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GB/T 18114.10-2010 English PDF

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GB/T 18114.10-2010: Chemical analysis methods of rare earth concentrates -- Part 10: Determination of water content -- Gravimetry
Status: Valid

GB/T 18114.10: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
GB/T 18114.10-2010English139 Add to Cart 3 days [Need to translate] Chemical analysis methods of rare earth concentrates -- Part 10: Determination of water content -- Gravimetry Valid GB/T 18114.10-2010
GB/T 18114.10-2000English199 Add to Cart 2 days [Need to translate] Methods for chemical analysis of monazite concentrates. Determination of water content Obsolete GB/T 18114.10-2000

PDF similar to GB/T 18114.10-2010


Standard similar to GB/T 18114.10-2010

GB/T 18882.1   GB/T 18115.2   GB/T 18882.2   GB/T 18114.3   GB/T 18114.8   GB/T 18114.11   

Basic data

Standard ID GB/T 18114.10-2010 (GB/T18114.10-2010)
Description (Translated English) Chemical analysis methods of rare earth concentrates -- Part 10: Determination of water content -- Gravimetry
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard H14
Classification of International Standard 77.120.99
Word Count Estimation 6,685
Date of Issue 1/14/2011
Date of Implementation 11/1/2011
Older Standard (superseded by this standard) GB/T 18114.10-2000
Regulation (derived from) Announcement of Newly Approved National Standards No. 2 of 2011
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This Standard specifies determination of rare earth concentrates moisture. This Standard is applicable to the determination of rare earth concentrates moisture measurement range: 0. 02% to 20. 00%.

GB/T 18114.10-2010: Chemical analysis methods of rare earth concentrates -- Part 10: Determination of water content -- Gravimetry


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Chemical analysis methods of rare earth concentrates Part 10. Determination of water content Gravimetry. ICS 77.120.99 H14 National Standards of People's Republic of China Replacing GB/T 18114.10-2000 Methods for chemical analysis of rare earth concentrates Part 10. Determination of moisture content - Gravimetric method Part 10. Determinationofwatercontent-Gravimetry Issued on. 2011-01-14 2011-11-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

GB/T 18114 "Methods for chemical analysis of rare earth concentrates" is divided into 11 parts. --- Part 1. Determination of total rare earth oxide gravimetric method; --- Part 2. Determination of thorium oxide content; --- Part 3. Determination of calcium oxide content; --- Part 4. niobium oxide, zirconium oxide, titanium oxide content - Inductively coupled plasma atomic emission spectrometry; --- Part 5. aluminum oxide content - Inductively coupled plasma atomic emission spectrometry; --- Part 6. Determination of the amount of silica; --- Part 7. Determination of the amount of iron oxide dichromate method; --- Part 8. fifteen rare earth element oxide with components measured by inductively coupled plasma atomic emission spectrometry; --- Part 9. Determination of the amount of phosphorus pentoxide bismuth molybdenum blue spectrophotometric method; --- Part 10. Determination of moisture content - Gravimetric method; --- Part 11. Determination of the amount of fluorine EDTA titration. This section section 10. This part is GB/T 18114.10-2000 "Methods for chemical analysis of monazite concentrates - Determination of water content" amendment. This section compared with the GB/T 18114.10-2000, have the following main changes. --- Measurement range from 0.02 to 1.00% was adjusted to 0.02% ~ 20.00%; --- Drying time from 3h sample was adjusted to 2h; --- Increasing the precision of the terms; --- Increased quality assurance and control provisions. This part of the National Standardization Technical Committee of rare earth (SAC/TC229) centralized. This section is Baotou Rare Earth Research Institute, China Nonferrous Metals Industry Institute of Standards Metrology and Quality is responsible for drafting. This section was drafted by the Baotou Rare Earth Research Institute. This part of the Inner Mongolia Baotou Steel Rare Earth (Group) Hi-Tech Company, China North Nuclear Fuel Co., Ltd. participated in the drafting. The main drafters of this section. Li Jing Yan, Hao Qian. The drafters of some of the participants. Wu Guangwei, Zhanggui Mei, Zhou Xiaodong, Liu Lisha, Dong red. This part of the standard replaces the previous editions are. --- GB/T 18114.10-2000. Methods for chemical analysis of rare earth concentrates Part 10. Determination of moisture content - Gravimetric method

1 Scope

GB/T 18114 provisions of this part of the determination of rare earth concentrates moisture. This section applies to the determination of rare earth concentrates in moisture measurement range. 0.02% to 20.00%.

2 principle of the method

Weigh a certain amount of rare earth concentrate sample, dried at 105 ℃ ~ 110 ℃ certain period of time, said its loss of quality, calculate the amount of water.

3 instruments and reagents

3.1 Oven. temperature greater than 110 ℃. 3.2 weighing bottle. 3.3 Balance. a sense of the amount of 0.0001g.

4 Sample

Rare earth concentrate sample sealed. Step 5 Analysis 5.1 Sample Weigh 10g ~ 20g sample (4), accurate to 0.0001g. 5.2 Determination of the number of Weigh two samples (5.1) parallel determination of the mean value. 5.3 Determination A sample (5.1) into constant weight weighing bottle (3.2), and placed 105 ℃ ~ 110 ℃ oven bake 2h, remove, add dried coolish Dryer, cooled to room temperature, weighed, and repeat this operation until constant weight.

6 Calculation and presentation of analysis results

According to equation (1) calculate the water content (%). w (H2O) = m1-m2m × 100 (1) Where. Mass m1 --- weighing bottle and sample before drying, in units of grams (g); Mass m2 --- dried sample and weighing bottle in grams (g); M --- the quality of the sample, in grams (g).

7 precision

7.1 Repeatability Found two independent test results obtained under repeatability conditions within the average range given below, these two test results The absolute difference does not exceed the repeatability limit (r), exceeds the repeatability limit (r) does not exceed 5% repeatability limit (r) by the data in Table 1 using a linear Obtained by interpolation.

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