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YC/T 244-2008 English PDF

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YC/T 244-2008: Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method
Status: Valid
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YC/T 244-2008English209 Add to Cart 3 days [Need to translate] Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method Valid YC/T 244-2008

PDF similar to YC/T 244-2008


Standard similar to YC/T 244-2008

YC/T 243   GB 5606.2   GB/T 5606.1   YC/T 242   YC/T 253   YC/T 236   

Basic data

Standard ID YC/T 244-2008 (YC/T244-2008)
Description (Translated English) Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method
Sector / Industry Tobacco Industry Standard (Recommended)
Classification of Chinese Standard X87
Classification of International Standard 65.160
Word Count Estimation 8,828
Date of Issue 2008-04-14
Date of Implementation 2008-04-14
Quoted Standard GB/T 5606.1; GB/T 19616; YC/T 31
Issuing agency(ies) State Tobacco Monopoly Administration
Summary This standard specifies the tobacco and tobacco products in the 1, 2 propylene glycol, glycerin and sorbitol by HPLC method. This standard applies to tobacco and tobacco products in the 1, 2 propylene glycol, glycerin and sorbitol determination. This standard does not apply to other humectants added to tobacco and tobacco products.

YC/T 244-2008: Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Tobacco and tobacco products.Determination of 1, 2-propylene glycol, glycerol and sorbitol.High performance liquid chromatographic method ICS 65.160 X87 Record Number. 23583-2008 People's Republic of China tobacco industry standards Tobacco and tobacco products 1,2-propanediol, glycerol, and Sorbitol by HPLC Posted 2008-04-14 2008-04-14 implementation State Tobacco Monopoly Bureau issued

Foreword

Tobacco and tobacco products Determination of 1,2-propanediol, the standard reference CORESTA recommended method No. 61 "high-performance liquid chromatography, prop Glycerin and sorbitol content "to develop. Appendix A of this standard is an informative annex. This standard was proposed by the State Tobacco Monopoly Bureau. This standard by the National Standardization Technical Committee on Tobacco (TC144) centralized. This standard was drafted. National Tobacco Quality Supervision and Inspection Center, the Guangdong Tobacco Industry Co., Ltd., Hongta Tobacco (Group) Co., Liability company. The main drafters of this standard. Gang Tang Ling, Konghao Hui, Qin Yunhua, Zhao Hui, Pang Yongqiang, while according to the sun, light Shen Lin, Hu Qingyuan. Tobacco and tobacco products 1,2-propanediol, glycerol, and Sorbitol by HPLC

1 Scope

This standard specifies a high performance liquid chromatographic method of tobacco and tobacco products in propylene glycol, glycerin and sorbitol. This standard applies to tobacco and tobacco products - Determination of propylene glycol, glycerin and sorbitol. This standard does not apply to add other humectants tobacco and tobacco products.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 5606.1 cigarette - Part 1. Sampling General principles GB/T 19616 batches of raw tobacco samples (GB/T 19616-2004, ISO 4874.2000, MOD) Preparation and water YC/T 31 samples of tobacco and tobacco products - Determination oven method Principle 3 Extracted with water in a sample of 1,2-propylene glycol, glycerin and sorbitol, purified extract was filtered with the use of a differential refractive index detector High performance liquid chromatograph, using external standard.

4 Reagents and materials

4.1 Use analytical grade reagents. 4.2 Water, or other secondary distilled water of the same quality. 4.3 disodium edetate calcium (Ca, Na-EDTA). 4.4 1,2-propanediol, should not be less than 99.5% purity, it should be stored in a desiccator. 4.5 glycerol, purity should not be less than 99.5%, it should be stored in a desiccator. 4.6 Sorbitol purity should not be less than 99.5%, should be stored in a desiccator. 4.7 diatomaceous earth, the particle size not greater than 5μm. 4.8 standard solution 4.8.1 Mixed stock solution Weigh about 0.25g of 1,2-propanediol (4.4), glycerol (4.5) and sorbitol (4.6), accurate to 0.0001g, placed 250mL flask with water (4.2) to the mark after the shake. Mixed stock solution should be stored in the dark at 0 ℃ ~ 5 ℃ condition, at least Stable 12d. 4.8.2 Working standard solution Pipette a certain volume of stock solution was mixed with (4.8.1), water (4.2) diluted to volume. Preparing at least five standard solutions, which The concentration range should cover the expected content detected in a sample of 1,2-propylene glycol, glycerin and sorbitol.

5 Instruments

5.1 Analytical balance, accurate to 0.1mg.

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