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GA/T 1934-2021 English PDF

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GA/T 1934-2021: Forensic sciences - Examination methods for six ephedrine class substances including norephedrine in suspected precursors - GC-MS, LC and LC-MS
Status: Valid
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GA/T 1934-2021English509 Add to Cart 4 days [Need to translate] Forensic sciences - Examination methods for six ephedrine class substances including norephedrine in suspected precursors - GC-MS, LC and LC-MS Valid GA/T 1934-2021

PDF similar to GA/T 1934-2021


Standard similar to GA/T 1934-2021

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Basic data

Standard ID GA/T 1934-2021 (GA/T1934-2021)
Description (Translated English) Forensic sciences - Examination methods for six ephedrine class substances including norephedrine in suspected precursors - GC-MS, LC and LC-MS
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Word Count Estimation 22,277
Issuing agency(ies) Ministry of Public Security

GA/T 1934-2021: Forensic sciences - Examination methods for six ephedrine class substances including norephedrine in suspected precursors - GC-MS, LC and LC-MS


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences -- Examination methods for six ephedrine class substances including norephedrine in suspected precursors -- GC-MS, LC and LC-MS ICS 13.310 CCSA92 People's Republic of China Public Safety Industry Standards Forensic Science Suspected Precursor Chemicals Norepine 6 kinds of ephedrines such as flavonoids are tested for gas phase Chromatography-Mass Spectrometry, Liquid Chromatography, and Liquid Chromatography-Mass Spectrometry LCandLC-MS Published on 2021-10-14 2022-05-01 Implementation Published by the Ministry of Public Security of the People's Republic of China

foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents" drafted. Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents. This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1). focal point. This document is drafted by. Anti-drug Information Technology Center of the Ministry of Public Security. The main drafters of this document. Hua Zhendong, Li Jing, Han Yu, Liu Cuimei, Li Tao, Zhang Tingting. Forensic Science Suspected Precursor Chemicals Norepine

6 kinds of ephedrines such as flavonoids are tested for gas phase

Chromatography-Mass Spectrometry, Liquid Chromatography, and Liquid Chromatography-Mass Spectrometry

1 Scope

This document specifies that norephedrine, norpseudoephedrine, ephedrine, pseudoephedrine, Gas chromatography-mass spectrometry (GC-mass spectrometry) of base ephedrine and N-methyl-1-phenyl-1-chloro-2-propylamine MS), liquid chromatography-mass spectrometry (LC-MS) qualitative test method and liquid chromatography (LC) quantitative test method. This document applies to norephedrine, norephedrine, ephedrine, pseudoephedrine, Qualitative and quantitative analysis of ephedrine and N-methyl-1-phenyl-1-chloro-2-propylamine.

2 Normative references

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to this document. GB/T 6682 Analysis Laboratory Water Specifications and Test Methods GA/T 122 Toxic Analysis Terminology

3 Terms and Definitions

Terms and definitions defined in GA/T 122 apply to this document.

4 Principles

Norephedrine, norephedrine, ephedrine, pseudoephedrine, methylephedrine and N-methyl-1- Phenyl-1-chloro-2-propylamine (see Appendix A for compound information) was extracted. Gas chromatography-mass spectrometry was used to detect retention time, characteristic ions and The ion abundance ratio was used as the basis for qualitative judgment; liquid chromatography-mass spectrometry was used for detection, and the retention time, mass spectral characteristic ion pairs and ion pair abundance ratios were used for detection. As the basis for qualitative judgment; liquid chromatography was used for detection, the chromatographic peak area was used as the quantitative basis, and the external standard single-point method or the external standard standard curve method was used. Perform quantitative analysis.

5 Reagents and Materials

5.1 Reagents The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade, Reagents include. a) methanol; b) n-hexane; c) Anhydrous sodium sulfate. analytically pure;

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