US$209.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 2385-2007: General method for the determination of crystallizing point dye intermediates Status: Valid GB/T 2385: Evolution and historical versions
Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
GB/T 2385-2007 | English | 209 |
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General method for the determination of crystallizing point dye intermediates
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GB/T 2385-2007
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GB/T 2385-1992 | English | 199 |
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Dye intermediates general method for the determination of crystallizing point
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GB/T 2385-1992
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PDF similar to GB/T 2385-2007
Basic data Standard ID | GB/T 2385-2007 (GB/T2385-2007) | Description (Translated English) | General method for the determination of crystallizing point dye intermediates | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G55 | Classification of International Standard | 71.100.01; 87.060.10 | Word Count Estimation | 8,870 | Date of Issue | 2007-11-28 | Date of Implementation | 2008-06-01 | Older Standard (superseded by this standard) | GB/T 2385-1992 | Quoted Standard | GB/T 629 | Adopted Standard | ISO 1392-1977, MOD | Regulation (derived from) | China National Standard Approval Announcement2007 No.12 (Total No.112) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the determination of the crystalline dye intermediate point with a double casing method common methods. This standard applies to the determination of dye intermediates crystallization point of crystallization temperature in the range of -10��C ~ 150��C. This standard applies to the direct determination of the sample crystallization point also applies to the determination of the dried sample after crystallization point. If the sample to be dried and drying methods otherwise specified in the product standard. |
GB/T 2385-2007: General method for the determination of crystallizing point dye intermediates---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
General method for the determination of crystallizing point dye intermediates
ICS 71.100.01; 87.060.10
G55
National Standards of People's Republic of China
Replacing GB/T 2385-1992
General method for the determination of crystallizing point of dye intermediates
(ISO 1392. 1977, Determinationofcrystalizingpoint-Generalmethod, MOD)
Posted 2007-11-28
2008-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This revised standard adopts ISO 1392. 1977 "Determination of crystallizing point --- General Methods."
This standard and ISO 1392. 1977 differences are as follows.
--- Standard format editorial changes;
--- This standard applies to the determination within the range of -10 ℃ ~ 150 ℃ dye intermediates crystallization point, the scope of ISO 1392 is
Determination of -50 ℃ ~ 250 ℃ crystallization point substance (in this standard in Chapter 1; ISO 1392. Chapter 1, 1977);
--- This standard specifies the use Dewar, beakers used as the cooling bath and a hot tub, ISO 1392. 1977 using Dewar and thermal bath (this standard
6.1.7 and 6.1.8,6.1.9; ISO 1392. 1977 of 4.5,4.6,4.7);
--- Coolant provisions of this standard is ice, ice saline, glycerol, water and air or other media, ISO 1392 dry ice - acetone,
Ice or water (this standard 5.2; ISO 1392. 1977, 4.5);
--- This standard simplifies the ISO 1392. specific provisions for sample drying process 1977 (ISO 1392. 1977 and 5.2.1
5.2.2.1 and 5.2.2.2; this standard 7.1);
Stop --- This standard specifies the sample was cooled with stirring, crystallization occurs when stirred; ISO 1392. 1977 stipulates that from the start of cooling the sample
The proceeds stirring without allowing liquid to extreme cold, after crystallization occurs if the temperature rises more than 1 ℃ ~ 2 ℃, should be re-measured
(This standard is 7.3; ISO 1392. 1977 5.4).
This standard replaces GB/T 2385-1992 "dye intermediates determination of crystallizing point - General method."
This standard compared with GB/T 2385-1992 The main changes are as follows.
--- Change the standard name is "common measurement method dye intermediate crystallization point";
--- Increased (Chapter 2 of this edition) "Normative references" chapter;
--- Increased (3rd edition chapter) chapter "Terms and Definitions";
--- Modify the formula of full immersion thermometer measurement, increasing the formulas Bureau immersion thermometer measurement (1992 edition 7
Chapter; Chapter 8 of this edition);
--- Increase in the content of the test report (Chapter 10 of this edition).
The standard proposed by China Petroleum and Chemical Industry Association.
This standard by the National Standardization Technical Committee Dye (SAC/TC134) centralized.
This standard was drafted. Shenyang Chemical Research Institute.
The main drafters of this standard. Kiran Qin, Shen Jiong day.
GB 2385 - 1980, 1992 second revision of GB/T 2385-1992.
General method for the determination of crystallizing point of dye intermediates
1 Scope
This standard specifies the determination of crystallizing point of dye intermediates double cuff technique common methods.
This standard applies to the determination of dye intermediates crystallization point of crystallization temperature in the range of -10 ℃ ~ 150 ℃.
This standard applies to direct measurement sample crystallization point, is also applicable to the measurement sample dried after crystallization point. Are samples need to do
Dry and dry methods in product standards separately.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 629 chemical reagent sodium hydroxide
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
The point means a liquid crystalline material during the cooling transition from liquid to solid phase transition temperature when.
Principle 4
Liquid or melted material cooled at atmospheric pressure, when the temperature control from the liquid phase to a solid phase during the phase transition, the release of latent heat is observed
The maximum temperature to maintain a certain stage of the crystallization point temperature.
5 Reagents and materials
5.1 Desiccant
5.1.1 anhydrous calcium chloride. AR.
5.1.2 Sodium hydroxide. shall comply with the provisions of GB T 629 /.
5.1.3 Molecular Sieve. size and type in the product standard specified. When used, subject to calcination at 550 ℃ 3h activated in a dry
It is in the back.
5.2 Coolant
5.2.1 crushed ice and salt mixture. for the range of -10 ℃ ~ 0 ℃ cooling medium.
5.2.2 The mixture of crushed ice and water. for the range of 0 ℃ ~ 25 ℃ cooling medium.
5.2.3 Glycerin. for in the range of 25 ℃ ~ 150 ℃ cooling or heating medium.
5.2.4 air or water and other media to meet the requirements.
6 instruments and devices
6.1 Instrument
6.1.1 crystallization tube. outer diameter of about 25mm, length of 150mm ± 5mm.
6.1.2 Casing. diameter of about 28mm, length of 120mm ± 5mm, wall thickness 2mm.
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