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GB/T 23296.22-2009 English PDF

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GB/T 23296.22-2009: Food contact materials -- Determination of isocyanates in plastics -- High performance liquid chromatography
Status: Obsolete
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GB/T 23296.22-2009English319 Add to Cart 3 days [Need to translate] Food contact materials -- Determination of isocyanates in plastics -- High performance liquid chromatography Obsolete GB/T 23296.22-2009

PDF similar to GB/T 23296.22-2009


Standard similar to GB/T 23296.22-2009

GB 22255   GB 22570   GB/T 22246   GB/T 23296.5   GB/T 23296.6   GB/T 23296.24   

Basic data

Standard ID GB/T 23296.22-2009 (GB/T23296.22-2009)
Description (Translated English) Food contact materials -- Determination of isocyanates in plastics -- High performance liquid chromatography
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard C53
Classification of International Standard 67.250
Word Count Estimation 8,825
Date of Issue 2009-03-31
Date of Implementation 2009-09-01
Quoted Standard GB/T 6682
Regulation (derived from) National Standard Approval Announcement 2009 No.3 (Total No.143)
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the method for determination of plastic food contact materials isocyanate content. This standard applies to food contact materials was measured by the production of polyurethane isocyanate content. This standard polyurethane plastics toluene-2 ??, 6-diisocyanate, diphenylmethane-4, 4 '- diisocyanate, toluene 2, 4-diisocyanate, naphthalene-1, 5-diisocyanate, phenyl isocyanate, and Determination of cyclohexyl isocyanate lower limit are 0. 1mg/kg.

GB/T 23296.22-2009: Food contact materials -- Determination of isocyanates in plastics -- High performance liquid chromatography


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Food contact materials. Determination of isocyanates in plastics. High performance liquid chromatography ICS 67.250 C53 National Standards of People's Republic of China Food contact materials Plastics - Determination of isocyanate content High Performance Liquid Chromatography Posted 2009-03-31 2009-09-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

The standard reference European Standard EN13130-8.2005 "food contact plastic materials and products for restricted substances - Part 8. Plastic Determination of isocyanate content of feed "(in English) to develop. Appendix A of this standard is an informative annex. This standard was proposed by the National Certification and Accreditation Administration Committee. This standard by the National Import and Export Food Safety Inspection Standardization Technical Committee (SAC/TC445) centralized. This standard was drafted. China Inspection and Quarantine Science Research Institute, People's Republic of China Shandong Exit Inspection and Quarantine, Ningxia Autonomous Region Food Testing Center, People's Republic of China Hubei Exit Inspection and Quarantine. The main drafters of this standard. Sun Lee, saffron yellow, Chen Zhifeng, Guo Xiaoming, Lingyun, Cui Hairong, Wang Xin, Yang Qian. Food contact materials Plastics - Determination of isocyanate content High Performance Liquid Chromatography

1 Scope

This standard specifies the method for determination of plastic food contact materials in the isocyanate content. This standard applies to the determination using food contact materials made of polyurethane isocyanate content. This standard specifies the polyurethane plastics toluene-2,6-diisocyanate, diphenylmethane-4,4'-diisocyanate, toluene-2,4-diisocyanate Ester, naphthalene 1,5-diisocyanate, phenyl isocyanate and determination cyclohexyl isocyanate low limits were 0.1mg/kg.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD) Principle 3 After the sample was extracted with dichloromethane, and methyl amino methyl 9- anthracene derivatized reaction, derivative products using high performance liquid chromatographic column separation, fluorescence Detector was measured, quantified by external standard.

4 Reagents and materials

Unless otherwise specified, all reagents were of analytical grade water as a water GB/T 6682 regulations. 4.1 2,6-toluene diisocyanate [C9H6N2O2; CH3C6H3 (NCO) 2, CAS number. 91-08-7]. purity of greater than 98%. 4.2-diphenyl-4,4'-diisocyanate (C15H10N2O2, CAS number. 101-68-8). purity of greater than 98%. 4.3 2,4-toluene diisocyanate (C9H6N2O2, CAS number. 86-91-9). purity of greater than 98%. 4.4 naphthalene-1,5-diisocyanate (C12H6N2O2, CAS number. 3173-72-6). purity of greater than 98%. 4.5 phenyl isocyanate (C7H5ON, CAS number. 103-71-9). purity of greater than 98%. 4.6 cyclohexyl isocyanate (C8H12O2N2, CAS number. 822-06-0). purity of greater than 98%. 4.7 A 9- aminomethyl anthracene. purity of greater than 99%. 4.8 dichloromethane. 5A molecular sieve and dried overnight reserve. 4.9 ether. 4.10 phosphate. 4.11 acetonitrile. chromatography. 4.12 N, N- dimethylformamide. 99%, respectively. 4.13 triethylamine (3% volume fraction). 4.14 buffer solution. in 1L flask, was added 950mL3% solution of triethylamine (4.13), adjusted to pH 3.0 with phosphoric acid, washed with water Volume.

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