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US$239.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 23296.13-2009: Food contact materials -- Determination of vinyl chloride monomer in plastics -- Gas chromatography Status: Obsolete
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 23296.13-2009 | English | 239 |
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Food contact materials -- Determination of vinyl chloride monomer in plastics -- Gas chromatography
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GB/T 23296.13-2009
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PDF similar to GB/T 23296.13-2009
Basic data | Standard ID | GB/T 23296.13-2009 (GB/T23296.13-2009) | | Description (Translated English) | Food contact materials -- Determination of vinyl chloride monomer in plastics -- Gas chromatography | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | C53 | | Classification of International Standard | 67.250 | | Word Count Estimation | 6,699 | | Date of Issue | 2009-03-31 | | Date of Implementation | 2009-09-01 | | Regulation (derived from) | National Standard Approval Announcement 2009 No.3 (Total No.143) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the method for the determination of food contact materials PVC vinyl chloride monomer. This standard applies to the determination of food contact polyvinyl chloride or vinyl chloride copolymers of vinyl chloride monomer. Determination of vinyl chloride in the standard lower limit of 0. 50 mg/kg. |
GB/T 23296.13-2009: Food contact materials -- Determination of vinyl chloride monomer in plastics -- Gas chromatography ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food contact materials.Determination of vinyl chloride monomer in plastics.Gas chromatography
ICS 67.250
C53
National Standards of People's Republic of China
Food contact materials
Gas chromatography plastic vinyl chloride monomer
Posted 2009-03-31
2009-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The standard reference ENISO 6401.2004 "vinyl chloride homopolymer and copolymer of vinyl chloride monomer by gas chromatography" (English
Version) develop.
The Standard Appendix A and Appendix B is an informative annex.
This standard was proposed by the National Certification and Accreditation Administration Committee.
This standard by the National Import and Export Food Safety Inspection Standardization Technical Committee (SAC/TC445) centralized.
This standard drafting unit. China Inspection and Quarantine Science Research Institute, People's Republic of China Hubei Entry-Exit Inspection and Quarantine, the State Environmental Protection
Product Quality Supervision and Inspection Center, Department of Chemistry.
Drafters of this standard. Chen Zhifeng Sun Lee, Yong Wei, Cui Hairong, Chu Xiaogang, Li Hui, Zhang Yan, Li Haifang.
Food contact materials
Gas chromatography plastic vinyl chloride monomer
1 Scope
This standard specifies the determination of food contact materials PVC vinyl chloride monomer.
This standard applies to the determination of food contact polyvinyl chloride or vinyl chloride copolymers of vinyl chloride monomer.
The standard vinyl chloride - Determination of low limit of 0.50mg/kg.
Principle 2
Test samples were dissolved in N, N- dimethylacetamide, a sample of vinyl chloride by automated headspace sampler injection using capillary gas
Phase column separation, hydrogen flame ionization detector measurement, external standard. Can be manual headspace sampling mode, the injection operation see sidebar
Record A.
3 Reagents and materials
Unless otherwise specified, all reagents were of analytical grade.
3.1 N, N- dimethylacetamide. 99%, respectively.
3.2 vinyl chloride standard solution. 5000mg/L, acetone or methanol as the solvent.
3.3 vinyl chloride stock solution (10mg/L). Join 10mLN in 10mL brown glass bottles, N- dimethylacetamide, using micro-injection
Absorb 20μL vinyl chloride standard solution (3.2) into a glass vial, immediately sealing cap, balance 2h after, kept in 4 ℃ refrigerator.
3.4 vinyl chloride standard solution. in seven vial were added 10mLN, N- dimethylacetamide, using micro-syringe, respectively
Draw 0μL, 50μL, 75μL, 100μL, 125μL, 150μL, 200μL chloride stock solution (3.3) slow injection top vial, Li
That capped, mixed, to give N, N- dimethylacetamide vinyl chloride concentrations were 0mg/L, 0.050mg/L,
0.075mg/L, 0.100mg/L, 0.125mg/L, 0.150mg/L, 0.200mg/L.
4 instruments and equipment
4.1 GC. Configure the automatic headspace sampler and flame ionization detector.
4.2 bottles. 10mL, bottle cap with silicone rubber or butyl rubber gasket.
4.3 bottles. 20mL, bottle cap with silicone rubber or butyl rubber gasket.
4.4 micro syringe. 25μL, 100μL, 200μL.
4.5 Analysis of balance. a sense of the amount of 0.0001g, 0.01g.
Step 5 Analysis
5.1 Sample Preparation
The sample was cut into small particles, accurately weighed amount of sample (eg 10g) in 150mL grinding mouth Erlenmeyer flask (accurate to 0.1mg), in accordance with
Per gram of sample was added 10mLN, N- dimethylacetamide proportion to the Erlenmeyer flask, an appropriate amount (e.g. 100mL) N, N- dimethylacetamide
Amines, immediately capped and shaken to dissolve (if difficult to dissolve, may be appropriate to heat up), to be completely dissolved into -18 ℃ refrigerator to cool save
spare.
5.2 Sample Preparation
From the refrigerator removed containing the sample solution Erlenmeyer flask, which weighed separately 10mL sample solution in two vial, immediately gland
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