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SN/T 0146-2016

Chinese Standard: 'SN/T 0146-2016'
Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusRelated Standard
SN/T 0146-2016English599 Add to Cart Days<=6 Determination of BHC and DDT in tobacco and tobacco products for export Valid SN/T 0146-2016
SN/T 0146-2016Chinese28 Add to Cart <=1-day [PDF from Chinese Authority, or Standard Committee, or Publishing House]

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Detail Information of SN/T 0146-2016; SN/T0146-2016
Description (Translated English): Determination of BHC and DDT in tobacco and tobacco products for export
Sector / Industry: Commodity Inspection Standard (Recommended)
Word Count Estimation: 26,294
Date of Issue: 2016-08-23
Date of Implementation: 2017-03-01
Older Standard (superseded by this standard): SN 0146-1992
Drafting Organization: Shanghai Entry-Exit Inspection and Quarantine Bureau, People's Republic of China
Administrative Organization: Certification and Accreditation Administration of the People's Republic of China
Regulation (derived from): State-Quality-Inspection-Certification (2016)438
Proposing organization: Certification and Accreditation Administration of the People's Republic of China
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China


SN/T 0146-2016
Determination of BHC and DDT in tobacco and tobacco products for export
People's Republic of China Exit Inspection and Quarantine standards
Replacing SN 0146-1992
Exports of tobacco and tobacco products in six six six,
DDT residue detection method
2016-08-23 released
2017-03-01 Implementation
People's Republic of China
General Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard replaces SN 0146-1992 "export tobacco leaves and tobacco products in the six six six DDT residue test methods." versus
SN 0146-1992 compared to editorial changes in addition to the main technical changes are as follows.
--- Modify the sample extraction method;
--- Determination of the sample was changed to a capillary column chromatography column;
--- Added GC-MS confirmation method;
--- omitted the sampling steps.
Please note that some of this document may be patentable. The issuing agencies of this document do not bear the responsibility of identifying these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted by Shanghai Entry-Exit Inspection and Quarantine Bureau, People's Republic of China.
The main drafters of this standard. When Yi Yin, Yang Huiqin, Sheng Yong Gang, Cao Chen, Yi Xiong Hai, Zhu Jian.
This standard replaces the standards previously issued as.
--- SN 0146-1992.
Exports of tobacco and tobacco products in six six six,
DDT residue detection method
1 Scope
This standard specifies the export of tobacco and tobacco products in BHC, DDT determination and confirmation methods.
This standard applies to the export of tobacco and tobacco products in BHC, DDT residues detection and confirmation.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 6682 analytical laboratory water specifications and test methods
3 method summary
Residues of the six six six, DDT with acetone - n-hexane ultrasonic extraction, the extract was concentrated sulfuric acid sulfonated, with electronic capture detection
Gas chromatography, external standard quantitative, if necessary, confirmed by gas chromatography - mass spectrometry.
4 reagent material
Unless otherwise indicated, the reagents used are of analytical grade, water is a water GB/T 6682 regulations.
4.1 acetone. Chromatography pure.
4.2 n-hexane. Chromatographic purity.
4.3 concentrated sulfuric acid.
4.4 anhydrous sodium sulfate. Burned at 650 ℃ 4h, cooled and stored in a closed container.
4.5 acetone - n-hexane (1 1, volume ratio) solution amount of 500mL of acetone and 500mL n-hexane to 1000mL reagent bottle.
4.6 2% sodium sulfate solution Weigh 20g of anhydrous sodium sulfate dissolved in water, constant volume to 1000mL.
4.7 Pesticide Standard Substance Alpha-BHC (α-BHC, CAS No.319-84-6); β-BHC (CAS No.319-85-7); γ-
(P, p ', p'-dihydropyridyl) hexahydrate (γ-BHC, CAS No. 58-89-9) -DDD, CAS
(P, p'-DDE, CAS No. 72-55-9); o, p'-DDT (o, p'-DDT, CAS No.789789-
6); p, p'-DDT (p, p'-DDT, CAS No.50-29-3) with purity greater than 98%.
4.8 Preparation of standard stock solution were weighed about 0.01g (accurate to 0.0001g) α-BHC, β-BHC, γ-BHC, δ-BHC
Sixth, p, p'-drops, p, p'-drops Iraq, o, p'- DDT and p, p'- DDT standards in 10mL volumetric flask, with n-hexane
Preparation of about 1000μg/mL standard stock solution, less than 5 ℃ dark storage.
4.9 Preparation of mixed standard intermediate solution Each pipette the standard stock solution 1.00mL to 100mL volumetric flask with n-hexane
Release to the mark, now with the current use.
5 instruments and equipment
5.1 Gas Chromatograph with Electronic Capture (ECD) Detector.
Related standard:   SN/T 0173-2018  SN/T 0306.1-2018
   
 
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