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PDF GB/T 26174-2023 English (GB/T 26174-2010: Older version)


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GB/T 26174-2023: PDF in English (GBT 26174-2023)

GB/T 26174-2023 GB NATIONAL STANDARD OF THE PEOPLE'S REPUBLIC OF CHINA ICS 85.060 CCS Y 32 Replacing GB/T 26174-2010 Kitchen towel 厨 房 纸 巾 ISSUED ON. AUGUST 6, 2023 IMPLEMENTED ON. SEPTEMBER 1, 2024 Issued by. State Administration for Market Regulation; Standardization Administration of PRC. Table of Contents Foreword... 3 1 Scope... 5 2 Normative references... 5 3 Terms and definitions... 6 4 Classification... 7 5 Raw material requirements... 7 6 Technical requirements... 7 7 Test methods... 10 8 Inspection rules... 13 9 Marking and packaging... 17 10 Transportation and storage... 18 Appendix A (Normative) Test method of water absorption time... 19 Appendix B (Normative) Determination of powder drop rate... 21 Appendix C (Normative) Determination of decolorization performance... 23 Appendix D (Normative) List of decomposable carcinogenic aromatic amines... 25 Appendix E (Normative) Determination of microorganisms... 26 Kitchen towel 1 Scope This document specifies the classification, raw material requirements, technical requirements, test methods, inspection rules, marking, packaging, transportation, and storage of kitchen towels. This document is applicable to paper towels used for kitchen wiping, cleaning, etc. 2 Normative references The following documents contain the provisions which, through normative reference in this document, constitute the essential provisions of this document. For the dated referenced documents, only the versions with the indicated dates are applicable to this document; for the undated referenced documents, only the latest version (including all the amendments) is applicable to this document. GB/T 450 Paper and board - Sampling for testing and identification of machine and cross direction, wire side and felt side GB/T 451.1 Paper and board - Determination of size and deviation GB/T 462 Paper, board and pulps - Determination of moisture content of analytical sample GB/T 742 Fibrous raw material, pulp, paper and board - Determination of residue(ash) on ignition at 575 ℃ and 900 ℃ GB/T 1535 Soya bean oil GB/T 1541 Paper and board - Determination of dirt GB/T 2828.1 Sampling procedures for inspection by attributes - Part 1.Sampling schemes indexed by acceptance quality limit (AQL) for lot-by-lot inspection GB/T 6682 Water for analytical laboratory use - Specification and test methods GB/T 7974 Paper, board and pulps - Measurement of diffuse blue reflectance factor - D65 brightness (Diff/Geometry, Outdoor daylight conditions) GB/T 10739 Paper, board and pulps - Standard atmosphere for conditioning and testing GB/T 17592 Textiles - Determination of the banned azo colourants GB/T 23344 Textiles - Determination of 4-aminoazobenzene GB/T 24328.3 Tissue paper and tissue products - Part 3.Determination of tensile strength, stretch at maximum force and tensile energy absorption GB/T 24328.4-2020 Tissue paper and tissue products - Part 4.Determination of wet tensile strength GB/T 24328.5 Tissue paper and tissue products - Part 5.Determination of grammage GB/T 24328.6 Tissue paper and tissue products - Part 6.Determination of water- absorption time and water-absorption capacity - Basket-immersion test method GB/T 24991 Paper, board and pulps - Determination of lead content - Graphite furnace atomic absorption spectrometry method GB/T 24992 Paper, board and pulps - Determination of arsenic GB/T 27741-2018 Paper and board - Determination of migratable fluorescent whitening agents GB 31604.49-2016 National food safety standard - Food contact materials and products - Determination of arsenic, cadmium, chromium and lead and determination of migration of arsenic, cadmium, chromium, nickel, lead, antimony and zinc GB/T 36420 Tissue paper and products - Safety assessment management system of chemicals and materials GB/T 37859 Paper, board and paper products - Determination of acrylamide JJF 1070-2005 Rules of metrological testing for net quantity of products in prepackages with fixed content QB/T 5742 Natural color pulp 3 Terms and definitions The following terms and definitions apply to this document. 3.1 kitchen towel from plant fiber Kitchen towels produced from native plant fibers. 