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GB/T 38139-2019 English PDF

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GB/T 38139-2019: Test methods for liquid raw materials of cement grinding aids - Gas chromatography
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PDF similar to GB/T 38139-2019


Standard similar to GB/T 38139-2019

GB/T 40376   GB/T 41060   GB/T 39701   GB/T 31289   GB/T 38140   

Basic data

Standard ID GB/T 38139-2019 (GB/T38139-2019)
Description (Translated English) Test methods for liquid raw materials of cement grinding aids - Gas chromatography
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard Q11
Classification of International Standard 91.100.10
Word Count Estimation 14,188
Date of Issue 2019-10-18
Date of Implementation 2020-09-01
Issuing agency(ies) State Administration for Market Regulation, China National Standardization Administration

GB/T 38139-2019: Test methods for liquid raw materials of cement grinding aids - Gas chromatography


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Test methods for liquid raw materials of cement grinding aids--Gas chromatography ICS 91.100.10 Q11 National Standards of People's Republic of China Liquid raw material composition for cement grinding aid production Determination method gas chromatography Published on.2019-10-18 2020-09-01 implementation State market supervision and administration China National Standardization Administration issued

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard was proposed by the China Building Materials Federation. This standard is under the jurisdiction of the National Cement Standardization Technical Committee (SAC/TC184). This standard was drafted. China Building Materials Science Research Institute Co., Ltd., Hunan Xijiesi Building Materials Technology Co., Ltd., China Resources Cement Technology Development (Guangxi) Co., Ltd., Sichuan Xinlingling Concrete Co., Ltd., Zhengzhou Wanglou Cement Industry Co., Ltd., Hunan University, Shenzhen Hongchao Technology Co., Ltd., Beijing Jinyu Cement Energy Saving Technology Co., Ltd., Jiangsu Yongtai Construction Engineering Co., Ltd., Chongqing Chenhe Building Engineering Co., Ltd., Tangshan Jidong Cement Admixture Co., Ltd., Chongqing Construction Engineering No. 8 Construction Co., Ltd., Hubei Jianke International Cheng Co., Ltd., Luoyang Aositesite Cement Technology Co., Ltd. The main drafters of this standard. Jiang Lizhen, Shi Caijun, Du Yong, Long Lan, Zhu Wenshang, Wang Haibo, Zeng Rong, Zhang Dakang, Jing Dongyu, Zeng Jun, Zhu Shuiyong, Teng Zhuoguang, Lin Xunhuang, Liu Qinghe, Zhao Hukui, Ji Tao, Guo Zigang, Song Xiaoxian, Luo Fangji, Huang Pu, Ju Pingguo, Liu Jianyong, Zou Jian. Liquid raw material composition for cement grinding aid production Determination method gas chromatography

1 Scope

This standard specifies the gas chromatographic method for quantitative determination of liquid raw material components for the production of cement grinding aids, including principles, test conditions, and tests. Agents and materials, instruments and equipment, test procedures, test data processing, precision. This standard applies to the production of cement grinding aid triethanolamine, triisopropanolamine (including isomers), diethylene glycol, diethanol monoisopropyl Alcoholamine (containing isomers), single or mixed liquid raw materials free of inorganic substances and having a mass fraction of less than 85%.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article. Pieces. For undated references, the latest edition (including all amendments) applies to this document. GB/T 3723 General rules for sampling safety of industrial chemical products General rules for sampling GB/T 6678 chemical products GB/T 6680 Liquid Chemical Product Sampling General GB/T 8170 Numerical Rounding Rules and Representation and Determination of Limit Values GB/T 9722 chemical reagent gas chromatography general rule GB/T 27564 industrial triisopropanolamine

3 Principle

Gas chromatography was used to separate the components of the sample under selected operating conditions and detected by a hydrogen flame ionization tester. in accordance with The standard curve was drawn and quantitatively tested using the external standard method.

4 test conditions

The laboratory temperature should be controlled within the range of 20 ° C ~ 25 ° C.

5 reagents and materials

5.1 Anhydrous ethanol. analytically pure. 5.2 High purity hydrogen. The volume fraction is not less than 99.999%. 5.3 High purity nitrogen. The volume fraction is not less than 99.999%. 5.4 Conventional compressed air. 5.5 External standard reagent. triethanolamine, triisopropanolamine, diethylene glycol, diethanol monoisopropanolamine reagent, should choose the chromatogram with analytical certificate Pure or analytically pure, wherein the mass fraction of triethanolamine, triisopropanolamine and diethylene glycol is not less than 99%, and the mass fraction of diethanol monoisopropanolamine Not less than 93%. Typical external standard reagents are triethanolamine (chromatographically pure) with a mass fraction of 99.595% and triisopropanolamine with a mass fraction of 99.7%. (Analytically pure, may contain isomers), diethylene glycol (chromatographic purity) with a mass fraction of 99.349%, diethanol monoisopropyl at a mass fraction of 93.9%

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