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GA/T 1319-2016: GC and GC - MS examination methods for amphetamines including amphetamine methamphetamine MDMA and tenamfetamine in urine of drug user in forensic science
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GC and GC - MS examination methods for amphetamines including amphetamine methamphetamine MDMA and tenamfetamine in urine of drug user in forensic science
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GA/T 1319-2016
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Basic data | Standard ID | GA/T 1319-2016 (GA/T1319-2016) | | Description (Translated English) | GC and GC - MS examination methods for amphetamines including amphetamine methamphetamine MDMA and tenamfetamine in urine of drug user in forensic science | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Word Count Estimation | 15,167 | | Date of Issue | 2016-07-11 | | Date of Implementation | 2016-07-11 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1319-2016: GC and GC - MS examination methods for amphetamines including amphetamine methamphetamine MDMA and tenamfetamine in urine of drug user in forensic science
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Court scientific drug addicts in the urine of amphetamines and other four kinds of amphetamines drugs by gas chromatography and gas chromatography - mass spectrometry)
ICS 13.310
A92
People 's Republic of China Public Security Industry Standard
Court scientific drug addicts in the urine of amphetamines and other four
Amphetamine - type drug gas chromatography and gas chromatography - mass spectrometry
Testing method
2016-07-11 released
2016-07-11 implementation
Issued by the Ministry of Public Security of the People 's Republic of China
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents.
This standard is proposed by the National Committee for the Standardization of Pharmaceutical Technology Standardization of Substances (SAC/TC179/SC1) and
Go back.
The drafting of this standard. the Ministry of Public Security evidence identification center, the Shanghai Municipal Public Security Bureau material identification center.
The main drafters of this standard. Zhu Jun, Zhao Jingzhen, Yu Zhong Shan, Cui Wei, Liu Yao, Zhang Yurong, Wang Rong
Court scientific drug addicts in the urine of amphetamines and other four
Amphetamine - type drug gas chromatography and gas chromatography - mass spectrometry
Testing method
1 Scope
This standard specifies the forensic urine of the law of amphetamines, ephedrine (methamphetamine), dimethylene bis
(GCMA) and gas chromatography-mass spectrometry (GC-MS) were used to determine the properties of the compounds (MDMA) and methamphetamine (MDA).
This standard applies to forensic science suspected drug addicts amphetamine drug screening test was positive in the urine of amphetamine, methamphetamine,
Qualitative and Quantitative Analysis of Dimethylenediamine Amphetamine and Phenamphetamine.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Analysis of laboratory water specifications and test methods GB/T 6682-2008
Glossary of Terminology for Poison Analysis
3 terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principle
The samples were extracted, purified and concentrated according to the requirements of the parallel operation. The gas phase
(TR), mass spectral characteristics of ion fragment peaks and relative abundance were used as qualitative judgment basis. The results were analyzed by gas chromatography-mass spectrometry.
Line operation to add the standard material response value comparison, according to the peak area ratio, with the external standard method or internal standard method for quantitative analysis.
5 reagents, materials and instruments
5.1 Reagent
Unless otherwise stated, the reagents used in this standard are of analytical grade and the test water shall comply with the tertiary water specified in GB/T 6682-2008.
a) Methanol;
b) Ethanol;
c) cyclohexane;
d) sodium chloride;
e) anhydrous sodium carbonate;
f) NaOH solution.
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