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GB/T 17413.2-2010 | English | 139 |
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Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 2: Determination of rubidium content
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GB/T 17413.2-2010
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GB/T 17413.2-1998 | English | 199 |
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Methods for chemical analysis of Lithium, Rubidium and Cesium ores. Determination of Rubidium content. Flame atomic absorption/emission spectrophotometric method
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GB/T 17413.2-1998
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Basic data Standard ID | GB/T 17413.2-2010 (GB/T17413.2-2010) | Description (Translated English) | Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 2: Determination of rubidium content | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | D43 | Classification of International Standard | 73.060 | Word Count Estimation | 6,696 | Date of Issue | 2010-11-10 | Date of Implementation | 2011-02-01 | Older Standard (superseded by this standard) | GB/T 17413.2-1998 | Quoted Standard | GB/T 6682 | Regulation (derived from) | National Standard Approval Announcement 2010 No.8 (Total No.163) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the lithium ores, rubidium ores, determination of the amount of cesium rubidium oxide ores. This section applies to lithium ore, rubidium ore, cesium ores, also applies to tantalum, determination of niobium and rare earth ores amount of rubidium oxide ores, measuring range: 50��g/g ~ 2 �� 104��g/g of rubidium oxide. Warning-this part of the staff should be using regular laboratory work experience. This section does not indicate that all possible safety problems. Users are responsible for taking appropriate safety and health practices, and to ensure compliance with the relevant conditions of the national regulations. |
GB/T 17413.2-2010: Methods for chemical analysis of lithium, rubidium and cesium ores -- Part 2: Determination of rubidium content ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of lithium, rubidium and cesium ores Part 2. Determination of rubidium content
ICS 73.060
D43
National Standards of People's Republic of China
Replacing GB/T 17413.2-1998
Lithium ore, ore rubidium, cesium ores chemical analysis
Part 2. Determination of the amount of rubidium
Methodsforchemicalanalysisoflithium, rubidiumandcesiumores-
Part 2. Determinationofrubidiumcontent
Issued on. 2010-11-10
2011-02-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 17413 "lithium ore, ore rubidium, cesium ores chemical analysis method" is divided into three parts.
--- Part 1. Determination of the amount of lithium;
--- Part 2. Determination of the amount of rubidium;
--- Part 3. Determination of the amount of cesium.
This section GB/T 17413 Part 2.
This Part replaces GB/T 17413.2-1998 "lithium ore, ore rubidium, cesium ores Chemical analysis by flame atomic absorption/emission points
Determination of the amount of rubidium "spectrophotometric method.
This section compared with the GB/T 17413.2-1998, the main changes are as follows.
--- Modify this part of Chinese name;
--- Modify this part of the English name;
--- Increased alert, warning of the content;
--- Increasing the purity of the reagents used and experimental water requirements;
--- Increasing the particle size of the sample and drying requirements;
--- Increased verification test content.
Appendix A of this section is informative appendix.
This section presents the People's Republic of China Ministry of Land Resources.
This part of the National Standardization Technical Committee under the jurisdiction of Land and Resources.
This section is responsible for drafting. National geology test center.
This section is drafted. Hubei Institute of Geology.
The main drafters of this section. to Zhao, Fang Jindong, Tangxing Min.
This part of the standard replaces the previous editions are.
--- GB/T 17413.2-1998.
Lithium ore, ore rubidium, cesium ores chemical analysis
Part 2. Determination of the amount of rubidium
Warning. Use of this standard shall have a person experiences regular laboratory work. This section does not indicate that all possible security issues.
Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.
1 Scope
GB/T 17413 provisions of this part of lithium ore, ore rubidium, cesium method of measuring the amount of rubidium oxide ores.
This section applies to lithium ore, ore rubidium, cesium ores, but also for tantalum, niobium, rubidium oxide ore and the determination of the amount of rare earth mineral.
Measuring range. 50μg/g ~ 2 × 104μg/g of rubidium oxide.
2 Normative references
The following documents contain provisions which, through GB/T 17413 in this part of the reference in terms of this section. For dated reference documents
Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section
Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this
section.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Sample hydrofluoric acid, sulfuric acid decomposition, adding a certain amount of potassium as deionization agent, 1% sulfuric acid medium, atomic absorption spectrophotometry
Acetylene flame measured absorbance or rubidium oxide emission intensity, calculated the amount of rubidium oxide - on the meter, at a wavelength of 780.0nm, the use of air.
4 Reagents
Unless otherwise indicated in the analysis are consistent with the use of analytical reagents and GB/T 6682 water analytical laboratory.
4.1 Hydrofluoric acid (ρ1.13g/mL). WARNING. Hydrofluoric acid is toxic and corrosive, the operation should wear gloves to prevent skin contact
4.2 sulfate (11). Warning. When diluted improper operation could easily cause burns
4.3 potassium chloride solution ρ (K2O) = 30mg/mL. Weigh 47.49g potassium chloride (KCl) in a beaker, dissolved in water and transferred to 1000mL
Volumetric flask, dilute to the mark, shake.
Rubidium oxide 4.4 Standard solution.
a) rubidium oxide standard stock solution. Weigh 0.6469g spectroscopically pure rubidium chloride (105 ℃ bake 2h and placed in the dryer to cool to room
Temperature) in 250mL beaker, add water, dissolved and transferred to 500mL volumetric flask, dilute to the mark, shake. This solution oxygen
Rubidium concentration of 1.0mg/mL;
b) rubidium oxide standard solution. Pipette 25.00mL rubidium oxide standard stock solution [4.4a)], set 500mL flask with water
Dilute to the mark. Rubidium oxide concentration of the solution was 50.00μg/mL.
5 Instruments
5.1 atomic absorption spectrophotometer (with transmitter function). Attached rubidium element hollow cathode lamp.
5.2 Analytical balance. three, a sense of the amount of 0.1mg.
6 Sample
6.1 Sample particle size less than 74μm.
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