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GB/T 21783-2008: Plastic capillary tube and polarizing microscope method of partially crystalline polymer melting behavior (melting temperature or melting range)
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| GB/T 21783-2008 | English | 359 |
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Plastic capillary tube and polarizing microscope method of partially crystalline polymer melting behavior (melting temperature or melting range)
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GB/T 21783-2008
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Basic data | Standard ID | GB/T 21783-2008 (GB/T21783-2008) | | Description (Translated English) | Plastic capillary tube and polarizing microscope method of partially crystalline polymer melting behavior (melting temperature or melting range) | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | A80 | | Classification of International Standard | 13.300 | | Word Count Estimation | 9,988 | | Date of Issue | 2008-05-12 | | Date of Implementation | 2008-09-01 | | Quoted Standard | GB/T 2918 | | Adopted Standard | ISO 3146-2000, IDT | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 7, 2008 (No. 120 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the evaluation of partially crystalline polymer melting behavior in two ways. Measured by different methods of melting temperature is usually a few degrees away, explanation has been made in the introduction to this. Method A: This method is based on capillary base polymer is shaped into a determination of the melting temperature, applicable to all semicrystalline polymers and their mixtures. Method B: This method is based on polarization microscopy changes in optical properties of the polymer based on determination of the melting temperature, suitable for containing birefringent crystalline melting temperature of the polymer phase is determined, is not applicable to a birefringence of the pigment will interfere and/or additives of the polymer crystalline melting temperature measurement. | GB/T 21783-2008: Plastic capillary tube and polarizing microscope method of partially crystalline polymer melting behavior (melting temperature or melting range)
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Plastic capillary tube and polarizing microscope method of partially crystalline polymer melting behavior (melting temperature or melting range)
ICS 13.300
A80
National Standards of People's Republic of China
GB/T 21783-2008/ISO 3146.2000
Plastic capillary tube and polarizing microscope assay
Melting behavior of the partially crystalline polymer
(Melting temperature or melting range)
(ISO 3146.2000, IDT)
Posted 2008-05-12
2008-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard is identical with ISO 3146.2000 (E) "Determination of partially crystalline polymer plastic capillary tube and polarizing microscopy melt
Behavior (melting temperature or melting range), "including Technical Corrigendum ISO 3146.2000/Cor. 1.2002 (E).
This standard is managed by the National Standardization Technical Committee chemicals dangerous (SAC/TC251) and focal points.
This standard was drafted. Guangdong Entry-Exit Inspection and Quarantine, Ningbo, the State Quality Supervision, Inspection synthetic resin
center.
The main drafters of this standard. Chengu Feng, Peng-speed standard, Xiaoda Hui, Chen Qiang, Chen Wenjie, Di Cuiping, Zheng Jianguo, Wu bud, Lin Zhenxing,
Wang Jiandong, Li Qingxiang.
This standard is the first release.
GB/T 21783-2008/ISO 3146.2000
Introduction
Melting behavior of crystalline or partially crystalline polymers exhibit a structure-sensitive properties.
Polymers that typically do not have a definite melting point low molecular weight substances, can be observed only when heated from a solid to a change of the start
High viscosity or viscoelastic liquid crystal phase and is accompanied by the disappearance of the melting temperature range. Melting range, such as molecular weight and molecular weight distribution, crystallinity, and
Many parameters of thermodynamic properties and so on.
Melting range may also be related to the thermal history of the sample. Melting range lower limit or upper limit or the average, sometimes referred to as the habit
"Melting temperature."
GB/T 21783-2008/ISO 3146.2000
Plastic capillary tube and polarizing microscope assay
Melting behavior of the partially crystalline polymer
(Melting temperature or melting range)
1 Scope
This standard specifies the evaluation of a partially crystalline polymer melting behavior of two ways.
Different methods of measuring the melting temperature is usually a few degrees difference, in the introduction to this explanation has been made.
Method A. capillary method
The method is based on determination of the melting temperature of the polymer into a shape-based, apply to all parts of the crystalline polymer and mix.
Note 1. A method can also be used to evaluate the softening behavior of non-crystalline solid.
Method B. polarizing microscopy
The method is based on changes in the optical properties of the polymer melt temperature measurement method based for birefringent crystalline phase of the polymer containing
The determination of the melting temperature, there is not applicable to interfere with the melting temperature of the birefringent pigments and/or additives in polymer crystalline regions measured.
Note 2. Another method is suitable for partially crystalline polymers can be found in the standard. GB/T 19466.3-2004 "plastic differential scanning calorimeter (DSC) method
Part 3. melting or crystallization temperature and enthalpy measurement "(ISO 11357-3.1999, IDT).
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 2918 standard plastic sample conditioning and environmental tests (idtGB/T 2918-1998, ISO 291.1997)
3 Terms and Definitions
This standard uses the following terms and definitions.
3.1
Crystalline phase and amorphous phase-containing polymer.
3.2
Crystalline or partially crystalline polymer crystallization when heated or particle shape characteristics disappearance temperature range.
Note. The definition of methods A and B measured "melting temperature" see 4.1 and 5.1 respectively.
4 Method A. capillary method
4.1 Principle
In the case of controlling the heating rate of the sample in the capillary heating. Record the temperature and specimen sample starts to deform when the last vestiges
Temperature crystal phase disappears.
A first temperature called the melting temperature of the sample is said to range between two temperatures for the melting range of the sample.
NOTE. According to the relevant regulations or agreed upon by the parties, this standard is also applicable to non-crystalline polymer.
GB/T 21783-2008/ISO 3146.2000
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