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Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - GC and GC-MS
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Basic data
| Standard ID | GA/T 2024-2023 (GA/T2024-2023) |
| Description (Translated English) | Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - GC and GC-MS |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | A92 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 13,180 |
| Date of Issue | 2023-03-01 |
| Date of Implementation | 2023-12-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 2024-2023: Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - GC and GC-MS
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ICS 13.310
CCSA92
Public safety industry standards of the People's Republic of China
Forensic Science Suspected Drugs 5-MeO-DiPT and
5-MeO-MiPT test gas chromatography and
Gas Chromatography-Mass Spectrometry
Published on 2023-03-01
Implemented on 2023-12-01
Released by the Ministry of Public Security of the People's Republic of China
Foreword
This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents"
Drafting.
Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents.
This document is proposed and submitted by the Toxic Analysis Sub-Technical Committee of the National Technical Committee for Standardization of Criminal Technology (SAC/TC179/SC1).
Return to home.
This document was drafted by. Ministry of Public Security Identification Center, China Criminal Police College, Hainan Provincial Public Security Department, Jiangsu Provincial Public Security Department Physical Evidence Identification Center
Center, Ministry of Public Security Anti-Narcotics Intelligence Technology Center.
The main drafters of this document. Li Peng, Zheng Xiaoyu, Zhao Yang, Zheng Hui, Zhang Chunshui, Jiang Zhaolin, Zhu Yu, Liu Guangming, Qian Kaiwen, Qian Zhenhua, Chang Ying,
Zhang Tingting, Zhao Yanbiao, Yang Hongxian, Wen Wu, Zhai Wanfeng, Liu Kelin, Gu Yuebao, Zhang Jing, Wang Xuehu, Zhang Qianshang, Yang Zhi, Wei Jiao, Gao Lisheng.
Forensic Science Suspected Drugs 5-MeO-DiPT and
5-MeO-MiPT test gas chromatography and
Gas Chromatography-Mass Spectrometry
1 Scope
This document describes 5-methoxy-N,N-diisopropyltryptamine (5-MeO-DiPT), N-methyl
Gas chromatography-mass spectrometry (GC-MS) qualitative detection method and gas chromatography (GC) of -N-isopropyl-5-methoxytryptamine (5-MeO-MiPT)
Quantitative testing methods.
This document is applicable to the qualitative analysis and quantification of 5-MeO-DiPT and 5-MeO-MiPT in suspected drug solids in the field of forensic science.
analyze.
2 Normative reference documents
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations
For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to
this document.
GB/T 27418 Evaluation and expression of measurement uncertainty
GA/T 122 Toxicological analysis terminology
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principles
Extract 5-MeO-DiPT and 5-MeO-MiPT from suspected drug solids (see Appendix A for compound information). Use gas phase color
Spectrometry-mass spectrometry is used for detection, based on retention time, mass spectrum characteristic ions and ion abundance ratios as the basis for qualitative judgment; gas chromatography is used for detection, based on
The chromatographic peak area was used as the quantitative basis, and the external standard single point method or the external standard standard curve method was used for quantitative analysis.
5 Reagents and materials
5.1 Reagents
Unless otherwise stated, the reagents used in the analysis were of chromatographic grade. Reagents include methanol and standard solutions.
a) Methanol.
b) Standard solution.
1) Standard material stock solution. 1.0mg/mL5-MeO-DiPT, 5-MeO-MiPT standard material stock solution, 0℃~4℃
Stored refrigerated, valid for 12 months.
2) Standard working solutions are divided into the following four categories according to experimental requirements.
...
