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Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method
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YS/T 923.1-2013
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Basic data | Standard ID | YS/T 923.1-2013 (YS/T923.1-2013) | | Description (Translated English) | Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method | | Sector / Industry | Nonferrous Metallurgy Industry Standard (Recommended) | | Classification of Chinese Standard | H13 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 7,789 | | Regulation (derived from) | Ministry of Industry and Information Technology Bulletin No. 52, 2013; industry standard for filing Notice No. 1 of 2014 (No. 169 overall) | | Issuing agency(ies) | Ministry of Industry and Information Technology | | Summary | This standard specifies the secret of high purity copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content determination. This standard applies to high-purity copper, lead, zinc, iron, silver, arsenic |
YS/T 923.1-2013: Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method
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Methods for chemical analysis of high purity bismuth Part 1. Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content Inductively coupled plasma-mass spectrum method
ICS 77.120.99
H13
People's Republic of China Nonferrous Metals Industry Standard
Methods for chemical analysis of high purity bismuth
Part 1. copper, lead, zinc, iron, silver, arsenic, tin,
Cadmium, magnesium, chromium, aluminum, gold and nickel contents -
Inductively Coupled Plasma Mass Spectrometry
Part 1. Determinationofcopper, lead, zinc, iron, silver,
arsenic, tin, cadmium, magnesium, chromium, aluminum,
Issued on. 2014-03-01 2013-10-17 implementation
Ministry of Industry and Information Technology of the People's Republic of China released
Foreword
YS/T 923 "purity bismuth chemical analysis method" is divided into two parts.
--- Part 1. copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content - Inductively coupled plasma mass
Spectroscopy;
--- Part 2. Determination of trace element contents of glow discharge mass spectrometry.
This section YS/T Part 1 923.
This section drafted in accordance with GB/T 1.1-2009 given rules.
The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized.
This section is responsible for drafting unit. Beijing Nonferrous Metal Research Institute.
Participated in the drafting of this section. Dongfang Electric Group Emei Semiconductor Materials Co., Ltd., Jinchuan Group Co., Ltd.
The main drafters of this section. Li Po City, Liu Ying, Sun Zeming, Tong Jian, Zang Muwen, Li Na, ZHANG Jin, Zhaoyong Shan, Wen-ying, Liu Aihua, Qiu Ping,
Qinfang Lin.
Methods for chemical analysis of high purity bismuth
Part 1. copper, lead, zinc, iron, silver, arsenic, tin,
Cadmium, magnesium, chromium, aluminum, gold and nickel contents -
Inductively Coupled Plasma Mass Spectrometry
1 Scope
YS/T of the provisions of section 923 of the high-purity bismuth in copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content determination.
This section applies to the copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content in high purity bismuth. Determination of the range in Table 1.
Table 1
Measuring element Measuring range w /% range of elements w /%
Cu 0.00005 ~ 0.0010 Cd 0.00005 ~ 0.0010
Pb 0.00005 ~ 0.0010 Sn 0.00005 ~ 0.0010
Mg 0.00005 ~ 0.0010 Ag 0.00005 ~ 0.0010
Al 0.00005 ~ 0.0010 Au 0.00005 ~ 0.0010
Cr 0.00005 ~ 0.0010 Zn 0.00005 ~ 0.0010
Fe 0.00005 ~ 0.0010 As 0.00005 ~ 0.0010
Ni 0.00005 ~ 0.0010
2 Method summary
The sample is dissolved in nitric acid to thallium internal standard calibration, inductively coupled plasma mass spectrometry directly determined by the working curve method to calculate each
Mass concentration of the element, expressed in mass fraction measurement results.
3 Reagents
Unless otherwise indicated, the reagents used in the tests were excellent pure; water used as a water.
3.1 nitric acid (ρ = 1.42g/mL).
3.2 nitric acid (11).
3.3 copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold, nickel, and thallium single element standard stock solution (national standard sample/national standards
Material), concentration of 1000μg/mL.
3.4 mixed standard solution A. Pipette respectively 10.00mL copper, lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel standard stock solution
(3.3) in 1000mL plastic flask, add 20mL of nitric acid (3.2), dilute to the mark and mix. This solution 1mL copper,
Lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel each 10μg.
3.5 mixed standard solution B. Pipette 10.00mL mixed standard solution A (3.4) in 1000mL plastic flask, add 20mL nitrate
Acid (3.2), dilute to the mark and mix. This solution 1mL copper, lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel each 0.1μg,
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