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GB/T 2382-2015 English PDF

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GB/T 2382-2015: Sulphur dyes -- Determination of content of free sulphur
Status: Valid

GB/T 2382: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
GB/T 2382-2015English129 Add to Cart 3 days [Need to translate] Sulphur dyes -- Determination of content of free sulphur Valid GB/T 2382-2015
GB/T 2382-2007English199 Add to Cart 2 days [Need to translate] Sulphur dyes -- Determination of content of free sulphur Obsolete GB/T 2382-2007
GB/T 2382-1995English199 Add to Cart 2 days [Need to translate] Determination of content of free sulphur in sulphur dyes Obsolete GB/T 2382-1995
GB 2382-1980English199 Add to Cart 2 days [Need to translate] Determination of free sulfur content in sulfur dyes and sulfurized reduced dyes Obsolete GB 2382-1980

PDF similar to GB/T 2382-2015


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Basic data

Standard ID GB/T 2382-2015 (GB/T2382-2015)
Description (Translated English) Sulphur dyes -- Determination of content of free sulphur
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard G55
Classification of International Standard 71.100.01; 87.060.10
Word Count Estimation 6,688
Date of Issue 2015-05-15
Date of Implementation 2015-12-01
Older Standard (superseded by this standard) GB/T 2382-2007
Quoted Standard GB/T 601; GB/T 603; GB/T 6682-2008; GB/T 8170-2008
Regulation (derived from) National Standard Announcement 2015 No. 15
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This Standard specifies the method for the determination of free sulfur content of sulfur. This Standard applies to the determination of free sulfur content of sulfur.

GB/T 2382-2015: Sulphur dyes -- Determination of content of free sulphur

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Sulphur dyes. Determination of content of free sulphur ICS 71.100.01; 87.060.10 G55 National Standards of People's Republic of China Replacing GB/T 2382-2007 Determination of free sulfur content of sulfur Issued on. 2015-05-15 2015-12-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard replaces GB/T 2382-2007 "Determination of free sulfur, sulfur content," compared with the GB/T 2382-2007, in addition to Editorial changes outside the main technical changes are as follows. --- Increased safety tips (see Chapter 4); --- Modify the sample weight of the sample (see 441, 2007 edition 6.1.); --- Modified extractive distillation operation reflux time (see 442, 2007 edition 6.2.); --- Modify the course of the reaction amount of sodium sulfite (see 443, 2007 edition 6.3.); --- Modify the dosage titration formaldehyde solution (see 444, 2007 edition 6.4.); --- Increasing the allowable difference (see 4.4.4). The standard proposed by China Petroleum and Chemical Industry Association. This standard by the National Standardization Technical Committee Dye (SAC/TC134) centralized. This standard was drafted. Zhejiang Changzheng Chemical Co., dye State Quality Supervision and Inspection Center, Shenyang Chemical Research Institute Co., Ltd. Drafters of this standard. Long Yan, Gao new, Jin Yonghui, Kiran Qin, Wang Yong. This standard replaces the previous editions of the standard. --- GB 2382-1980, GB/T 2382-1995, GB/T 2382-2007. Determination of free sulfur content of sulfur

1 Scope

This standard specifies the method for the determination of free sulfur content of sulfur. This standard applies to the determination of free sulfur content of sulfur.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Preparation of GB/T 601 chemical reagent standard titration solution GB/T 603 chemical reagent in test methods - Preparations with Laboratory use specifications and test methods GB/T 6682-2008 Analysis GB/T 8170-2008 revised value represents about rules and limit values \u200b\u200band judgment

3 Principle of Measurement

Extraction with an organic solvent free from sulfur in the sulfur dye, and then the organic solvent was distilled off, the residue was then reacted with sodium sulfite, with Iodine titration standard solution titration. Standard iodine titration solution free sulfur content is calculated according to consumption. S Na2SO3 → Na2S2O3 2Na2S2O3 I2 → 2NaI Na2S4O6

4 Determination

Warning --- volatile organic solvent used in this standard is harmful to human health and the Flammable vapor can form explosive mixtures with air, It should be performed in a fume hood, and prevent contact with open flame. 4.1 General provisions Unless otherwise specified, use only recognized as analytical reagents and GB/T 6682-2008 specified in the third grade water. Test used in the standard Quasi titration solution and indicator, did not indicate when the other requirements, according to GB/T 601 and GB/T 603 requirements Preparation and calibration. test The results of the determination of GB/T 8170-2008 4.3.3 Rounding the value comparison method. 4.2 Reagents and solutions 4.2.1 filter. rapid qualitative filter paper. 4.2.2 toluene. 4.2.3 Anhydrous sodium sulfite. 4.2.4 acetic acid solution. 36% (mass fraction). 4.2.5 Formaldehyde solution. 37% to 40% (by mass). 4.2.6 standard iodine titration solution. c 12I2 ÷ = 0.1mol/L.

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