US$299.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 30166-2024: Textiles - Determination of acrylamide compounds Status: Valid GB/T 30166: Evolution and historical versions
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GB/T 30166-2024 | English | 299 |
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Textiles - Determination of acrylamide compounds
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GB/T 30166-2024
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GB/T 30166-2013 | English | 319 |
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Textiles -- Determination of acrylamide
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PDF similar to GB/T 30166-2024
Basic data Standard ID | GB/T 30166-2024 (GB/T30166-2024) | Description (Translated English) | Textiles - Determination of acrylamide compounds | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | W04 | Classification of International Standard | 59.080.01 | Word Count Estimation | 14,197 | Date of Issue | 2024-03-15 | Date of Implementation | 2024-10-01 | Older Standard (superseded by this standard) | GB/T 30166-2013 | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration |
GB/T 30166-2024: Textiles - Determination of acrylamide compounds---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 59.080.01
CCS W04
National Standards of People's Republic of China
Replaces GB/T 30166-2013
Determination of acrylamide compounds in textiles
Released on 2024-03-15
2024-10-01 Implementation
State Administration for Market Regulation
The National Standardization Administration issued
Foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents"
Drafting.
This document replaces GB/T 30166-2013 "Determination of acrylamide in textiles". Compared with GB/T 30166-2013, except for the structure
In addition to adjustments and editorial modifications, the main technical changes are as follows.
--- Changed the scope of the standard (see Chapter 1, Chapter 1 of the.2013 edition);
--- Deleted formic acid and formic acid solution (see 4.4 and 4.5 of the.2013 edition);
--- Added "N-hydroxymethyl acrylamide standard" and "methacrylamide standard" (see 5.4 and 5.5);
--- Changed the standard stock solution and standard working solution (see 5.6 and 5.7, 4.6 and 4.7 of the.2013 edition);
--- Added analytical balance with a graduation value of 0.01g (see 6.3);
--- Changed the limit of quantification (see 9.1, 8.1 of the.2013 edition);
--- Deleted the recovery rate (see 8.2 of the.2013 edition).
This document was proposed by the China National Textile and Apparel Council.
This document is under the jurisdiction of the National Technical Committee on Standardization of Textiles (SAC/TC209).
This document was drafted by. Zhejiang Sci-Tech University, Tianjin University of Technology Textile Additives Co., Ltd., China Textile Standards Inspection and Certification Co., Ltd., Zhejiang
Provincial Institute of Inspection and Quarantine Science and Technology, Shaoxing Shangyu District Xiaoyifeng Clothing Co., Ltd., Zhejiang Shengfa Textile Printing and Dyeing Co., Ltd., Shaoxing Fang
Yuan Testing Technology Co., Ltd., China Textile Standard (Fujian) Testing Co., Ltd., Chongqing Metrology and Quality Inspection Institute, Zibo Lurui Fine Chemical Co., Ltd.
Co., Ltd., Beijing Yaoyang High-Tech Service Co., Ltd., and Hangzhou Nomo Testing Technology Co., Ltd.
The main drafters of this document are. Chen Haixiang, Xu Jinyun, Cai Baixue, Liu Feifei, Gao Yang, Mao Wenliang, Cheng Zijian, Wu Ling, Wu Gang, Zhao Shanhong,
Liu Baisong, Yang Wenlong, Zhu Zilong, Wang Aide, Lin Xianzhen, Liu Deming, and Lü Wangyang.
The previous versions of this document and the documents it replaces are as follows.
---First published in.2013 as GB/T 30166-2013;
---This is the first revision.
Determination of acrylamide compounds in textiles
Warning. Operators using this document should have practical experience in regular laboratory work. This document does not indicate all possible safety hazards.
The user is responsible for taking appropriate safety and health measures and ensuring that the conditions stipulated by relevant national laws and regulations are met.
1 Scope
This document describes a method for the determination of acrylamide compounds in textiles using high performance liquid chromatography.
This document is applicable to the testing of various types of textile products.
2 Normative references
The contents of the following documents constitute the essential clauses of this document through normative references in this document.
For referenced documents without a date, only the version corresponding to that date applies to this document; for referenced documents without a date, the latest version (including all amendments) applies to
This document.
GB/T 6682 Specifications and test methods for water used in analytical laboratories
3 Terms and definitions
There are no terms or definitions that require definition in this document.
4 Principle
The sample was extracted by water shaking, and the extract was filtered and purified, and then the acrylamide compounds in Appendix A were determined by high performance liquid chromatography.
Quantitative analysis was performed by external standard method.
5 Reagents
Unless otherwise specified, all reagents used were of analytical grade.
Grade 3 water as specified in GB/T 6682.
5.1 Methanol. Chromatographic grade.
5.2 Acetonitrile. chromatographic grade.
5.3 Acrylamide standard. purity not less than 99%.
5.4 N-Hydroxymethyl acrylamide standard product. purity not less than 98%.
5.5 Methacrylamide standard. purity not less than 98%.
5.6 Standard stock solution (1000 μg/mL). Accurately weigh appropriate amounts of acrylamide standard (5.3), N-hydroxymethyl acrylamide standard
The standard sample (5.4) and methacrylamide standard (5.5) were dissolved in water to make up to volume, and the standard stock solutions with a mass concentration of 1000 μg/mL were prepared respectively.
Note. The standard stock solution should be stored at 4℃~8℃ away from light and has a validity period of 2 months.
5.7 Standard working solution (10 μg/mL). Accurately transfer 1.0 mL of the standard stock solution (5.6) into a 100 mL volumetric flask and add water.
Dilute to the scale to prepare a mixed standard working solution with a mass concentration of 10 μg/mL.
Note. The standard working solution should be stored at 4℃~8℃ away from light and has a shelf life of 7 days.
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