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GA/T 597-2006 English PDF

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GA/T 597-2006: Qualitative and quantitative analysis for Xylazoli in poisoning samples
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Basic data

Standard ID GA/T 597-2006 (GA/T597-2006)
Description (Translated English) Qualitative and quantitative analysis for Xylazoli in poisoning samples
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Classification of International Standard 13.310
Word Count Estimation 8,844
Date of Issue 2006-01-17
Date of Implementation 2006-05-01
Quoted Standard GA/T 122-1995
Issuing agency(ies) Ministry of Public Security
Summary This standard prescribes the test method of Jing Songling in poisoned samples. This standard is applicable to qualitative analysis and quantitative analysis of Jingsongling in poisoned samples.

GA/T 597-2006: Qualitative and quantitative analysis for Xylazoli in poisoning samples

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Qualitative and quantitative analysis for Xylazoli in poisoning samples ICS 13.310 A92 People's Republic of China Public Safety Industry Standard Qualitative and quantitative analysis method of Jingsongling in poisoning samples Released on.2006-01-17 2006-05-01 implementation Ministry of Public Security

Foreword

This standard is proposed and managed by the Technical Committee of the National Institute of Criminal Technology Standardization. This standard was drafted. the Criminal Police Detachment of the Public Security Bureau of Jinan City, Shandong Province, and the Science and Technology Department of the Shandong Provincial Public Security Department. The main drafters of this standard. Liang Kaijun, Li Changli, Chen Lujun, Liu Haiyan, Wang Ke. Qualitative and quantitative analysis method of Jingsongling in poisoning samples

1 Scope

This standard specifies the test method for Jingsongling in poisoning samples. This standard is applicable to the qualitative analysis and quantitative analysis of Jingsongling in poisoning samples.

2 Normative references

The terms in the following documents become the terms of this standard by reference to this standard. All dated references, followed by all Modifications (not including errata content) or revisions do not apply to this standard, however, parties to agreements based on this standard are encouraged to study Is it possible to use the latest version of these files? For undated references, the latest edition applies to this standard. GA/T 122-1995 Toxic Analysis Terminology

3 Terms and definitions

The following terms and definitions established in GA/T 122-1995 apply to this standard. 3.1 C11H14N2S = 206.3, other names. xylylamine thiazole. 3.2 C23H31NO2=353.3, other names. propyl acetaminophen, poluricin.

4 samples

4.1 The vomit, blood, and urine of the poisoned person. 4.2 The stomach and leftover food, stomach contents, urine, lung, liver, kidney, heart, brain and blood of poisoned corpses. 4.3 For those who are suspected of being injected into the human body, muscles, suspicious injections, syringes and utensils at the injection site are also required. 5 gas chromatography, gas chromatography-mass spectrometry 5.1 Principle 5.1.1 Principle of Gas Chromatography (GC/NPD) This method uses SKF525A as the internal standard, after separation, purification, concentration, and gas chromatography with nitrogen and phosphorus detector (NPD). Detected; characterized by retention time or relative retention time compared to Jingsongling standard; parallel reference with parallel operation (known concentration Jingsongling and SKF525A) were compared, and the content of Jingsongling in the sample was calculated by internal standard method according to the ratio of peak height to peak area. 5.1.2 Principle of Gas Chromatography-Mass Spectrometry (GC/MS) This method is based on the mass spectrum of Jingsongling peak; the ion peak of mass/charge ratio M/Z206 is selected for Jingsongling, and the internal standard is used to select the mass-to-charge ratio. The ion peak of M/Z86 is compared with the parallel reference (known concentrations of Jingsongling and SKF525A), based on peak height ratio or peak surface The product value ratio was calculated by internal standard method to calculate the content of Jingsongling in the sample. 5.2 Reagents 5.2.1 Conventional reagents The reagents used in this method are of analytical grade, and the test water is distilled water. a) methanol;

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