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GB/T 23296.4-2009: Food contact materials -- Polymer -- Determination of 1-octene and tetrahydrofuran in food simulants -- Gas chromatography
Status: Obsolete
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 23296.4-2009 | English | 479 |
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Food contact materials -- Polymer -- Determination of 1-octene and tetrahydrofuran in food simulants -- Gas chromatography
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GB/T 23296.4-2009
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Basic data | Standard ID | GB/T 23296.4-2009 (GB/T23296.4-2009) | | Description (Translated English) | Food contact materials -- Polymer -- Determination of 1-octene and tetrahydrofuran in food simulants -- Gas chromatography | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | C53 | | Classification of International Standard | 67.250 | | Word Count Estimation | 12,190 | | Date of Issue | 2009-03-31 | | Date of Implementation | 2009-09-01 | | Quoted Standard | GB/T 6682; GB/T 23296.1-2009 | | Regulation (derived from) | National Standard Approval Announcement 2009 No.3 (Total No.143) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the food simulants 1-Determination of octene and tetrahydrofuran. This standard applies to water, 3% (mass concentration) acetic acid, 10% (volume fraction) ethanol solution, such as water-based food simulants and olive oil 1-Determination of the content of octene and tetrahydrofuran. Water-based food simulants 1-Determination of low-octene and tetrahydrofuran limits were 2. 0mg/L and 7. 0mg/L., olive oil 1-octene and tetrahydrofuran limit of determination was 2. 0mg/kg and 7. 0mg/kg. | GB/T 23296.4-2009: Food contact materials -- Polymer -- Determination of 1-octene and tetrahydrofuran in food simulants -- Gas chromatography
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Food contact materials. Polymer. Determination of 1-octene and tetrahydrofuran in food simulants. Gas chromatography
ICS 67.250
C53
National Standards of People's Republic of China
Food contact materials - Polymer
Determination of food simulants 1-octene and tetrahydrofuran
Gas chromatography
Posted 2009-03-31
2009-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The reference standard adopted by the European Technical Specification CEN/T S13130-26.2005 "food contact plastic materials and products was limited
Part 26 Quality. Food simulants 1-octene and tetrahydrofuran determination "(in English) to develop.
Appendix A of this standard is an informative annex.
This standard was proposed by the National Certification and Accreditation Administration Committee.
This standard by the National Import and Export Food Safety Inspection Standardization Technical Committee (SAC/TC445) centralized.
This standard was drafted. People's Republic of China Hubei Exit Inspection and Quarantine, Chinese Academy of Inspection and Quarantine, the People's Republic of China
States and the Guangdong Entry-Exit Inspection and Quarantine of Guangxi People's Republic of China.
The main drafters of this standard. Cui Hairong, about Ling Tao, ZHOU Ming-hui, Chen Zhifeng, Li Dan, Ye Cheng VETERINARY Lv Chunqiu, wind Yang, Guo Jian,
Chen Jianhua, Hude Cong.
Food contact materials - Polymer
Determination of food simulants 1-octene and tetrahydrofuran
Gas chromatography
1 Scope
This standard specifies the method for determination of food simulants 1-octene and tetrahydrofuran.
This standard applies to water, 3% (mass concentration) solution of acetic acid, 10% (volume fraction) ethanol and other water-based food simulants and olive oil
Determination of 1-octene and tetrahydrofuran content.
Determination of 1-octene and tetrahydrofuran in food simulants water-based low limits were 2.0mg/L and 7.0mg/L, 1-octene olive oil
And tetrahydrofuran lower limit of detection was 2.0mg/kg and 7.0mg/kg.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
GB/T 23296.1-2009 plastic food contact materials restricted substances in food and food simulants to specific substances in plastics
Migration testing and determination of methods and conditions of exposure to food simulants Guide selection
Principle 3
Food simulants 1-octene, tetrahydrofuran after headspace, in the column and the internal standard and other components separated from the hydrogen flame
Ionization detector, within the standard method.
4 Reagents and materials
Unless otherwise indicated, water GB/T 6682 provided a water, reagents were of analytical grade.
4.1 glacial acetic acid.
4.2 ethanol.
4.3 olive oil.
4.4 1-octene standards. purity of greater than 97.5%.
4.5 isooctane standards. purity of greater than 99.0%.
4.6 Tetrahydrofuran (THF) Standards. than 99.5% purity.
4.7 tetrahydropyranyl (in THP) Standards. than 99.5% purity.
4.8 N, N- dimethylacetamide (DMAC). more than 99.0% purity.
4.9 3% (mass concentration) acetic acid solution. Weigh 30g (accurate to 0.1g) in glacial acetic acid (4.1) in 1L flask, water volume.
4.10 to 10% (by volume) ethanol. Measure 100mL anhydrous ethanol (4.2) in 1L flask, water volume.
4.11 1-octene stock standard solution (2mg/mL). amount of 45mLDMAC (4.8) in 50mL volumetric flask, stoppered weighing (accurate to
0.001g). Added 100mg1- octene (4.4), about 150μL, again weighed (accurate to 0.001g). DMAC with constant volume. accurate
Calculate the concentration of 1-octene. At 4 ℃ dark preservation, valid for three months.
4.12 1-octene intermediate standard solution (200μg/mL). accurate Pipette 1.0mL1- octene standard stock solution (4.11) in 10mL volumetric flask
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