6.6 The paper surface of kitchen towels shall be clean, and there shall be no obvious dead wrinkles, broken, damage, sand, hard lumps, raw pulp clumps, or other paper defects. 6.7 The net content (mass, length, quantity) of kitchen towels shall comply with the provisions of Table 3 in JJF 1070-2005. 7 Test methods 7.1 Sampling and processing of specimens The sampling shall be carried out in accordance with GB/T 450.When determining grammage, water absorption time, water absorption capacity, oil absorption capacity, transverse tensile strength, and longitudinal wet tensile strength, the specimen processing and standard atmospheric conditions for testing shall be in accordance with the provisions of GB/T 10739. 7.2 Grammage Grammage determination is carried out according to GB/T 24328.5, and the result is expressed as a single layer. 7.3 D65 brightness D65 brightness is measured according to GB/T 7974. 7.4 Water absorption time The water absorption time is measured according to Appendix A. 7.5 Water absorption capacity The water absorption capacity is measured according to GB/T 24328.6. 7.6 Oil absorption capacity The oil absorption capacity is measured according to GB/T 24328.6; the first-grade soybean oil that complies with GB/T 1535 is used instead of the standard water for testing, and the draining time is (120±2) s. 7.7 Transverse tensile strength The transverse tensile strength is measured according to GB/T 24328.3 and measured according to the finished product layer. The width of the specimen is (50.0±0.5) mm or (15.0±0.1) mm. The width of the specimen during arbitration is (50.0±0.5) mm. 7.8 Longitudinal wet tensile strength For kitchen towels from plant fiber, the samples need to be subjected to accelerated aging (maturation) treatment before testing. The processing temperature is (105±2) °C and the time is 15 minutes; kitchen towels from other fibers do not need to undergo accelerated aging (maturation) treatment. Then it is measured according to GB/T 24328.4-2020 with the finished product layer; a horizontal tensile strength tester is used, and the immersion time is 5 seconds. 7.9 Powder drop rate The powder drop rate is measured according to Appendix B. 7.10 Holes Hold the two corners of the specimen (finished product layer) with both hands and observe with the naked eye against the light. If holes are found, use a steel ruler to measure the maximum size of the holes. The area of the specimen (finished product layer) measured for each sample shall be no less than 0.5 m2 and then converted into the number of holes per square meter (finished product layer). If there are holes larger than 5 mm, at least 1 m2 of the specimen shall be measured. 7.11 Dirt count The dirt count is measured according to GB/T 1541 and measured according to the finished product layer. That is, regardless of whether the product is a single layer, double layer, or multi-layer, take at least 0.25 m2 finished product layer specimen, measure the dirt count on both sides of the finished product layer, and then convert it into dirt count per square meter (finished product layer). Fiber bundle impurities in natural color kitchen towels are not counted as dirt. 7.12 Ash The ash is measured according to GB/T 742, the ignition temperature is 575 ℃, and the ignition time is 4 h. 7.13 Delivery moisture The delivery moisture content is measured according to GB/T 462. 7.14 Migratable fluorescent substances Place the specimen under an ultraviolet lamp and check whether there is fluorescence under ultraviolet light at wavelengths 254 nm and 365 nm. If the specimen has no fluorescence under UV light, the result is that there is no migratable fluorescent substance; if the specimen has fluorescence, the migratable fluorescent substance shall be measured in accordance with Chapter 5 of GB/T 27741-2018. 7.15 Acrylamide Acrylamide is measured according to GB/T 37859. 7.16 Decolorization performance Decolorization performance is measured according to Appendix C. 7.17 Heavy metals (lead, arsenic) Lead and arsenic are measured according to the first part of GB 31604.49-2016.The lead content can also be determined according to GB/T 24991, and the arsenic content can be determined according to GB/T 24992.For arbitration, they shall be measured according to the first part of GB 31604.49-2016.When testing, try to take samples from darker areas of printing or dyeing. 