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GA/T 1647-2019: Forensic sciences - Examination methods for five benzodiazepines including bromozepam in suspected drugs - LC and LC-MS
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Forensic sciences - Examination methods for five benzodiazepines including bromozepam in suspected drugs - LC and LC-MS
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GA/T 1647-2019
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Basic data | Standard ID | GA/T 1647-2019 (GA/T1647-2019) | | Description (Translated English) | Forensic sciences - Examination methods for five benzodiazepines including bromozepam in suspected drugs - LC and LC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.310 | | Word Count Estimation | 18,128 | | Date of Issue | 2019 | | Date of Implementation | 2019-12-01 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1647-2019: Forensic sciences - Examination methods for five benzodiazepines including bromozepam in suspected drugs - LC and LC-MS
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Forensic sciences - Examinationg methods for five benzodiazepines including bromozepam in suspected drugs - LC and LC-MS
ICS 13.310
A92
Public Safety Industry Standard of the People's Republic of China
Forensic science suspects five kinds of drugs including brozepam
Liquid Chromatography and Benzodiazepines Testing
Liquid chromatography-mass spectrometry
Published on October 14,.2019
2019-12-01 Implementation
Issued by the Ministry of Public Security of the People's Republic of China
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some content of this document may involve patents. The issuer of this document does not assume responsibility for identifying these patents.
This standard was proposed by the National Toxic Analysis Sub-Committee of Criminal Technology Standardization Technical Committee (SAC/TC179/SC1) and
Be in charge.
This standard was drafted by. Physical Evidence Appraisal Center of the Ministry of Public Security, Tianjin Public Security Bureau.
The main drafters of this standard. Gao Lisheng, Zhang Chunshui, Zheng Hun, Zhai Wanfeng, Wang Qun, Chang Ying, Zhao Yang, He Jianfeng, Liu Kelin, Huang Xing, Wang Yi,
Wang Weixin, Zhao Yanbiao, Li Peng, Yang Hongxian, Zheng Xiaoyu.
Forensic science suspects five kinds of drugs including brozepam
Liquid Chromatography and Benzodiazepines Testing
Liquid chromatography-mass spectrometry
1 Scope
This standard specifies the benzodiazepines (brozepam, chlordiazepoxide, diazepam, estazolam and triazole) in suspected drugs in the field of forensic science.
Liquid chromatography-mass spectrometry (LC-MS) qualitative test method and liquid chromatography (LC) quantitative test method.
This standard applies to benzodiazepines (brazepam, chlordiazepoxide, diazepam, estazolam and triazole) in suspected drugs in the field of forensic science
Qualitative analysis and quantitative analysis.
2 Normative references
The following documents are essential for the application of this document. For dated reference documents, only the dated version applies to this article
Pieces. For the cited documents without date, the latest version (including all amendments) applies to this document.
GB/T 4883-2008 Statistical processing of data and interpretation of judgment and processing of normal sample outliers
GB/T 6682 Analysis of laboratory water specifications and test methods
JJF1059.1-2012 Evaluation and expression of measurement uncertainty
GA/T 122 Nomenclature of poison analysis
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principle
Extract bromozepam (chlordiazepam, diazepam, estazolam or triazolam) from suspected drug samples. Liquid chromatography-mass spectrometry
For detection, the retention time, characteristic ion fragment peak of mass spectrometry and ion abundance ratio are used as the basis for qualitative judgment; liquid chromatography is used for detection, and standard music is used.
Line method for quantitative analysis.
5 Reagents and materials
5.1 Reagents
The experimental water shall comply with the first-grade water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are chromatographically pure,
Reagents include.
a) Acetonitrile;
b) methanol;
c) Standard solution.
1) Standard substance solution. 1.0mg/mL bromazepam (chlorazide, diazepam, estazolam or triazolam) standard substance solution;
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