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GB/T 19267.7-2023 English PDF

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GB/T 19267.7-2023: Forensic sciences - Physical and chemical examination of trace evidence - Part 7: Gas chromatography-mass spectrometry
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GB/T 19267.7: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
GB/T 19267.7-2023English369 Add to Cart 4 days [Need to translate] Forensic sciences - Physical and chemical examination of trace evidence - Part 7: Gas chromatography-mass spectrometry Valid GB/T 19267.7-2023
GB/T 19267.7-2008English359 Add to Cart 3 days [Need to translate] Physical and chemical examination of trace evidence in forensic sciences -- Part 7: Gas chromatography/mass spectrometry Obsolete GB/T 19267.7-2008
GB/T 19267.7-2003English359 Add to Cart 3 days [Need to translate] Physical and chemical examination of trace evidence in forensic sciences -- Part 7: Gas chromatography/mass spectrometry Obsolete GB/T 19267.7-2003

PDF similar to GB/T 19267.7-2023


Standard similar to GB/T 19267.7-2023

GB 16796   GA/T 1788.2   GA/T 424   GB/T 19267.13   GB/T 19267.1   GB/T 19267.11   

Basic data

Standard ID GB/T 19267.7-2023 (GB/T19267.7-2023)
Description (Translated English) Forensic sciences - Physical and chemical examination of trace evidence - Part 7: Gas chromatography-mass spectrometry
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard A92
Classification of International Standard 07.140
Word Count Estimation 18,152
Date of Issue 2023-12-28
Date of Implementation 2024-07-01
Older Standard (superseded by this standard) GB/T 19267.7-2008
Issuing agency(ies) State Administration for Market Regulation, China National Standardization Administration

GB/T 19267.7-2023: Forensic sciences - Physical and chemical examination of trace evidence - Part 7: Gas chromatography-mass spectrometry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 07:140 CCSA92 National Standards of People's Republic of China Replace GB/T 19267:7-2008 Physical and chemical examination of trace evidence in forensic science Part 7: Gas Chromatography-Mass Spectrometry evidence-Part 7:Gaschromatography-massspectrometry Published on 2023-12-28 2024-07-01 Implementation State Administration for Market Regulation Released by the National Standardization Administration Committee

Foreword

This document complies with the provisions of GB/T 1:1-2020 "Standardization Work Guidelines Part 1: Structure and Drafting Rules of Standardization Documents" Drafting: This document is Part 7 of GB/T 19267: GB/T 19267 has released the following parts: ---Part 1: Infrared absorption spectrometry; ---Part 2: UV-visible absorption spectrometry; ---Part 3: Molecular fluorescence spectrometry; ---Part 4: Atomic emission spectrometry; ---Part 5: Atomic absorption spectrometry; ---Part 6: Scanning electron microscopy/X-ray spectroscopy; ---Part 7: Gas Chromatography-Mass Spectrometry; ---Part 8: Microspectrophotometry; ---Part 9: Thin layer chromatography; ---Part 10: Gas Chromatography; ---Part 11: High performance liquid chromatography; ---Part 12: Thermal analysis method: This document replaces GB/T 19267:7-2008 "Physical and chemical examination of criminal technical trace evidence - Part 7: Gas chromatography-mass spectrometry", Compared with GB/T 19267:7-2008, in addition to structural adjustments and editorial changes, the main technical changes are as follows: ---Changed the applicable field, changing "criminal technology" to "forensic science" (see Chapter 1, Chapter 1 of the:2008 edition); ---Added GB/T 13966 "Terminology for Analytical Instruments" and GA/T 242 "Terminology for Physical and Chemical Testing of Trace Evidence in Forensic Science" Normative references (see Chapter 3); ---Added the term "secondary mass spectrometry" (see 3:4); ---Changed the terms of "gas chromatography-mass spectrometry", "gas chromatography-mass spectrometry", "total ion chromatogram" and "ion relative abundance" Terms and/or definitions (see 3:1~3:3, 3:5, 3:3, 3:4, 3:11, 3:25 of the:2008 edition); ---Deleted some terms (see 3:1, 3:2, 3:5~3:10, 3:12~3:24 of the:2008 edition); ---Changed the "principle" (see Chapter 4, Chapter 4 of the:2008 edition); ---Added "instrument configuration" (see Chapter 5) and deleted "instrument composition" (see 5:1 of the:2008 edition); ---Added "Performance indicators of gas chromatography part" (see 6:1); ---Changed the "Performance Indicators of the Mass Spectrometry Part" (see 6:2, 5:2 of the:2008 version); ---Added relevant content on "sampling" technology (see 7:1:2); ---Changed the relevant contents of "carrier gas", "sampling mode", "column flow", "injection volume" and "gas chromatography column" (see 7:1:1, 7:1:3~ 7:1:5, 7:2, 7:3, 7:4:1:1, 7:4:1:3, 7:4:1:4, 7:2 of the:2008 version); ---Deleted "other injection ports" and "sampling pre-treatment" (see 7:4:1:2 and 7:4:1:5 of the:2008 edition); ---Changed the relevant contents of "Instrument Tuning and Calibration", "Full Scan Mode" and "Selected Ion Detection Mode" (see 8:1, 8:2:1, 8:2:2, 5:3, 7:4:2:1, 7:4:2:2 of the:2008 version); ---Added "multiple reaction monitoring (MRM) mode" and "ion trap multi-stage mass spectrometry (MSn) mode" (see 8:2:3, 8:2:4); ---Changed the relevant contents of "Environmental Conditions" and "Sample Processing" (see 9:1, 9:3, 7:1, 6:3 of the:2008 version); ---Deleted "requirements for inspection materials" and "handling of inspection materials" (see 6:1 and 6:2 of the:2008 edition); ---Added "comparison confirmation of target compounds" and "comparison test" (see 10:1:1, 10:1:3); ---Changed the relevant content of "Quantitative Analysis" (see 10:2, 7:4:3 of the:2008 version); ---Deleted "qualitative accuracy and quantitative error" (see Chapter 8 of the:2008 edition); ---Changed the relevant content of "result expression" (see Chapter 11, Chapter 9 of the:2008 edition): Please note that some content in this document may be subject to patents: The publisher of this document assumes no responsibility for identifying patents: This document is under the jurisdiction of the National Criminal Technology Standardization Technical Committee (SAC/TC179): This document was drafted by: Public Security Department of Inner Mongolia Autonomous Region, China Criminal Police College, and Identification Center of the Ministry of Public Security: The main drafters of this document: Zhang Qiang, Zhu Yu, Liu Zhanfang, Guo Wei, Hu Can, Shao Mingyun, and Wang Yanan: The previous versions of this document and the documents it replaces are as follows: ---First published as GB/T 19267:7-2003 in:2003, first revised in:2008; ---This is the second revision:

