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GB/T 17413.3-2010 | English | 139 |
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Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 3: Determination of cesium content
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GB/T 17413.3-2010
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GB/T 17413.3-1998 | English | 239 |
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Methods for chemical analysis of lithium, rubidium and cesium ores. Determination of Cesium content. Flame atomic absorption/emission spectrophotometric method
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GB/T 17413.3-1998
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Basic data Standard ID | GB/T 17413.3-2010 (GB/T17413.3-2010) | Description (Translated English) | Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 3: Determination of cesium content | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | D43 | Classification of International Standard | 73.060 | Word Count Estimation | 6,623 | Date of Issue | 2010-11-10 | Date of Implementation | 2011-02-01 | Older Standard (superseded by this standard) | GB/T 17413.3-1998 | Quoted Standard | GB/T 6682 | Regulation (derived from) | National Standard Approval Announcement 2010 No.8 (Total No.163) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the lithium ores, rubidium ores, determination of the amount of cesium cesium oxide ores. This section applies to lithium ore, rubidium ore, cesium ores, also applies to tantalum, determination of the amount of cesium oxide ore of niobium and rare earth ores. Measuring range: 10��g/g ~ 1 �� 104��g/g of cerium oxide. Warning-this part of the staff should be using regular laboratory work experience. This section does not indicate that all possible safety problems. Users are responsible for taking appropriate safety and health practices, and to ensure compliance with the relevant conditions of the national regulations. |
GB/T 17413.3-2010: Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 3: Determination of cesium content ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of lithium, rubidium and cesium ores Part 3. Determination of cesium content
ICS 73.060
D43
National Standards of People's Republic of China
Replacing GB/T 17413.3-1998
Lithium ore, ore rubidium, cesium ores chemical analysis
Part 3. Determination of the amount of cesium
Methodsforchemicalanalysisoflithium, rubidiumandcesiumores-
Part 3. Determinationofcesiumcontent
Issued on. 2010-11-10
2011-02-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 17413 "lithium ore, ore rubidium, cesium ores chemical analysis method" is divided into three parts.
--- Part 1. Determination of the amount of lithium;
--- Part 2. Determination of the amount of rubidium;
--- Part 3. Determination of the amount of cesium.
This section GB/T 17413 Part 3.
This Part replaces GB/T 17413.3-1998 "lithium ore, ore rubidium, cesium ores Chemical analysis by flame atomic absorption/emission points
Determination of the amount of cesium, "spectrophotometric method.
This section compared with the GB/T 17413.3-1998, the main changes are as follows.
--- Modify the standard Chinese name;
--- Modify the standard English name;
--- Increased alert, warning of the content;
--- Increasing the purity of the reagents used and experimental water requirements;
--- Increasing the particle size of the sample and drying requirements;
--- Increased verification test content.
Appendix A of this section is informative appendix.
This section presents the People's Republic of China Ministry of Land Resources.
This part of the National Standardization Technical Committee under the jurisdiction of Land and Resources.
This section is responsible for drafting. National geology test center.
This section is drafted. Hubei Institute of Geology.
The main drafters of this section. to Zhao, Fang Jindong, Tangxing Min.
This part of the standard replaces the previous editions are.
--- GB/T 17413.3-1998.
Lithium ore, ore rubidium, cesium ores chemical analysis
Part 3. Determination of the amount of cesium
Warning. Use of this standard shall have a person experiences regular laboratory work. This section does not indicate that all possible security issues.
Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.
1 Scope
GB/T 17413 provisions of this part of lithium ore, ore rubidium, cesium ores Determination of amount of cesium oxide ores.
This section applies to lithium ore, ore rubidium, cesium ore minerals, but also for tantalum, niobium, cesium oxide ore and the determination of the amount of rare earth mineral.
Measuring range. 10μg/g ~ 1.0 × 104μg/g of cesium oxide.
2 Normative references
The following documents contain provisions which, through GB/T 17413 in this part of the reference in terms of this section. For dated reference documents
Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section
Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this
section.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Sample hydrofluoric acid, sulfuric acid decomposition of the samples contained traces of cesium oxide, the dispensing part extract separation with ammonia and ammonium carbonate, iron and aluminum
An alkaline earth metal; cerium oxide samples containing higher amounts of directly dispensing the extract, then adding a certain amount of potassium as deionization agent, in 1% sulfuric acid medium
Quality, and on the atomic absorption spectrophotometer, at a wavelength of 852.1nm, using air - acetylene flame measured absorbance or cerium oxide emission intensity
Degrees, calculate the amount of cesium oxide.
4 Reagents
Unless otherwise indicated in the analysis are consistent with the use of analytical reagents and GB/T 6682 water analytical laboratory.
4.1 Hydrofluoric acid (ρ1.13g/mL). WARNING. Hydrofluoric acid is toxic and corrosive, the operation should wear gloves to prevent skin contact
4.2 sulfate (11). Warning. When diluted improper operation could easily cause burns
4.3 potassium chloride solution ρ (K2O) = 30mg/mL. Take 47.49g potassium chloride (KCl) in a beaker, dissolved in water and transferred to 1000mL capacity
Volumetric flask, dilute to the mark, shake.
4.4 Aqueous ammonia (11).
4.5 ammonium carbonate solution [ρ (NH4HCO3 NH2COONH4) = 100g/L].
4.6 ammonium carbonate solution [ρ (NH4HCO3 NH2COONH4) = 10g/L].
Cesium oxide 4.7 Standard solution.
a) cerium oxide standard stock solution. Weigh 0.5974g spectroscopically pure cesium chloride (105 ℃ bake 2h and placed in the dryer to cool to room
Temperature) in 250mL beaker, add water, dissolved and transferred to 1000mL volumetric flask, dilute to the mark, shake. This solution
Cerium oxide concentration was 0.50mg/mL;
b) cerium oxide standard solution. Pipette 25.00mL cesium oxide standard stock solution [4.7a)], set 500mL flask with water
Dilute to the mark. Cerium oxide concentration of the solution was 25.00μg/mL.
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