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GB/T 18294.5-2010 English PDF

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GB/T 18294.5-2010: Technical identification methods for fire -- Part 5: Gas chromatography-mass spectrometry analysis
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Basic data

Standard ID GB/T 18294.5-2010 (GB/T18294.5-2010)
Description (Translated English) Technical identification methods for fire -- Part 5: Gas chromatography-mass spectrometry analysis
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard C82
Classification of International Standard 13.220.01
Word Count Estimation 7,782
Date of Issue 2011-01-14
Date of Implementation 2011-06-01
Quoted Standard GB/T 19267.7; GB/T 20162
Regulation (derived from) Announcement of Newly Approved National Standards No. 2 of 2011
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

GB/T 18294.5-2010: Technical identification methods for fire -- Part 5: Gas chromatography-mass spectrometry analysis


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Technical identdication methods for fire.Part 5. Gas chromatography-mass spectrometry analysis ICS 13.220.01 C82 National Standards of People's Republic of China Fire technology identification method Part 5. Gas chromatography - mass spectrometry Part 5. Gaschromatography-massspectrometryanalysis 2011-01-14 release 2011-06-01 Implementation General Administration of Quality Supervision, Inspection and Quarantine of the People 's Republic of China China National Standardization Management Committee released

Foreword

GB/T 18294 "fire technology identification method" is divided into six parts. - Part 1. Ultraviolet spectroscopy; - Part 2. Thin layer chromatography; - Part 3. Gas Chromatography; - Part 4. High performance liquid chromatography; - Part 5. Gas chromatography - mass spectrometry; Part 6. Infrared spectroscopy. This part is part 5 of GB/T 18294. This part is drafted in accordance with the rules given in GB/T 1.1-2009. This part is made by the Ministry of Public Security of the People's Republic of China. This section is headed by the National Fire Safety Standardization Technical Committee Fire Investigation Subcommittee (SAC/TC113/SC11). This part of the drafting unit. Ministry of Public Security Tianjin Fire Research Institute. The main drafters of this section. Tian Guihua, Lu Zhibao, Deng Zhenyu, Liang Guofu, Geng Huimin. Fire technology identification method Part 5. Gas chromatography - mass spectrometry

1 Scope

This part of GB/T 18294 specifies the terms and definitions of gas chromatography-mass spectrometry (GC-MS) in fire technology identification. Test equipment, test conditions and test methods. This part applies to gasoline, kerosene, diesel, paint thinner and other fire scene common flammable liquid and its combustion residue identification.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article Pieces. For undated references, the latest edition (including all modifications) applies to this document. GB/T 19267.7 Physical and chemical testing of microchemical evidence for criminal technology - Part 7. Gas chromatography - mass spectrometry GB/T .20162 Fire technology identification material extraction method

3 terms and definitions

GB/T 19267.7 and GB/T .20162 and the following terms and definitions apply to this document. 3.1 Total ion chromatogram total ionchromatogram In the chromatographic conditions under which the flammable liquid is passed through a capillary column, the total ion current of each component obtained by mass spectrometry The intensity varies with the scan time. 3.2 Extraction of ion - flow chromatograms extractedionchromatogram A map of the characteristic ion peaks of the flammable liquid selected from the total ion chromatogram.

4 test principle

After the laboratory pretreatment to be analyzed samples, injected into the gas chromatography-mass spectrometry instrument, after a pair of analytical samples with good Good separation of the capillary column into the mass spectrum, the total ion chromatogram, using the total ion chromatogram and extraction of ion current chromatography The characteristic of the flammable liquid is determined qualitatively by distinguishing the characteristic peaks.

5 test equipment

5.1 Gas Chromatography - Mass Spectrometer A combination of a capillary chromatograph that separates flammable liquids and a mass spectrometer that identifies flammable liquids. 5.2 syringes 5.2.1 Liquid syringe. Volume injector in the range of 0.1 μL to 10.0 μL.

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