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Food contact materials - Polymers - Determination of BADGE, BFDGE and their hydroxy and chlorinated derivatives in food simulants - Liquid chromatography-tandem mass spectrometry
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SN/T 4084-2014
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Basic data Standard ID | SN/T 4084-2014 (SN/T4084-2014) | Description (Translated English) | Food contact materials - Polymers - Determination of BADGE, BFDGE and their hydroxy and chlorinated derivatives in food simulants - Liquid chromatography-tandem mass spectrometry | Sector / Industry | Commodity Inspection Standard (Recommended) | Classification of Chinese Standard | X08 | Classification of International Standard | 67.250 | Word Count Estimation | 9,949 | Date of Issue | 12/1/2014 | Date of Implementation | 5/1/2015 | Quoted Standard | GB/T 6682; GB/T 23296.1 | Regulation (derived from) | State-Quality-Inspection-accreditation [2014] 614 | Issuing agency(ies) | General Administration of Customs | Summary | This standard specifies the food simulants bisphenol A- diglycidyl ether (bisphenol A diglycidyl ether, referred to as BADGE), bisphenol F- diglycidyl ether (bisphenol F diglycidyl ether, referred BFDGE) and its hydroxy and chlorinated derivatives by liqu |
SN/T 4084-2014: Food contact materials - Polymers - Determination of BADGE, BFDGE and their hydroxy and chlorinated derivatives in food simulants - Liquid chromatography-tandem mass spectrometry
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(Food contact materials - Polymer food simulants BADGE, BFDGE and their hydroxy and chlorinated derivatives measured by liquid chromatography - mass spectrometry/mass spectrometry)
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Food contact materials - Polymer
Food simulants BADGE, BFDGE and
Determination of hydroxy and chlorinated derivatives
Liquid chromatography - mass spectrometry/mass spectrometry
Foodcontactmaterials-Polymers-DeterminationofBADGE, BFDGEand
Issued on. 2014-11-19
2015-05-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Shandong CIQ.
The main drafters of this standard. Sunzhong Song, Liu Jingjing, Wang Tong territory, Zhaozu Liang, Wang Haibing.
Food contact materials - Polymer
Food simulants BADGE, BFDGE and
Determination of hydroxy and chlorinated derivatives
Liquid chromatography - mass spectrometry/mass spectrometry
1 Scope
This standard specifies the food simulants bisphenol A- diglycidyl ether (bisphenolAdiglycidylether, called BADGE), bis
Phenol F- diglycidyl ether (bisphenolFdiglycidylether, referred BFDGE) and its hydroxy and chlorinated derivatives by liquid chromatography - mass
Spectroscopy/mass spectrometry.
This standard applies to food simulant 3% (mass fraction) solution of acetic acid, 10% (by volume) ethanol, 20% (volume fraction) B
Alcohol solution, 50% (by volume) ethanol, olive oil, diglycidyl ether of bisphenol A- (bisphenolAdiglycidylether), bisphenol
F- diglycidyl ether (bisphenolFdiglycidylether) determination and its hydroxy and chlorinated derivatives.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
GB/T 23296.1 plastic food contact materials in plastics restricted substances test substance specific migration into foods and food simulants
Experience and determination method and conditions of exposure to food simulants Guide selection
3 Method summary
Food simulants bisphenol A- diglycidyl ether, diglycidyl ether of bisphenol F- its hydroxy and chlorinated derivatives by liquid chromatography
Spectrum - MS/MS separation and determination. 3% (mass fraction) solution of acetic acid, 10% (by volume) ethanol, 20% (volume fraction) ethanol
Solution, 50% (volume fraction) ethanol four kinds of aqueous food simulants with direct injection method, olive oil was extracted with acetonitrile mimics backward sample test
Fixed, external standard.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 stipulated.
4.1 Bisphenol A- diglycidyl ether (BADGE). CAS No. 1675-54-3, purity of greater than or equal to 99%.
4.2 bisphenol A- bis (2,3-dihydroxypropyl) ether (BADGE · 2H2O). CAS No. 5581-32-8, purity of greater than or equal to 99%.
4.3 Bisphenol A- (2,3- dihydroxypropyl) ether (BADGE · H2O). CAS No. 76002-91-0, purity of greater than or equal
At 99%.
4.4 Bisphenol A- bis (3-chloro-2-hydroxypropyl) ether (BADGE · 2HCl). CAS No. 4809-35-2, purity of greater than or equal to 99%.
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