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GA/T 1316-2016: GC and GC-MS examination methods for ketamine in hair and blood samples of forensic science
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| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GA/T 1316-2016 | English | 349 |
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GC and GC-MS examination methods for ketamine in hair and blood samples of forensic science
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GA/T 1316-2016
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Basic data | Standard ID | GA/T 1316-2016 (GA/T1316-2016) | | Description (Translated English) | GC and GC-MS examination methods for ketamine in hair and blood samples of forensic science | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Word Count Estimation | 15,172 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1316-2016: GC and GC-MS examination methods for ketamine in hair and blood samples of forensic science
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(Forensic science hair, blood ketamine gas chromatography and gas chromatography - mass spectrometry)
ICS 13.310
A92
People 's Republic of China Public Security Industry Standard
Court science hair, blood ketamine gas chromatography and
Gas Chromatography - Mass Spectrometry
2016-06-30 release
2016-06-30 implementation
Issued by the Ministry of Public Security of the People 's Republic of China
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents.
This standard is proposed by the National Committee for the Standardization of Pharmaceutical Technology Standardization of Substances (SAC/TC179/SC1) and
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The drafting of this standard. the Ministry of Public Security evidence identification center, the Shanghai Municipal Public Security Bureau material identification center.
The main drafters of this standard. Zhu Jun, Liu Yao, Yu Zhong Shan, Chang Jing, Cui Wei, Zhang Yurong, Wang Rong.
Court science hair, blood ketamine gas chromatography and
Gas Chromatography - Mass Spectrometry
1 Scope
This standard specifies the method of scientific hair, blood ketamine in the blood chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) test method.
This standard applies to forensic and quantitative analysis of ketamine in the hair and blood of the forensic science.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Analysis of laboratory water specifications and test methods GB/T 6682-2008
Glossary of Terminology for Poison Analysis
3 terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principle
Take the blank sample and add the sample as a control, according to the requirements of parallel operation, the hair, blood samples for extraction, purification, concentration or derivative
(GC) and GC-MS were used to determine the retention time (tR), mass spectral characteristic ion fragment peak and relative abundance as the qualitative judgment basis.
Using the standard curve method for quantitative analysis, or parallel operation with the addition of standard response value, according to the peak area ratio, with the external standard or internal
Standard method for quantitative analysis.
5 Reagent equipment and materials
5.1 Reagent
The reagents used in this method are of analytical grade and the test water is tertiary water (see GB/T 6682-2008);
a) ketamine hydrochloride;
b) internal standard 4-phenylbutylamine (4-PBA) or other equivalent internal standard;
c) Methanol;
d) cyclohexane;
e) dichloromethane;
f) ethyl acetate;
g) isopropanol;
h) Ammonia;
i) potassium dihydrogen phosphate;
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