Xu Zizhen, Qin Shiyang, Zhu Kongwen, Li Mengmeng, Zhang Yurong, Liang Chen, Pei Maoqing, Zhang Liang, Huang Kejian, Liu Xiaofeng, Guofei, Li Xiaofei, Ying Jianbo, Song Xin, Wu Hai, Gao Mi, Chen Jie, Bayinfu, Wu Zhipeng, Yan Zhiqiang, Zhang Gaoqin, Guo Liang, Zhang Zhonghui. Forensic Science Suspected Drugs 2'-Clodiazepam and 4'-Clodiazepam test gas chromatography and Gas Chromatography-Mass Spectrometry

1 Scope

This document describes the gas chromatography-mass spectrometry (GC-MS) determination of 2'-chlordiazepam and 4'-chlordiazepam in suspected narcotics in the field of forensic science. sexual testing method and gas chromatography (GC) quantitative testing method. This document is applicable to the qualitative and quantitative analysis of 2'-chlordiazepam and 4'-chlordiazepam in suspected drugs in the field of forensic science.

2 Normative reference documents

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document. GB/T 6682 Specifications and test methods for water used in analytical laboratories GB/T 27418 Evaluation and expression of measurement uncertainty GA/T 122 Toxicological analysis terminology

3 Terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 Principles

Extract 2'-chlordiazepam and 4'-chlordiazepam from the suspected drugs (see Appendix A for compound information). Using gas chromatography-mass For spectrometric detection, the retention time, mass spectrum characteristic ions and ion abundance ratio are used as the basis for qualitative judgment; for gas chromatography detection, the chromatographic peaks are used for detection. The area was used as the quantitative basis, and the external standard single point method or the external standard standard curve method was used for quantitative analysis.

5 Reagents and materials

5.1 Reagents Unless otherwise stated, the reagents used in the analysis were of analytical grade. Reagents include methanol and standard solutions. a) Methanol. b) Standard solution. 1) Standard material stock solution. After conversion according to the purity and salt type of the 2'-chlordiazepam and 4'-chlordiazepam standard materials, weigh each Appropriate amount, use methanol to prepare 1.0 mg/mL 2'-chlordiazepam and 4'-chlordiazepam standard material stock solutions respectively. Seal, store below -18℃, valid for 12 months, or use commercially available standard solutions. 2) Standard working solutions are divided into the following four categories according to experimental requirements.
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