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GB/T 8661-2008: Plastics -- Styrene/acrylonitrile copolymers -- Determination of residual acrylonitrile monomer content -- Gas chromatography method
Status: Valid GB/T 8661: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 8661-2008 | English | 229 |
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Plastics -- Styrene/acrylonitrile copolymers -- Determination of residual acrylonitrile monomer content -- Gas chromatography method
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GB/T 8661-2008
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| GB/T 8661-1988 | English | 239 |
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Determination of residual acrylonitrile monomer content in acrylonitrile-butadiene-styrene resin by gas chromatography
| Obsolete |
GB/T 8661-1988
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PDF similar to GB/T 8661-2008
Basic data | Standard ID | GB/T 8661-2008 (GB/T8661-2008) | | Description (Translated English) | Plastics -- Styrene/acrylonitrile copolymers -- Determination of residual acrylonitrile monomer content -- Gas chromatography method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G31 | | Classification of International Standard | 83.080 | | Word Count Estimation | 10,160 | | Date of Issue | 2008-06-19 | | Date of Implementation | 2009-02-01 | | Older Standard (superseded by this standard) | GB/T 8661-1988 | | Quoted Standard | ISO 2561 | | Adopted Standard | ISO 4581-1994, MOD | | Regulation (derived from) | National Standard Approval Announcement 2008 No.10 (Total No.123) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination by gas chromatography styrene-acrylonitrile copolymers and blends residual acrylonitrile monomer content approach. This standard applies to the determination of styrene/acrylonitrile copolymers and blends residual acrylonitrile monomer content. | GB/T 8661-2008: Plastics -- Styrene/acrylonitrile copolymers -- Determination of residual acrylonitrile monomer content -- Gas chromatography method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Plastics. Styrene/acrylonitrile copolymers. Determination of residual acrylonitrile monomer content. Gas chromatography method
ICS 83.080
G31
National Standards of People's Republic of China
Replacing GB/T 8661-1988
Plastic styrene - acrylonitrile copolymer
Determination of residual acrylonitrile monomer content
Gas chromatography
(ISO 4581.1994, MOD)
Posted 2009-02-01 2008-06-19 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This revised standard adopts ISO 4581.1994 test "Plastic --- styrene/acrylonitrile copolymers --- residual acrylonitrile monomer content
Set --- GC "(in English).
This standard and ISO 4581.1994 as compared to the main differences are as follows.
--- Instrument "GC" added article note, indicating that you can use to achieve the same separation capillary column (5.1);
--- According to domestic specifications flask, the flask 20mL to 25mL volumetric flask, and the corresponding calculation formula has been modified
(8.1).
This standard replaces GB/T 8661-1988 "was measured by gas chromatography acrylonitrile - butadiene - styrene (ABS) resin residual acrylamide
Nitrile monomer content ", and GB/T 8661-1988 The main differences are as follows.
--- Extends the scope of this standard applies not only to the determination of acrylonitrile - butadiene - styrene (ABS) resin residual acrylonitrile monomer
Content, but also for the determination of styrene - acrylonitrile copolymer (SAN) resin residual acrylonitrile monomer content;
--- Instrument "GC" added article note, indicating that you can use to achieve the same separation capillary column;
--- According to domestic specifications flask, the flask 20mL to 25mL volumetric flask, and the corresponding calculation formula has been modified;
--- Added Appendix A "Determination of acrylonitrile content of less than 3mg/kg of headspace gas chromatography (NPD)."
Appendix A of this standard is an informative annex.
The standard proposed by China Petroleum and Chemical Corporation.
This standard by the National Standardization Technical Committee plastic plastic resins and petrochemical products Club (SAC/TC15/SC1) centralized.
This standard was drafted. China PetroChina Lanzhou Petrochemical Company company.
The main drafters of this standard. Yangwei Yan, Zou Liqiong, Europe Jun Jun, Zhaojun Xia, Wang is.
This standard was first released in January 1988, this revision is the first time.
Plastic styrene - acrylonitrile copolymer
Determination of residual acrylonitrile monomer content
Gas chromatography
1 Scope
This standard specifies the determination by gas chromatography styrene - acrylonitrile copolymers and blends of residual acrylonitrile monomer content approach.
This standard applies to the determination of styrene/acrylonitrile copolymers and blends of residual acrylonitrile monomer content.
2 normative documents Applications
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequently
Some amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Study whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
ISO 2561 Determination of polystyrene and impact polystyrene plastic --- residual styrene monomer --- Gas Chromatography
Principle 3
With dimethyl formamide sample was dissolved, the solution was injected into a small volume equipped with a flame ionization detector gas chromatograph to points
Isolation and detection of volatile components. Propionitrile or acetonitrile containing a known amount of solvent as internal standard. This method is suitable for the acrylonitrile content
Not less than 3mg/kg of the case, to make the determination to reach the lower limit of 0.3mg/kg ~ 0.4mg/kg, can be selected A method Appendix. in
Appendix A, the sample was dissolved in 1,2-propylene carbonate (PC), and the solution was poured into a NPD gas chromatograph in order propionitrile
As an internal standard.
4 Reagents
During the test, use only approved analytical grade reagents. When using the following reagents to be very careful, especially acrylonitrile.
4.1-dimethyl formamide. purity in the retention time of the test substance can not have impurity peaks.
4.2 propionitrile. if they can prove the same results obtained can be used in place of acetonitrile, propionitrile as an internal standard.
4.3 Acrylonitrile. chromatography.
5 Instruments
5.1 Gas chromatograph. equipped with a flame ionization detector gas chromatography.
GC test conditions.
Column. recommended length 1m ~ 2m, an inner diameter of 3mm ~ 4mm stainless steel or glass, with a diameter of 150μm ~ 270μm
(Ie, 50 mesh to 100 mesh) PorapakQ1) fill. In order to prevent non-volatile matter in solution into the column, you can take the appropriate method, for example,
Such as. inlet plus a glass liner or install a replacement handy 5cm long preliminary column (the column with the same packing material).
Column filling method not specified, but the requirements get satisfactory separation, column 24h to aging at 230 ℃ in the air stream.
If they can prove the same results obtained, the size of the column may be different.
Column (if the column preparation, including preparatory column) Temperature. 160 ℃ ~ 180 ℃.
1) PorapakQ Milipore company is a trade name. This information is provided of this standard provide users with convenient, according to the agreements concerned, you can use
The same performance alternative.
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