7.18 Decomposable carcinogenic aromatic amine dyes Decomposable carcinogenic aromatic amine dyes are measured in accordance with GB/T 17592 and GB/T 23344, and the list of decomposable carcinogenic aromatic amines is in Appendix D. Generally, it is tested according to GB/T 17592 first. When aniline and/or 1,4-phenylenediamine are detected, it is tested according to GB/T 23344. When testing, try to take samples from darker areas of printing or dyeing. 7.19 Microbiological indicators Microbiological indicators are determined according to Appendix E. 7.20 Dimensional deviation 7.20.1 Width deviation of roll and jumbo roll kitchen towels Take 3 complete specimens from each sample, measure the width of each specimen (reel) with a steel ruler or steel tape measure with a graduation value of 1 mm, and subtract the nominal width from the average width of the 3 specimens to express the width deviation; the results are rounded to 1 mm. 7.20.2 Pitch deviation of roll and jumbo roll kitchen towels Take any 1 roll (jumbo roll) of kitchen towels. After removing the first 5 sections, take 10 sections in succession, and use a steel ruler with a graduation value of 1 mm to measure the length of each of the 10 sections. Calculate the average value and subtract the nominal pitch from the average value to express the pitch deviation of the specimen; the results are rounded to 1 mm. damaged and shall not be opened before testing. 8.4 Judgment rules 8.4.1 Judgment of items 8.4.1.1 Technical indicators If the technical indicators of the sample meet the requirements of 6.1 or 6.2 respectively, the items will be judged to be qualified, otherwise, they will be judged to be unqualified. 8.4.1.2 Chemical performance indicators If the chemical performance indicators of the sample meet the requirements of 6.3 respectively, the items will be judged to be qualified, otherwise, they will be judged to be unqualified. 8.4.1.3 Microbiological indicators If the microbiological indicators of the sample meet the requirements of 6.4, the items will be judged as qualified, otherwise, they will be judged as unqualified. 8.4.1.4 Dimensional deviation and deviation If the dimensional deviation and deviation of the sample meet the requirements of 6.5, the items will be judged to be qualified, otherwise, they will be judged to be unqualified. 8.4.1.5 Appearance quality If the appearance quality of the sample meets the requirements of 6.6, the item will be judged to be qualified, otherwise, it will be judged to be unqualified. 8.4.1.6 Net content If the net content of the sample meets the requirements of 6.7, the item will be judged to be qualified, otherwise, it will be judged to be unqualified. 8.4.2 Judgment of batches Among all inspection items, if the microbiological indicator test results are unqualified, the batch will be judged to be unqualified; for technical indicators, chemical performance indicators, dimensional deviation, deviation, appearance quality, and net content, the number of samples for the first inspection shall be equal to the first sample size given in the plan. If the number of non-conforming products found in the first sample size is less than or equal to the first acceptance number in Table 6, the batch is judged to be qualified; if the number of non-conforming products found in the first sample size is greater than or equal to the first rejection number in Table 6, the batch is Appendix E (Normative) Determination of microorganisms E.1 Product collection and sample processing E.1.1 Take at least 6 minimum sales package samples from 3 transport packages of the same batch number (if the number of samples cannot meet the experimental requirements, the number of samples shall be increased accordingly), of which 1/3 samples are used for testing, 2/3 samples are used as retained samples. The minimum sales package sampled shall not be damaged and shall not be opened before inspection. E.1.2 Use aseptic methods to open at least 2 packages for testing under purification conditions of level-5 air cleanliness, take samples from each package, and accurately weigh 10 g±1 g of the sample. Cut the sample into pieces, add 200 mL of sterilized saline or modified broth culture solution (MLTBL, containing neutralizer), and mix thoroughly to obtain a saline or neutralizer sample solution. E.1.3 If the tested sample has an antibacterial effect, a suitable neutralizing agent shall be selected for neutralization, and the maximum dilution gradient shall not exceed 1.100.If there is no corresponding neutralizer, the membrane filtration method is