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Forensic sciences - Screening methods for 29 drugs and metabolites including morphine in biological samples - LC-MS
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GA/T 1903-2021
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Basic data | Standard ID | GA/T 1903-2021 (GA/T1903-2021) | | Description (Translated English) | Forensic sciences - Screening methods for 29 drugs and metabolites including morphine in biological samples - LC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.310 | | Word Count Estimation | 24,238 | | Date of Issue | 2021-10-14 | | Date of Implementation | 2022-05-01 | | Issuing agency(ies) | Ministry of Public Security |
GA/T 1903-2021: Forensic sciences - Screening methods for 29 drugs and metabolites including morphine in biological samples - LC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310
CCSA92
People's Republic of China Public Security Industry Standards
Morphine and other 29 kinds of drugs and
Metabolite Screening Liquid Chromatography-Mass Spectrometry
Released on 10-14-2021
2022-05-01 implementation
Released by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules for Standardization Documents"
drafting.
Please note that some contents of this document may refer to patents. The issuing agency of this document assumes no responsibility for identifying patents.
This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted
Focus on.
This document was drafted by. The Physical Evidence Appraisal Center of the Ministry of Public Security, the Narcotics Detachment of the Nanjing Public Security Bureau of Jiangsu Province, and the Public Security Department of Guangxi Zhuang Autonomous Region
Investigation Corps, Criminal Technology Center of Guangdong Provincial Public Security Bureau, Criminal Police Detachment of Shenzhen Public Security Bureau, Physical Evidence Identification Center of Chongqing Public Security Bureau, Shanghai Public Security Bureau
Public Security Bureau Evidence Identification Center, People's Public Security University of China, Criminal Science and Technology Research Institute of Jining Public Security Bureau, Criminal Science and Technology of Hangzhou Public Security Bureau
graduate School.
The main drafters of this document. Chang Jing, Song Ge, Wang Ruihua, Zhang Zhonghui, Huang Kejian, Pei Maoqing, Li Shuhui, He Jianfeng, Shi Yintao, Liang Chen,
Wang Aihua, Zhang Yunfeng, Yu Zhongshan, Wang Jifen, Liu Xiaofeng, Zhang Liang, Wang Rong, Qu Xiaojing, Ying Jianbo, Hong Liang.
Morphine and other 29 kinds of drugs and
Metabolite Screening Liquid Chromatography-Mass Spectrometry
1 Scope
This document specifies the liquid chromatography-mass spectrometry screening method for 29 drugs such as morphine in forensic science biological samples (blood, urine).
This document applies to the qualitative analysis of 29 drugs in forensic science biological samples (blood, urine). Other test materials can be used as reference.
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text. Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document.
GB/T 6682 Analytical laboratory water specifications and test methods
GA/T 122 Toxicological Analysis Terminology
3 Terms and definitions, abbreviations
3.1 Terms and Definitions
The terms and definitions defined in GA/T 122 apply to this document.
3.2 Abbreviations
The following abbreviations apply to this document.
spectrometry)
4 principles
Using the blank sample and the added sample as a control, according to the requirements of parallel operation, the 29 kinds of drugs in the biological samples (see Appendix A) were tested.
Extraction, purification and concentration were performed by liquid chromatography-triple quadrupole tandem mass spectrometry (LC-TQ/MS) and liquid chromatography-high resolution mass spectrometry (LC-
HRMS) detection.
5 Reagents and Materials
5.1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are chromatographic
Pure, reagents include.
a) Methanol;
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