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GB/T 34405-2017: Determination for migration of acrylamide in household papers -- Liquid chromatography-tandem mass spectrometry (LC-MS/MS) method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 34405-2017 | English | 199 |
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Determination for migration of acrylamide in household papers -- Liquid chromatography-tandem mass spectrometry (LC-MS/MS) method
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GB/T 34405-2017
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Basic data | Standard ID | GB/T 34405-2017 (GB/T34405-2017) | | Description (Translated English) | Determination for migration of acrylamide in household papers -- Liquid chromatography-tandem mass spectrometry (LC-MS/MS) method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y33 | | Classification of International Standard | 85.080 | | Word Count Estimation | 10,158 | | Date of Issue | 2017-09-29 | | Date of Implementation | 2018-01-01 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | GB/T 34405-2017: Determination for migration of acrylamide in household papers -- Liquid chromatography-tandem mass spectrometry (LC-MS/MS) method
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Determination for migration of acrylamide in household papers - Liquid chromatography-tandem mass spectrometry (LC-MS/MS) method
ICS 85.080
Y33
National Standards of People's Republic of China
Determination of acrylamide transfer in household paper products
Liquid chromatography - tandem mass spectrometry
Liquidchromatography-tandem mass spectrometry (LC-MS/MS) method
2017-09-29 Posted
2018-01-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
China National Standardization Administration released
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard by the National Quality Supervision Key Products Testing Methods Standardization Technical Committee (SAC/TC374) and focal point.
This standard was drafted unit. Guangzhou Quality Supervision, Inspection and Research Institute, the quality of Warner (Beijing) Technology Center Co., Ltd., the Federation of inspection (North
Beijing) Quality Inspection Technology Co., Ltd., Guangdong Yu-sheng Health Products Co., Ltd., Zhejiang Tiger Leap Packaging Materials Co., Ltd., standard-through
Technical Services (Shanghai) Co., Ltd., Spectrum Test Group Co., Ltd., Yiwu City Products (Goods) Quality Supervision, Inspection and Research Institute.
The main drafters of this standard. Xie Wen-chi, Liu Donghong, Xiong Xiaoting, Jia Fang, Wu Yuluan, Dai Hang, Hu Xiaolu, Chen Zhajian, Mai Qing Mei, Wang Zhenglin,
Zhu Huijun, Song Wei, Wei Shunwen.
Determination of acrylamide transfer in household paper products
Liquid chromatography - tandem mass spectrometry
1 Scope
This standard specifies the household paper products in the migration of acrylamide in artificial sweat liquid chromatography - triple quadrupole tandem mass spectrometer
(LC-MS/MS) method.
This standard applies to paper towels (paper towels, paper napkins, paper handkerchiefs, etc.), wet wipes (wipes, baby wipes), toilet paper, sanitary napkins, paper urine
Pants and other home paper products in the detection of acrylamide migration, which sanitary napkins and diapers products only apply to skin contact with the outer cover
Part of the test.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
Textiles - Tests for color fastness - Color fastness to perspiration GB/T 3922-2013
GB/T 6682 analytical laboratory water specifications and test methods
3 principle
The acrylamide content in the soaking solution was measured under simulated human contact conditions. Electrospray ionization in LC-MS/MS
(ESI) positive mode, multiple reaction monitoring (MRM) scans, with retention time and ion pair qualitative, deuterated acrylamide as internal
Calibration volume.
4 reagent
4.1 water
GB/T 6682 provisions of a water.
4.2 Methanol
Chromatographic purity.
4.3 Formic acid
Chromatographic purity.
4.4 standard substance
Acrylamide (CAS 79-06-1) in an amount of more than 98%.
4.5 Internal standard substance
Deuterated acrylamide (2,3,3-D3 acrylamide, CAS122775-19-3), content greater than 98%.
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