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SN/T 2266-2009 English PDF

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SN/T 2266-2009: Determination of glyphosate-isopropylammonium in roundup. High performance liquid chromatography
Status: Valid
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SN/T 2266-2009English169 Add to Cart 3 days [Need to translate] Determination of glyphosate-isopropylammonium in roundup. High performance liquid chromatography Valid SN/T 2266-2009

PDF similar to SN/T 2266-2009


Standard similar to SN/T 2266-2009

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Basic data

Standard ID SN/T 2266-2009 (SN/T2266-2009)
Description (Translated English) Determination of glyphosate-isopropylammonium in roundup. High performance liquid chromatography
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard G23
Classification of International Standard 65.100
Word Count Estimation 6,624
Date of Issue 2009-02-20
Date of Implementation 2009-09-01
Regulation (derived from) National Quality Inspection [2009] No. 67
Issuing agency(ies) General Administration of Customs
Summary This standard specifies Roundup Lin isopropylamine salt of glyphosate content liquid chromatography method. This standard applies to 41% water emulsion glyphosate isopropylamine salt of glyphosate Lin content.

SN/T 2266-2009: Determination of glyphosate-isopropylammonium in roundup. High performance liquid chromatography


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of glyphosate-isopropylammonium in roundup.High performance liquid chromatography Exit inspection and quarantine industry standard book People's Republic of China Determination Roundup Glyphosate isopropylamine salt content High Performance Liquid Chromatography Posted 2009-02-20 2009-09-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

Appendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Guangdong CIQ. The main drafters of this standard. Liu Yingfeng, Homocysteine on ZHOU Ming-hui, Di Cuiping, Zheng Jianguo. This standard is the first release of the entry-exit inspection and quarantine industry standards. Determination Roundup Glyphosate isopropylamine salt content High Performance Liquid Chromatography

1 Scope

This standard specifies the liquid chromatographic method Roundup Glyphosate isopropylamine salt content. This standard applies to the determination of glyphosate 41% aqueous emulsion of glyphosate isopropylamine salt content.

2 Method summary

This method uses high performance liquid chromatography, after the samples were separated by strong cation exchange column using a diode array detector, with reservations Time qualitative and quantified by external standard method.

3 Reagents and materials

Unless otherwise indicated, in the analysis double-distilled water. 3.1 potassium dihydrogen phosphate. AR. 3.2 Methanol. HPLC grade. 3.3 phosphoric acid. 85%. Glyphosate 3.4 Sample. Glyphosate mass fraction ≥99.0% (glyphosate, CASN o. 1071-83-6). 3.5 potassium dihydrogen phosphate buffer solution. Weigh 0.8437g potassium dihydrogen phosphate (accurate to 0.0002g), in 1000mL volumetric flask, add Into 900mL of water, with 85% phosphoric acid adjusted to pH 1.9, was added 40mL of methanol to volume with water, shake, before the machine using 0.45μm Filtration membrane. 3.6 quality nylon or regenerated cellulose membrane filter. 0.45μm, the diameter of 47mm. 3.7 syringe filter. 0.45μm, the diameter of 13mm.

4 instruments and equipment

4.1 high performance liquid chromatography with diode array detector or a UV detector. 4.2 Column. SynChropakS300 strong cation exchange column, 100mm × 4.6mm (inside diameter), 6μm or equivalent other strong Cation exchange column. 4.3 filter device. 4.4 vacuum pump. 4.5 ultrasonic cleaner.

5 chromatographic operating conditions

a) Column. SynChropakS300 column, 100mm × 4.6mm (inside diameter), 6μm; b) Mobile phase. potassium dihydrogen phosphate buffer solution/methanol 95 + 5 = (1 + Vp Vp 2); c) flow rate. 0.5mL/min; d) Column temperature. 40 ℃; e) Injection volume. 20.0μL; f) detection wavelength. 195nm; g) retention time. about 2.5min.

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