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Test method of impermeable graphite materials - Part 12: Thermal conductivity
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GB/T 13465.12-2023
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Basic data Standard ID | GB/T 13465.12-2023 (GB/T13465.12-2023) | Description (Translated English) | Test method of impermeable graphite materials - Part 12: Thermal conductivity | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G94 | Classification of International Standard | 71.120 | Word Count Estimation | 11,142 | Date of Issue | 2023-11-27 | Date of Implementation | 2024-06-01 | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration |
GB/T 13465.12-2023: Test method of impermeable graphite materials - Part 12: Thermal conductivity---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 71:120
CCSG94
National Standards of People's Republic of China
Test methods for impermeable graphite materials
Part 12: Thermal conductivity
Part 12: Thermalconductivity
2024-06-01 Implementation
State Administration for Market Regulation
Released by the National Standardization Administration Committee
Table of contents
PrefaceⅠ
Introduction II
1 Scope 1
2 Normative references 1
3 Terms and Definitions 1
4 Principle 1
5 Test equipment and materials 1
6 Sample 3
7 Test method 4
8 Test results 5
9 test report 6
Foreword
This document complies with the provisions of GB/T 1:1-2020 "Standardization Work Guidelines Part 1: Structure and Drafting Rules of Standardization Documents"
Drafting:
This document is Part 12 of GB/T 13465: GB/T 13465 has released the following parts:
---Test Methods for Impermeable Graphite Materials Part 1: General Principles of Mechanical Properties Test Methods;
---Test methods for impermeable graphite materials Part 2: Flexural strength;
---Test methods for impermeable graphite materials Part 3: Compressive strength;
---Test methods for impermeable graphite materials Part 4: Impact strength;
---Test method for shrinkage of impermeable graphite phenolic adhesive;
---Water pressure burst test method for impermeable graphite tubes;
---Test method for weight gain rate and porosity filling rate of impermeable graphite;
---Test method for bonding shear strength of impermeable graphite adhesive;
---Test method for tensile strength of impermeable graphite adhesive;
---Test methods for impermeable graphite materials Part 12: Thermal conductivity:
Please note that some content in this document may be subject to patents: The publisher of this document assumes no responsibility for identifying patents:
This document is proposed by China Petroleum and Chemical Industry Federation:
This document is under the jurisdiction of the National Technical Committee for Standardization of Non-Metallic Chemical Equipment (SAC/TC162):
This document was drafted by: Nantong Shanjian Anti-corrosion Technology Co:, Ltd:, Nantong Planet Graphite Co:, Ltd:, Guangzhou Special Pressure Equipment Inspection
Testing Research Institute, Nantong Jingtong Graphite Equipment Co:, Ltd:, Jiangsu Special Equipment Safety Supervision and Inspection Institute, Nantong Best Graphite Equipment Co:, Ltd:
Co:, Ltd:, Nantong Institute of Technology, Zhejiang Huarong Technology Co:, Ltd:, Suzhou Taijinuo New Materials Technology Co:, Ltd:, Guangdong Siquan New Materials Co:, Ltd:
Co:, Ltd:, Tianhua Chemical Machinery and Automation Research and Design Institute Co:, Ltd:
The main drafters of this document: Wang Xiaoliang, Chen Jun, Li Maodong, Chen Hanjun, Deng Zhiqiang, Yao Songnian, Chen Hanming, Zhao Guihua, He Hua, Yang Jun,
Yu Peng, Zhou Zhiqiang, Li Zhaoqiang, Ren Zeming, Xiao Lijuan, He Zhengwen, Sang Linchun:
Introduction
GB/T 13465 aims to accurately measure the mechanical properties, permeability and thermal conductivity of impermeable graphite materials used in chemical production: It is proposed to be
Composed of 12 parts:
---Part 1: General principles: The purpose is to provide basic requirements and principles for performance testing of impermeable graphite materials:
---Part 2: Flexural strength: The purpose is to determine the flexural strength of impermeable graphite materials:
---Part 3: Compressive strength: The purpose is to determine the compressive strength of impermeable graphite materials:
---Part 4: Impact strength: The purpose is to determine the impact strength of impermeable graphite materials:
---Part 5: Phenolic adhesive shrinkage: The purpose is to determine the shrinkage rate of impermeable graphite phenolic adhesive:
---Part 6: Hydraulic blasting of graphite tubes: The purpose is to determine the hydraulic bursting performance of impermeable graphite tubes:
