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Forensic sciences--Examination methods for buprenorphine in suspected drugs--GC and GC-MS
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Basic data
| Standard ID | GA/T 2028-2023 (GA/T2028-2023) |
| Description (Translated English) | Forensic sciences--Examination methods for buprenorphine in suspected drugs--GC and GC-MS |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | A92 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 16,149 |
| Date of Issue | 2023-03-01 |
| Date of Implementation | 2023-12-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 2028-2023: Forensic sciences--Examination methods for buprenorphine in suspected drugs--GC and GC-MS
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13:310
CCSA92
People's Republic of China Public Security Industry Standards
Buprenorphine test in suspected drug in forensic science
Gas Chromatography and Gas Chromatography-Mass Spectrometry
GC and GC-MS
Released on 2023-03-01
2023-12-01 implementation
Released by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1:1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules for Standardization Documents"
drafting:
Please note that some contents of this document may refer to patents: The issuing agency of this document assumes no responsibility for identifying patents:
This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted
Focus on:
This document was drafted by: Guangdong Provincial Public Security Department Criminal Technology Center, Ministry of Public Security Evidence Appraisal Center, Guangxi Zhuang Autonomous Region Public Security Department Criminal
The Investigation Corps, the Criminal Investigation Bureau of the Shaanxi Provincial Public Security Department, and the China Criminal Police Academy:
The main drafters of this document: Pei Maoqing, Zhang Liang, Hu Haolang, Shi Wenbing, Wang Bin, Xu Ruolun, Zheng Hui, Liu Xiaofeng, Zhang Aidong, Wang Yan:
Buprenorphine test in suspected drug in forensic science
Gas Chromatography and Gas Chromatography-Mass Spectrometry
1 Scope
This document specifies the gas chromatography-mass spectrometry (GC-MS) qualitative test method for buprenorphine in suspected drug solid samples in the field of forensic science:
method and gas chromatography (GC) quantitative test method:
This document applies to the qualitative and quantitative analysis of buprenorphine in suspected drug solid samples in the field of forensic science: Other in vitro test materials
Can refer to use:
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text: Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document:
GB/T 6682 Analytical laboratory water specifications and test methods
GB/T 27418 Evaluation and Expression of Measurement Uncertainty
GA/T 122 Toxicological Analysis Terminology
3 Terms and Definitions
The terms and definitions defined in GA/T 122 apply to this document:
4 principles
Buprenorphine (see Appendix A for compound information) in suspected drug solid samples was extracted: detected by gas chromatography-mass spectrometry,
The qualitative judgment is based on retention time, characteristic ion of mass spectrum and ion abundance ratio; gas chromatography is used for detection, and chromatographic peak area (or peak
Area ratio) as the basis for quantification, using external standard single point method, external standard standard curve method, internal standard single point method or internal standard standard curve method for quantification
analyze:
5 Reagents and materials
5:1 Reagents
The experimental water should meet the third-grade water specified in GB/T 6682: The reagents used in the analysis are analytically pure, and the reagents include:
a) Methanol;
b) Standard solution:
1) Standard substance stock solution: buprenorphine standard substance stock solution;
2) Internal standard stock solution: Weigh 10 mg of internal standard propyl spasmolyticin (SKF525A), and prepare 1:0 mg/mL internal standard stock solution with methanol:
Prepare liquid, refrigerated storage at 0℃~4℃, valid for 12 months;
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