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Forensic sciences - Examination methods for (S)-methamphetamine and (R)-methamphetamine in suspected drugs - LC and LC-MS
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GA/T 1933-2021
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Basic data Standard ID | GA/T 1933-2021 (GA/T1933-2021) | Description (Translated English) | Forensic sciences - Examination methods for (S)-methamphetamine and (R)-methamphetamine in suspected drugs - LC and LC-MS | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | Classification of Chinese Standard | A92 | Word Count Estimation | 19,166 | Issuing agency(ies) | Ministry of Public Security |
GA/T 1933-2021: Forensic sciences - Examination methods for (S)-methamphetamine and (R)-methamphetamine in suspected drugs - LC and LC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for (S)-methamphetamine and (R)-methamphetamine in suspected drugs - LC and LC-MS
ICS 13.310
CCSA92
People's Republic of China Public Safety Industry Standards
Forensic Science Suspected Drug L-Methamphetamine
and dextromethamphetamine test
Liquid chromatography and liquid chromatography-mass spectrometry
Published on 2021-10-14
2022-05-01 Implementation
Published by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1).
focal point.
This document is drafted by. Physical Evidence Identification Center of the Ministry of Public Security, Anti-drug Information Technology Center of the Ministry of Public Security, Criminal Justice Department of Xinjiang Uygur Autonomous Region Public Security Department
Investigation Corps, People's Public Security University of China.
The main drafters of this document. Zhao Yanbiao, Yang Hongxian, Zhai Wanfeng, Zheng Hui, Zhang Chunshui, Xu Peng, Li Wei, He Hongyuan, Zhao Yang, Qian Zhenhua, Chang Ying,
Li Peng, Zheng Xiaoyu, Wen Wu, Liu Kelin, Gao Lisheng.
Forensic Science Suspected Drug L-Methamphetamine
and dextromethamphetamine test
Liquid chromatography and liquid chromatography-mass spectrometry
1 Scope
This document specifies the liquid chromatography-mass spectrometry of L-Methamphetamine and D-Methamphetamine in suspected drug samples in the field of forensic science
(LC-MS) qualitative test method and liquid chromatography (LC) quantitative test method.
This document applies to the qualitative analysis and analysis of L-Methamphetamine and D-Methamphetamine in solid samples of suspected narcotics in the field of forensic science.
Quantitative analysis.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 6682 Analysis Laboratory Water Specifications and Test Methods
GB/T 27418 Evaluation and representation of measurement uncertainty
GA/T 122 Toxic Analysis Terminology
3 Terms and Definitions
Terms and definitions defined in GA/T 122 apply to this document.
4 Principles
Extraction of L-methamphetamine and D-methamphetamine (see Appendix A for compound information) in suspected drug samples. using liquid
Gas chromatography-mass spectrometry detection, with retention time, mass spectrometry characteristic ion pair and ion pair abundance ratio as the qualitative judgment basis; liquid chromatography detection was used.
The chromatographic peak area was used as the quantitative basis, and the external standard single-point method or the external standard standard curve method was used for quantitative analysis.
5 Reagents and Materials
5.1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade,
Reagents include.
a) methanol;
b) Ethanol;
c) n-hexane;
d) isopropyl alcohol;
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