used to remove the effect of antibacterial components in the sample on the growth of microorganisms, and then the sample solution is prepared according to E.1.2. E.2 Detection method of the total number of bacterial colonies E.2.1 Operation steps After the saline or neutralizer sample solution obtained according to E.1 has naturally settled, take the supernatant and perform a 10-fold serial dilution if necessary. Select the appropriate dilution for colony counting. Inoculate a total of 2 plates, add 2.0 mL of sample solution to each plate, and then pour 15 mL~20 mL of molten nutrient agar medium cooled to 40 °C~45 °C into each plate and mix evenly. After the agar solidifies, turn the plates over and place them at 36 °C±1 °C to culture for 48 hours, and count the number of colonies on the plates. E.2.2 Colony counting Plates with colonies growing in sheets should not be used. Make sure that the two plates meet the counting requirements and count the colonies. Calculate the results according to formula (E.1). morphology on the plate. Typical coliform colonies are black-purple or red-purple, round, with neat edges, smooth and moist surfaces, and often have a metallic luster. Some are purple-black with no or slightly metallic luster, or pink with a darker center. E.3.1.3 Staining microscopy and identification. Take 1~2 suspected bacterial colonies for Gram staining microscopic examination, inoculate lactose fermentation tubes at the same time, culture them at 36 °C±1 °C for 18 h~24 h, and observe the acid and gas production. E.3.2 Result reporting If the lactose and bile salt fermentation tube produces acid and gas, the lactose fermentation tube produces acid and gas, and there are typical coliform colonies on the eosin methylene blue plate, and the Gram stain is negative and contains no bacilli, the sample can be reported as coliform detected. E.4 Pseudomonas aeruginosa detection method E.4.1 Operation steps E.4.1.1 Enrichment culture. Take 5 mL of sample solution, add it to 50 mL of SCDLP culture solution, mix thoroughly, and place at 36 °C±1 °C for 18 h~24 h. If Pseudomonas aeruginosa grows, a thin bacterial film will appear on the surface of the culture solution, and the culture solution will often appear yellow-green or blue-green. E.4.1.2 The isolation culture steps are as follows. a) Pick the culture from the thin bacterial film of the culture solution, streak- inoculate the cetyltrimethylammonium bromide agar plate, culture it at 36 ℃±1 ℃ for 18 h~24 h, and observe the colony characteristics. Pseudomonas aeruginosa grows well on this culture medium. The colonies are flat with uneven edges, and the culture medium around the colonies is slightly pink. b) In the absence of cetyltrimethylammonium bromide agar, acetamide culture medium can also be used for isolation. streak-inoculate the bacterial suspension on a plate and culture it at 36 ℃±1 ℃ for 18 h~24 h to observe the colony characteristics. Pseudomonas aeruginosa grows well on this culture medium. The colonies are flat with uneven edges, and the culture medium around the colonies is slightly pink. E.4.1.3 Staining microscopy. Take a smear of suspicious colonies from the identification medium for Gram staining. If the microscopic examination shows Gram- negative bacteria, the test must be carried out according to E.4.1.4~E.4.1.8. E.4.1.4 Oxidase test. Take a small piece of clean white filter paper and place it on a sterilized plate. Use a sterile glass rod to pick out the suspicious colonies on the identification medium, apply it on the filter paper piece, and then add a drop of newly prepared 1% dimethyl-p-phenylenediamine test solution on it. If it appears pink or purple within 30 seconds, the oxidase test result is positive; if it does not change color, it is negative. Commercial oxidase test strips or reagents can also be used for detection. E.4.1.5 Pyocyanin test. Take 2~3 suspicious colonies on the identification medium, respectively inoculate them on the slant of the medium for pyocyanin determination, culture at 36 ℃±1 ℃ for 24 h, add 3 mL~5 mL of chloroform, and shake thoroughly to dissolve the possible pyocyanin in the culture. When the chloroform turns blue, use a pipette to move it to another test tube, add 1 mL of 1 mol/L hydrochloric acid, shake it, and let it stand for a while. If the upper layer appears pink or purple, it is positive, indicating the presence of pyocyanin. E.4.1.6 Nitrate reduction gas