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US$209.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3318.1-2012: Chemical analysis of zircon. Part 1: Determination of Thorium, Uranium. Inductively coupled plasma atomic emission spectrometry Status: Valid
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Chemical analysis of zircon. Part 1: Determination of Thorium, Uranium. Inductively coupled plasma atomic emission spectrometry
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SN/T 3318.1-2012
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Basic data | Standard ID | SN/T 3318.1-2012 (SN/T3318.1-2012) | | Description (Translated English) | Chemical analysis of zircon. Part 1: Determination of Thorium, Uranium. Inductively coupled plasma atomic emission spectrometry | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | Q40 | | Word Count Estimation | 8,850 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | National Quality Inspection (2012) 777; industry standard filing Notice 2013 No. 4 (No. 160 overall) | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the inductively coupled plasma atomic emission spectrometry (ICP-AES) Determination of zircon sand export thorium, uranium content approach. This standard applies to import zircon sand in thorium, uranium and the determination of t |
SN/T 3318.1-2012: Chemical analysis of zircon. Part 1: Determination of Thorium, Uranium. Inductively coupled plasma atomic emission spectrometry ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical analysis of zircon.Part 1. Determination of Thorium, Uranium.Inductively coupled plasma atomic emission spectrometry
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Zircon chemical analysis methods - Part 1.
Inductively coupled thorium, uranium content
Plasma atomic emission spectrometry
Chemicalanalysisofzircon-Part 1. DeterminationofThorium, Uranium-
Issued on. 2012-12-12
2013-07-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This section SN/T 3318 Part 1.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section proposed and managed by the National Certification and Accreditation Administration Committee.
This section was drafted by. People's Republic of China, Xiamen CIQ.
The main drafters of this section. Heron Cai Yan, Pan honest, Laitian Yue, Yangming Kun, Cai Yanping.
Zircon chemical analysis methods - Part 1.
Inductively coupled thorium, uranium content
Plasma atomic emission spectrometry
1 Scope
SN/T 3318 This section provides an inductively coupled plasma atomic emission spectrometry (ICP-AES) Determination of the import and export of thorium zircon sand,
The method of uranium content.
This section applies to the import and export of zircon sand thorium, uranium content determination, the detection limit of the elements are as follows. 0.011% thorium, uranium
0.018%.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Sample with sodium carbonate - mixing borax flux melting frit leaching with hydrochloric acid, and diluted to a predetermined volume. Inductively coupled plasma
Atomic emission spectrometer intensity measured elements, according to the standard solution prepared working curve calculated from the concentration of each element. Then according to the concentration
Degree, the quality of the sample and the sample solution volume, calculate the amount of each element in a sample.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade, water as a secondary water GB/T 6682 regulations.
4.1 hydrochloric acid (ρ = 1.19g/mL).
4.2 thorium standard solution (national certified reference material). 1000μg/mL.
4.3 uranium standard solution (national certified reference material). 100μg/mL.
4.4 zirconium oxychloride.
4.5 sodium carbonate.
4.6 borax.
4.7 hydrochloride (13).
4.8 Zr substrate solution (1mg/mL). Weigh 3.53g of zirconium oxychloride (4.4), was added 50mLHCl (1 3) (4.7), dissolved by heating, will be
Capacity in 1000mL volumetric flask.
4.9 mixed flux. Weigh sodium carbonate (4.6), borax (4.7) by mass ratio of 1/1 were mixed and finely ground, into a plastic bottle into the dryer
Saved.
4.10 curve solution. Add 40mL zirconium matrix solution (4.8) in a 100mL flask, 30mLHCl (4.7), 0.8g
Mixed flux (4.9), respectively, and then draw a certain amount of each standard solution (4.2, 4.3) in the flask, diluted with water to the mark. Wait
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