Introduction

GB/T 19267 is a professional basic standard for forensic scientific trace evidence examination, aiming to improve the quality of identification and unify identification results: Discussion, increase the credibility of identification opinions, and provide norms and guidance for forensic scientific trace evidence examination: GB/T 19267 is planned to consist of 12 parts: ---Part 1: Infrared absorption spectrometry: ---Part 2: UV-visible absorption spectrometry: ---Part 3: Molecular fluorescence spectrometry: ---Part 4: Atomic emission spectrometry: ---Part 5: Atomic absorption spectrometry: ---Part 6: Scanning electron microscopy/X-ray spectroscopy: ---Part 7: Gas Chromatography-Mass Spectrometry: ---Part 8: Microspectrophotometry: ---Part 9: Thin layer chromatography: ---Part 10: Gas Chromatography: ---Part 11: High performance liquid chromatography: ---Part 12: Thermal analysis method: This document is Part 7 of GB/T 19267: It describes the overall principles and basic principles of gas chromatography-mass spectrometry in the examination of trace evidence: The requirements are generally applicable to the physical and chemical examination of trace evidence, and will play an important role in the examination of trace evidence in various cases such as explosions, arson, and gun-related cases: It is used for the standardization and normalization construction of forensic scientific trace evidence examination, improve the quality of identification, unify identification conclusions, and increase the validity of identification opinions: Credibility is important: It has been more than 13 years since the last version of GB/T 19267:7 was released: With the gas chromatography of trace evidence in forensic science- With the development of mass spectrometry testing technology, the content of this standard is no longer applicable to new analytical technologies and methods, and there is also a lack of specific pre-treatment methods for test materials: It is not practical in terms of practicality, identification and expression of results, and needs to be revised and improved urgently: Therefore, this document will be officially launched again in 2021: Revision: Physical and chemical examination of trace evidence in forensic science Part 7: Gas Chromatography-Mass Spectrometry

1 Scope

This document describes gas chromatography-mass spectrometry testing methods for forensic science trace evidence examination: This document is applicable to the physical and chemical examination of trace evidence in the field of forensic science:

2 Normative reference documents

The contents of the following documents constitute essential provisions of this document through normative references in the text: Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document: GB/T 13966 Analytical Instrument Terminology GB/T 14666 Analytical Chemistry Terminology GA/T 242 Terminology for physical and chemical examination of trace evidence in forensic science

3 Terms and definitions

The terms and definitions defined in GB/T 13966, GB/T 14666, GA/T 242 and the following apply to this document: 3:1 gas chromatography-mass spectrometry gaschromatography-massspectrometry; GC-MS An analytical method that combines separation by gas chromatography with qualitative analysis by mass spectrometry: [Source: GB/T 13966-2013,6:3] 3:2 Gas chromatograph-massspectrometer; GC-MS A gas chromatograph is an analytical instrument that implements gas chromatography-mass spectrometry by combining an interface with a mass spectrometer: [Source: GB/T 13966-2013,6:79] 3:3 Within the specified mass range, the ion current signal generated by all ions of each component changes with the elution time or scan number of the component: curve: [Source: GB/T 13966-2013,6:168, with modifications] 3:4 The precursor ions selected by the primary mass spectrometer are further fragmented in the collision cell to form secondary fragment ions, and then the generated secondary fragment ions are processed The mass spectrum obtained by mass analysis: 3:5 The intensity of the base peak in the mass spectrum is taken as 100%, and the remaining ion peaks are expressed as relative percentages of the base peak, and the relative values obtained by normalization are

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