production test. Take the suspicious bacterial colonies on the identification medium and inoculate them into the nitrate peptone water medium, place them at 36 ℃±1 ℃, and incubate for 24 hours. If there is gas in the small inverted tube of the culture medium, it is considered Positive. E.4.1.7 Gelatin liquefaction test. Take the pure culture of the suspected bacterial colony on the identification medium, stab-inoculate it into the gelatin medium, place it at 36 ℃±1 ℃ for 24 hours, then take it out and place it at 4 ℃~10 ℃; if the culture medium is still in liquid state, the test result is positive; if the culture medium is coagulated, the test result is negative. E.4.1.8 42 °C growth test. Take the suspicious culture on the identification medium, inoculate it on a common agar slant medium, and culture it at 42 °C for 24 h~48 h. If there is growth of Pseudomonas aeruginosa, the test result is positive. E.4.2 Result reporting If the tested sample is confirmed to be Gram-negative bacilli after enrichment culture and isolation culture, and the oxidase and pyocyanin test results are both positive, it can be reported that Pseudomonas aeruginosa is detected in the tested sample. If the pyocyanin test result is negative but the liquefied gelatin, nitrate reduction gas production, and 42 °C growth test results are all positive, it can still be reported that Pseudomonas aeruginosa is detected in the tested sample. E.5 Staphylococcus aureus detection method E.5.1 Operation steps E.5.1.1 Enrichment culture. Take 5 mL of sample solution, add it to 50 mL SCDLP culture solution, mix thoroughly, and culture at 36 °C±1 °C for 18 h~24 h. E.5.1.2 Isolation culture. Take 1~2 inoculation loops from the self-enriched bacterial E.6.1.3 Staining microscopy. Select typical colonies for smear Gram staining microscopic examination. When the microscopic examination result is Gram-positive cocci arranged in a chain, the streptokinase test and bacitracin sensitivity test are also required. E.6.1.4 Streptokinase test. Take 0.2 mL of potassium oxalate plasma (add 0.01 g of potassium oxalate to 5 mL of rabbit plasma, mix well, precipitate by centrifugation, and draw the supernatant), add 0.8 mL of sterile physiological saline, and mix well; add 0.5 mL of the 24-hour broth culture of the bacteria to be tested and 0.25 mL of 0.25% calcium chloride, mix well, and place it in a 36 °C±1 °C water bath; observe once every 2 minutes (generally it can coagulate within 10 minutes), and continue to observe and record dissolution time after the plasma has coagulated. If it does not dissolve within 2 hours, continue to leave it for 24 hours for observation. If the clot is completely dissolved, the test result is positive; if it still does not dissolve after 24 hours, the test result is negative. E.6.1.5 Bacitracin sensitivity test. Apply the suspension of the tested bacteria on the blood agar plate, use sterilized tweezers to take a piece of paper containing 0.04 units of bacitracin, and place it on the surface of the plate; at the same time, use a known Positive strain as control, and place at 36 °C±1 °C for 24 h~48 h. Those with inhibitory zones are considered positive. E.6.2 Result reporting If the microscopic examination result is Gram-positive chain-like cocci, hemolytic circles appear on the blood agar plate, and streptokinase and bacitracin test results are both positive, it can be reported that hemolytic streptococci are detected in the tested sample. E.7 Detection method of total number of fungal colonies E.7.1 Operation steps After the physiological saline or neutralizer sample solution obtained according to E.1 has naturally settled, take the supernatant, and perform a 10-fold serial dilution if necessary. Select the appropriate dilution for fungal colony counting. A total of 2 plates are inoculated; add 2.0 mL of sample solution to each plate, then pour 15 mL~20 mL of melted Sandcastle weak agar medium or modified Sandcastle weak agar medium cooled to 40 °C~45 °C into each plate, and mix evenly. After the agar solidifies, turn the plates over and culture at 25 °C±1 °C (Sandcastle weak agar medium) or 28 °C±1 °C (modified Sandcastle weak agar medium) for 3 days; observe on the 1st, 2nd, and 3rd days respectively, and count the number of colonies on the plates. If colonies are found to spread, the previous colony count shall prevail. E.7.2 Colony counting ......
 
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