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GB/T 22964-2008: Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 22964-2008 | English | 279 |
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Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method
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GB/T 22964-2008
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Basic data | Standard ID | GB/T 22964-2008 (GB/T22964-2008) | | Description (Translated English) | Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | X04 | | Classification of International Standard | 67.050 | | Word Count Estimation | 12,120 | | Date of Issue | 2008-12-31 | | Date of Implementation | 2009-05-01 | | Quoted Standard | GB/T 6379.1; GB/T 6379.2; GB/T 6682 | | Regulation (derived from) | National Standard Approval Announcement 2008 No.26 (Total No.139) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the puffer fish and eels lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kitasamycin and josamycin residues in liquid chromatography-tandem mass spectrometry. This standard applies to puffer fish and eels lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, determination Kitasamycin and josamycin residues. This standard method detection limit: puffer fish in lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kitasamycin and josamycin are 2. 0��g/kg. Eel in lincomycin, erythromycin, tylosin, kitasamycin are 2. 0��g/kg, spiramycin, oleandomycin, Josamycin, tilmicosin were 5. 0��g/kg. | GB/T 22964-2008: Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel. LC-MS-MS method
ICS 67.050
X04
National Standards of People's Republic of China
Puffer fish, eels lincomycin, oleandomycin,
Erythromycin, tilmicosin, tylosin, spiramycin,
Determination of neomycin guitar, josamycin residues
Liquid chromatography - tandem mass spectrometry
Posted 2009-05-01 2008-12-31 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The Standard Appendix A, Appendix B is an informative annex.
This standard is proposed and managed by the State Administration of Quality Supervision, Inspection and Quarantine.
This standard was drafted. People's Republic of China Qinhuangdao Exit Inspection and Quarantine.
The main drafters of this standard. Wang Fei, Wang Haiyang, Caoyan Zhong Jia light group, Zhang Jinjie, Shiyu Qiu, Pang Guofang.
Puffer fish, eels lincomycin, oleandomycin,
Erythromycin, tilmicosin, tylosin, spiramycin,
Determination of neomycin guitar, josamycin residues
Liquid chromatography - tandem mass spectrometry
1 Scope
This standard specifies the puffer fish and eel lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, guitar mildew
Su and josamycin residues liquid chromatography - tandem mass spectrometry.
This standard applies to puffer fish and eel lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, guitar mildew
Su and josamycin residues determination.
The standard method detection limit. puffer fish lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kyrgyzstan
He neomycin and josamycin were 2.0μg/kg. Eel lincomycin, erythromycin, tylosin, neomycin guitar were 2.0μg/kg,
Spiramycin, oleandomycin, josamycin, tilmicosin were 5.0μg/kg.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions
(GB/T 6379.1-2004, ISO 5725-1.1994, IDT)
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
Principle 3
Puffer fish and eels in lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, josamycin guitar and neomycin
The residue was extracted with Tris buffer solution by OasisHLB SPE column 1) purification, methanol eluate was concentrated to volume liquid
Tandem mass spectrometry, internal standard - chromatography.
1) OasisHLB SPE waters is the company's product trade name, this information is given for the convenience of users of this standard, does not mean
Endorsement of the product. If other equivalent product has the same effect, you can use these equivalent products.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade.
4.1 Water. GB/T 6682, level.
4.2 Methanol. chromatographically pure.
4.3 ammonium acetate.
4.4 acetonitrile. chromatography.
4.5 hydrochloric acid.
4.6 Tris (tris). C4H11NO3.
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