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YC/T 585-2019 | English | 169 |
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(Determination of solid content in extracts and concentrates in the production process of reconstituted tobacco)
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YC/T 585-2019
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Basic data Standard ID | YC/T 585-2019 (YC/T585-2019) | Description (Translated English) | (Determination of solid content in extracts and concentrates in the production process of reconstituted tobacco) | Sector / Industry | Tobacco Industry Standard (Recommended) | Classification of Chinese Standard | X85 | Classification of International Standard | 65.160 | Word Count Estimation | 7,734 | Date of Issue | 2019 | Date of Implementation | 2020-01-15 | Issuing agency(ies) | State Tobacco Monopoly Administration |
YC/T 585-2019: (Determination of solid content in extracts and concentrates in the production process of reconstituted tobacco) ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Determination of solid content in extracts and concentrates in the production process of reconstituted tobacco)
ICS 65.160
X85
People's Republic of China Tobacco Industry Standard
Extracts and concentrates from the production process of reconstituted tobacco
Determination of solid content
2019-12-26 released
2020-01-15 implementation
Issued by the State Tobacco Monopoly Administration
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009 and GB/T.20001.4-2015.
Please note that certain contents of this document may involve patents. The issuing agency of this document is not responsible for identifying these patents.
This standard was proposed by the State Tobacco Monopoly Administration.
This standard is under the jurisdiction of the National Tobacco Standardization Technical Committee Cigarette Sub-committee (SAC/TC144/SC1).
Drafting organizations of this standard. China Tobacco Anhui Industrial Co., Ltd., China Tobacco Yunnan Industrial Co., Ltd., China Tobacco Yunnan Reconstituted Tobacco
Limited Liability Company, Fujian China Tobacco Industry Co., Ltd., Zhengzhou Tobacco Research Institute, China Tobacco Standardization Research Center, Guangdong Golden Leaf Technology
Development Co., Ltd., National Tobacco Quality Supervision and Inspection Center, Anhui China Tobacco Reconstituted Tobacco Technology Co., Ltd.
The main drafters of this standard. Ge Shaolin, Wu Lijun, Huang Lan, Wang Baoxing, Xu Yingbo, Xu Guangjin, Li Huajie, Chen Chen, Duan Rumin, Wang Hua,
Chen Gang, Ni Jun, Liu Xiaoping, Liu Jing, Tang Gangling, Zhang Chao, She Shike, Wang Jian, Chen Kaibo, Li Zhengyong, Tang Li, Gao Jun.
Extracts and concentrates from the production process of reconstituted tobacco
Determination of solid content
1 Scope
This standard specifies the method for determination of solid content in extracts and concentrates during the production process of reconstituted tobacco.
This standard applies to the determination of solid content in extracts and concentrates during the production process of reconstituted tobacco, including total solids, soluble solids, and insoluble solids.
2 Normative references
The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this article
Pieces. For undated references, the latest version (including all amendments) applies to this document.
GB/T 6682 Analytical laboratory water specifications and test methods
3 Principle
Take a certain amount of extract or concentrate sample from the production process of reconstituted tobacco and pretreat it with ethanol containing internal standard substance (isopropanol).
The water content of the obtained treated liquid is determined by gas chromatography, and the water content is deducted to be the solid content of the extract or concentrate. Which can
Water-soluble substances are soluble solids, water-insoluble substances are insoluble solids, and the sum of soluble solids and insoluble solids is the total solids.
4 reagent
4.1 The water should meet the requirements of Grade 1 water in GB/T 6682.
4.2 Anhydrous ethanol, the moisture content should be less than 1.0mg/mL.
4.3 Internal standard, isopropanol, with a purity of not less than 99%.
4.4 Pretreatment reagent
Take 12.5mL of the internal standard substance (4.3) and add it to 1L of absolute ethanol (4.2) and mix well.
The pretreatment reagent should be shaken continuously before use to make the moisture even. Pretreatment reagents and test samples used in the preparation of standard working solutions
The pretreatment reagent should be the same batch.
4.5 Standard working solution
Accurately weigh a certain amount of water (4.1), accurate to 0.0001g, in a 50mL conical flask with stopper, add 50mL of pretreatment reagent (4.4),
Mix well to obtain a series of standard working solutions. The standard working solution should be prepared for immediate use. The quality of the recommended series of standard working solutions is shown in Table 1.
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