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Metrological Technical Specification for Purity Assessment of Certified Reference Materials - High Purity Metal Certified Reference Materials
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JJF 1961-2022
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Standard similar to JJF 1961-2022 JJF 1033 JJF 1050 JJF 1030
Basic data Standard ID | JJF 1961-2022 (JJF1961-2022) | Description (Translated English) | Metrological Technical Specification for Purity Assessment of Certified Reference Materials - High Purity Metal Certified Reference Materials | Sector / Industry | Metrology & Measurement Industry Standard | Word Count Estimation | 20,297 | Date of Issue | 2022-04-29 | Date of Implementation | 2022-10-29 | Issuing agency(ies) | State Administration for Market Regulation |
JJF 1961-2022: Metrological Technical Specification for Purity Assessment of Certified Reference Materials - High Purity Metal Certified Reference Materials ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Metrological Technical Specification for Purity Assessment of Certified Reference Materials - High Purity Metal Certified Reference Materials
National Metrology Technical Specifications of the People's Republic of China
Purity standard substance definite value measurement technical specification
High purity metal purity reference material
Released on 2022-04-29
Implementation on 2022-10-29
Released by the State Administration for Market Regulation
Purity standard substance definite value measurement technical specification
High purity metal purity reference material
Responsible unit. National Standard Substance Metrology Technical Committee
Main drafting unit. China Institute of Metrology
Participating in the drafting unit. Shanghai Materials Research Institute
National Standard (Beijing) Inspection and Certification Co., Ltd.
Steel Research Nanoco Testing Technology Co., Ltd.
This specification entrusts the National Standard Substance Metrology Technical Committee to be responsible for interpretation
The main drafters of this specification.
Zhou Tao (National Institute of Metrology)
Cui Yanjie (National Institute of Metrology)
Wu Bing (National Institute of Metrology)
Zhang Jianying (National Institute of Metrology)
Participating drafters.
Ma Chongxian (Shanghai Materials Research Institute)
Chen Xiongfei (GB (Beijing) Inspection and Certification Co., Ltd.)
Tang Benling (Steel Research Nanoco Testing Technology Co., Ltd.)
Table of contents
Introduction (Ⅱ)
1 Scope(1)
2 References(1)
3 terms(1)
4 General requirements(1)
4.1 Screening and pretreatment of reference material candidates (1)
4.2 Qualitative analysis of reference materials (1)
4.3 Principles of Purity Valuation Method (1)
5 Classification, principle and key points of valuation methods (2)
5.1 Direct measurement method(2)
5.2 Impurity element deduction method (3)
6 Evaluation of fixed value and uncertainty (4)
6.1 Statutory value of deduction of impurity elements (4)
6.2 Coulomb value(5)
6.3 Combined Standard Uncertainty and Expanded Uncertainty(7)
7 Metrological traceability(7)
8 Value expression (8)
Appendix A Examples of High Purity Copper Purity Determination (9)
Introduction
This specification is used to standardize the denomination of high-purity metal purity standard substances in my country.
This specification is published for the first time.
Purity standard substance definite value measurement technical specification
High purity metal purity reference material
1 Scope
This specification is applicable to the development of high-purity metal purity standard substances, and the determination of pure metal purity can also refer to
use.
2 References
This specification references the following documents.
General terms and definitions of JJF 1005 reference materials
JJF 1342 General requirements for reference material development (production) institutions
JJF 1343 General Principles and Statistical Principles for Valuation of Standard Substances
JJF 1507 Selection and application of reference materials
For dated references, only the dated version applies to this specification; for undated references
document, its latest version (including all amendments) applies to this specification.
3 terms
The terms and definitions defined in JJF 1005 and below apply to this specification.
The proportion of main elements in high-purity metals is usually expressed in mass fraction (% or g/g) and its multiples.
On the premise that the sum of the element mass fractions is 100%, by subtracting the total amount of all impurity elements, the
Method for obtaining the chemical purity value of an element.
4 General requirements
4.1 Screening and pretreatment of standard substance candidates
4.1.1 Under the premise of reasonable cost, select samples with relatively high purity, good uniformity and stability.
NOTE. Can be commercially available, custom-made, or re-prepared samples.
4.1.2 Samples should be in a form that is easy to clean the surface (such as columns, flakes, chips, etc.), to reduce the possibility of contamination such as cutting
operate.
Note. The selection of samples should avoid the powder form, and consider the convenience of weighing and adapt to the measurement method.
4.1.3 Before the sample is measured, the surface should be cleaned according to an appropriate method to remove surface pollutants and oxide layers.
4.2 Qualitative analysis of reference materials
Qualitative analysis was performed by mass spectrometry or spectroscopy to ensure that the element types of the main components of the candidates meet the expected requirements.
4.3 Principles of Purity Valuation Method
4.3.1 Two methods can be used to measure the purity of pure metals. one is the direct measurement method, which directly measures the content of main elements;
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