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YS/T 923.1-2013 English PDF

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YS/T 923.1-2013: Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method
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YS/T 923.1-2013English189 Add to Cart 3 days [Need to translate] Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method Valid YS/T 923.1-2013

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Basic data

Standard ID YS/T 923.1-2013 (YS/T923.1-2013)
Description (Translated English) Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H13
Classification of International Standard 77.120.99
Word Count Estimation 7,789
Regulation (derived from) Ministry of Industry and Information Technology Bulletin No. 52, 2013; industry standard for filing Notice No. 1 of 2014 (No. 169 overall)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the secret of high purity copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content determination. This standard applies to high-purity copper, lead, zinc, iron, silver, arsenic

YS/T 923.1-2013: Methods for chemical analysis of high purity bismuth. Part 1: Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content. Inductively coupled plasma-mass spectrum method



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Methods for chemical analysis of high purity bismuth Part 1. Determination of copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content Inductively coupled plasma-mass spectrum method ICS 77.120.99 H13 People's Republic of China Nonferrous Metals Industry Standard Methods for chemical analysis of high purity bismuth Part 1. copper, lead, zinc, iron, silver, arsenic, tin, Cadmium, magnesium, chromium, aluminum, gold and nickel contents - Inductively Coupled Plasma Mass Spectrometry Part 1. Determinationofcopper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, Issued on. 2014-03-01 2013-10-17 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 923 "purity bismuth chemical analysis method" is divided into two parts. --- Part 1. copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content - Inductively coupled plasma mass Spectroscopy; --- Part 2. Determination of trace element contents of glow discharge mass spectrometry. This section YS/T Part 1 923. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Beijing Nonferrous Metal Research Institute. Participated in the drafting of this section. Dongfang Electric Group Emei Semiconductor Materials Co., Ltd., Jinchuan Group Co., Ltd. The main drafters of this section. Li Po City, Liu Ying, Sun Zeming, Tong Jian, Zang Muwen, Li Na, ZHANG Jin, Zhaoyong Shan, Wen-ying, Liu Aihua, Qiu Ping, Qinfang Lin. Methods for chemical analysis of high purity bismuth Part 1. copper, lead, zinc, iron, silver, arsenic, tin, Cadmium, magnesium, chromium, aluminum, gold and nickel contents - Inductively Coupled Plasma Mass Spectrometry

1 Scope

YS/T of the provisions of section 923 of the high-purity bismuth in copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content determination. This section applies to the copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel content in high purity bismuth. Determination of the range in Table 1. Table 1 Measuring element Measuring range w /% range of elements w /% Cu 0.00005 ~ 0.0010 Cd 0.00005 ~ 0.0010 Pb 0.00005 ~ 0.0010 Sn 0.00005 ~ 0.0010 Mg 0.00005 ~ 0.0010 Ag 0.00005 ~ 0.0010 Al 0.00005 ~ 0.0010 Au 0.00005 ~ 0.0010 Cr 0.00005 ~ 0.0010 Zn 0.00005 ~ 0.0010 Fe 0.00005 ~ 0.0010 As 0.00005 ~ 0.0010 Ni 0.00005 ~ 0.0010

2 Method summary

The sample is dissolved in nitric acid to thallium internal standard calibration, inductively coupled plasma mass spectrometry directly determined by the working curve method to calculate each Mass concentration of the element, expressed in mass fraction measurement results.

3 Reagents

Unless otherwise indicated, the reagents used in the tests were excellent pure; water used as a water. 3.1 nitric acid (ρ = 1.42g/mL). 3.2 nitric acid (11). 3.3 copper, lead, zinc, iron, silver, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold, nickel, and thallium single element standard stock solution (national standard sample/national standards Material), concentration of 1000μg/mL. 3.4 mixed standard solution A. Pipette respectively 10.00mL copper, lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel standard stock solution (3.3) in 1000mL plastic flask, add 20mL of nitric acid (3.2), dilute to the mark and mix. This solution 1mL copper, Lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel each 10μg. 3.5 mixed standard solution B. Pipette 10.00mL mixed standard solution A (3.4) in 1000mL plastic flask, add 20mL nitrate Acid (3.2), dilute to the mark and mix. This solution 1mL copper, lead, zinc, iron, arsenic, tin, cadmium, magnesium, chromium, aluminum, gold and nickel each 0.1μg,

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