---Part 7: Weight gain rate and hole filling rate: The purpose is to determine the weight gain rate and pore filling rate of impermeable graphite:
---Part 8: Adhesive bonding shear strength: The purpose is to determine the bonding shear strength of impermeable graphite adhesives:
---Part 9: Adhesive bonding tensile strength: The purpose is to determine the bonding tensile strength of impermeable graphite adhesive:
---Part 10: Tensile strength: The purpose is to determine the tensile strength of impermeable graphite materials:
---Part 11: Permeability coefficient: The purpose is to determine the permeability coefficient of impermeable graphite materials:
---Part 12: Thermal conductivity: The purpose is to determine the thermal conductivity of impermeable graphite materials:
Thermal conductivity is one of the most important performance parameters of impermeable graphite materials and is used to evaluate impermeable graphite heat exchangers:
Thermal conductivity performance is an essential performance parameter for calculating the heat transfer area of impermeable graphite heat exchangers:
Because impermeable graphite equipment has excellent thermal conductivity, corrosion resistance and temperature resistance, it is mostly used in heat exchange equipment and is a
It is a very important anti-corrosion heat exchange equipment with large usage and wide application range: The advantages and disadvantages of thermal conductivity of impermeable graphite materials are directly
It is related to the heat transfer efficiency of impermeable graphite heat exchanger: This document is formulated to accurately determine the thermal conductivity of impermeable graphite materials and improve
Material properties, improve the accuracy of equipment heat exchange area calculation and equipment heat exchange efficiency, and promote the high quality of my country's impermeable graphite equipment manufacturing industry
Development is of great significance:
Test methods for impermeable graphite materials
Part 12: Thermal conductivity
1 Scope
This document describes a method for measuring the thermal conductivity of impermeable graphite materials:
This document is suitable for measuring the thermal conductivity of impermeable graphite materials at room temperature between 20°C and 40°C using the comparative method:
This document is applicable to the measurement of thermal conductivity of impermeable graphite materials with thermal conductivity less than or equal to 250W/(m·K):
2 Normative reference documents
The contents of the following documents constitute essential provisions of this document through normative references in the text: Among them, the dated quotations
For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to
this document:
HG/T 2370 Technical conditions for chemical equipment made of impermeable graphite
3 Terms and definitions
There are no terms or definitions to be defined in this document:
4 Principles
Fix the standard sample with known thermal conductivity between two measuring heads with set temperature (see Figure 1), so that the two ends of the sample are in contact with the measuring head end:
The measuring head is divided into a heating end (hereinafter referred to as "hot end") and a cooling end (hereinafter referred to as "cold end"): The set temperature of the hot end is
40℃±0:1℃, the cold end set temperature is 20℃±0:1℃: The temperature at both ends of the head to be measured is stable at the set temperature, and the voltage value at the hot end is within
When it remains unchanged for more than 10 minutes, record the heating voltage value of the hot end: By measuring standard tests of the same material, same diameter, and different heights
sample, draw the U-λ/h curve (see Figure 2), where U is the hot end voltage value, in mV; λ is the thermal conductivity of the standard sample, in unit
W/(m·K); h is the height of the standard sample, in mm: Then, use the test sample instead of the standard sample for testing, and the head temperature to be measured
When the temperature is stable at 40℃±0:1℃ and 20℃±0:1℃ respectively, record the heating voltage value of the hot end, and then, with the help of the drawn U-λ/h curve
Figure, Calculate the thermal conductivity of the test specimen:
The thermal conductivity of the standard sample material should be similar to the thermal conductivity of the tested sample material:
5 Test equipment and materials
5:1 Test device
The schematic diagram of the thermal conductivity measurement device is shown in Figure 1:
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