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Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method
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YC/T 244-2008
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Basic data Standard ID | YC/T 244-2008 (YC/T244-2008) | Description (Translated English) | Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method | Sector / Industry | Tobacco Industry Standard (Recommended) | Classification of Chinese Standard | X87 | Classification of International Standard | 65.160 | Word Count Estimation | 8,828 | Date of Issue | 2008-04-14 | Date of Implementation | 2008-04-14 | Quoted Standard | GB/T 5606.1; GB/T 19616; YC/T 31 | Issuing agency(ies) | State Tobacco Monopoly Administration | Summary | This standard specifies the tobacco and tobacco products in the 1, 2 propylene glycol, glycerin and sorbitol by HPLC method. This standard applies to tobacco and tobacco products in the 1, 2 propylene glycol, glycerin and sorbitol determination. This standard does not apply to other humectants added to tobacco and tobacco products. |
YC/T 244-2008: Tobacco and tobacco products. Determination of 1, 2-propylene glycol, glycerol and sorbitol. High performance liquid chromatographic method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Tobacco and tobacco products.Determination of 1, 2-propylene glycol, glycerol and sorbitol.High performance liquid chromatographic method
ICS 65.160
X87
Record Number. 23583-2008
People's Republic of China tobacco industry standards
Tobacco and tobacco products 1,2-propanediol, glycerol, and
Sorbitol by HPLC
Posted 2008-04-14
2008-04-14 implementation
State Tobacco Monopoly Bureau issued
Foreword
Tobacco and tobacco products Determination of 1,2-propanediol, the standard reference CORESTA recommended method No. 61 "high-performance liquid chromatography, prop
Glycerin and sorbitol content "to develop.
Appendix A of this standard is an informative annex.
This standard was proposed by the State Tobacco Monopoly Bureau.
This standard by the National Standardization Technical Committee on Tobacco (TC144) centralized.
This standard was drafted. National Tobacco Quality Supervision and Inspection Center, the Guangdong Tobacco Industry Co., Ltd., Hongta Tobacco (Group) Co.,
Liability company.
The main drafters of this standard. Gang Tang Ling, Konghao Hui, Qin Yunhua, Zhao Hui, Pang Yongqiang, while according to the sun, light Shen Lin, Hu Qingyuan.
Tobacco and tobacco products 1,2-propanediol, glycerol, and
Sorbitol by HPLC
1 Scope
This standard specifies a high performance liquid chromatographic method of tobacco and tobacco products in propylene glycol, glycerin and sorbitol.
This standard applies to tobacco and tobacco products - Determination of propylene glycol, glycerin and sorbitol.
This standard does not apply to add other humectants tobacco and tobacco products.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 5606.1 cigarette - Part 1. Sampling
General principles GB/T 19616 batches of raw tobacco samples (GB/T 19616-2004, ISO 4874.2000, MOD)
Preparation and water YC/T 31 samples of tobacco and tobacco products - Determination oven method
Principle 3
Extracted with water in a sample of 1,2-propylene glycol, glycerin and sorbitol, purified extract was filtered with the use of a differential refractive index detector
High performance liquid chromatograph, using external standard.
4 Reagents and materials
4.1 Use analytical grade reagents.
4.2 Water, or other secondary distilled water of the same quality.
4.3 disodium edetate calcium (Ca, Na-EDTA).
4.4 1,2-propanediol, should not be less than 99.5% purity, it should be stored in a desiccator.
4.5 glycerol, purity should not be less than 99.5%, it should be stored in a desiccator.
4.6 Sorbitol purity should not be less than 99.5%, should be stored in a desiccator.
4.7 diatomaceous earth, the particle size not greater than 5μm.
4.8 standard solution
4.8.1 Mixed stock solution
Weigh about 0.25g of 1,2-propanediol (4.4), glycerol (4.5) and sorbitol (4.6), accurate to 0.0001g, placed
250mL flask with water (4.2) to the mark after the shake. Mixed stock solution should be stored in the dark at 0 ℃ ~ 5 ℃ condition, at least
Stable 12d.
4.8.2 Working standard solution
Pipette a certain volume of stock solution was mixed with (4.8.1), water (4.2) diluted to volume. Preparing at least five standard solutions, which
The concentration range should cover the expected content detected in a sample of 1,2-propylene glycol, glycerin and sorbitol.
5 Instruments
5.1 Analytical balance, accurate to 0.1mg.
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