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GB/T 29635-2013 English PDF

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GB/T 29635-2013: GC and GC-MS examination methods for heroin in suspected drug
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PDF similar to GB/T 29635-2013


Standard similar to GB/T 29635-2013

GB/T 28181   GA/T 1788.2   GA/T 424   GB/T 19267.13   GB/T 29637   GB/T 29636   

Basic data

Standard ID GB/T 29635-2013 (GB/T29635-2013)
Description (Translated English) GC and GC-MS examination methods for heroin in suspected drug
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard A92
Classification of International Standard 13.310
Word Count Estimation 11,120
Quoted Standard GA/T 122; JJF 1059.1-2012
Regulation (derived from) National Standards Bulletin 2013 No. 10
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the heroin by gas chromatography - mass spectrometry (GC-MS) and qualitative analysis by gas chromatography (GC) quantitative analysis. This standard applies to solid samples of heroin drug cases qualitative and quantitative inspec

GB/T 29635-2013: GC and GC-MS examination methods for heroin in suspected drug

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GC and GC-MS examination methods for heroin in suspected drug ICS 13.310 A92 National Standards of People's Republic of China Suspected drug heroin gas chromatography, Gas chromatography - mass spectrometry test methods Issued on. 2013-07-19 2013-11-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents. This standard by the National Standardization Technical Committee for Standardization of Poison Analyses for Criminal Technology Technical Committee (SAC/TC179/SC1) mention And the focal point. This standard was drafted. Ministry of Public Security Evidence Identification Center. The main drafters of this standard. Gregory students, Chang Chun, Zheng Hui, Qian Zhenhua, Xu Peng, Huang Xing, Wang, Wang Wei Xin, Chang Ying, Liu Kelin. Suspected drug heroin gas chromatography, Gas chromatography - mass spectrometry test methods

1 Scope

This standard specifies the heroin gas chromatography - mass spectrometry (GC-MS) and qualitative analysis by gas chromatography (GC) quantitative analysis. This standard applies to solid samples of heroin drug cases qualitative and quantitative inspection and appraisal.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. GA/T 122 toxicological analysis Terminology JJF1059.1-2012 Evaluation and Expression of Uncertainty in Measurement

3 Terms and Definitions

Terms and definitions GA/T 122 defined apply to this document. Principle 4 This method uses the internal standard method or external standard method for quality control of drugs in solid samples of suspected heroin organic solvent extraction using Gas chromatography - mass spectrometry (GC-MS) qualitative analysis by gas chromatography - flame ionization detector (GC-FID) of heroin were Quantitative analysis. 5 Reagents and reference materials, instruments and appliances volume 5.1 Reagents and Standards The reagents used were of analytical grade reagents and reference materials include. a) chloroform. b) methanol. c) extraction reagent preparation. chloroform and methanol mixed at a ratio of 9.1 to prepare an extraction reagent. d) traceable standard substance. heroin. e) quantified by external standard 1.0mg/mL standard stock solution heroin. heroin weighed standard substance (according to the standard material purity and salt type After the conversion is equal to 50.0mg heroin), into 50mL volumetric flask, dissolved by shaking after 20mL extraction solvent is added, with The extraction solvent is diluted to the mark, the preparation of 1.0mg/mL standard stock solution of heroin, home refrigerator freezer to save, save for six Months. f) external standard quantitation using 0.1mg/mL heroin working standard solution. Pipette 1.0mg/mL standard solution 5mL added heroin To 50mL volumetric flask, dilute to the mark with the extraction solvent to prepare a 0.1mg/mL heroin working standard solution, set the refrigerator

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