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GC and GC-MS examination methods for drugs. Part 5: MDMA
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GA/T 1008.5-2013
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Basic data | Standard ID | GA/T 1008.5-2013 (GA/T1008.5-2013) | | Description (Translated English) | GC and GC-MS examination methods for drugs. Part 5: MDMA | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.130 | | Word Count Estimation | 11,154 | | Quoted Standard | GA/T 122; JJF 1059-1999 | | Regulation (derived from) | Industry standard filing notice 2015 No. 4 (total 184) | | Issuing agency(ies) | Ministry of Public Security | | Summary | This standard specifies the qualitative analysis of gas chromatographic-mass spectrometry (MD-MS) and the quantitative analysis of gas chromatography (GC) for dimethylene bisoxymandatamine (MDMA). This standard is applicable to qualitative and quantitativ | GA/T 1008.5-2013: GC and GC-MS examination methods for drugs. Part 5: MDMA---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
GC and GC-MS examination methods for drugs.Part 5. MDMA
ICS 13.130
A92
People's Republic of China Public Security Industry Standards
Common drugs by gas chromatography, gas chromatography - mass spectrometry
Testing method
Part 5. Two-methylenedioxymethamphetamine amphetamine
Part 5. MDMA
Issued on. 2013-01-16
2013-03-01 implementation
People's Republic of China Ministry of Public Security
Table of Contents
Introduction Ⅲ
1 Scope 1
2 Normative references 1
3 Terms and definitions
4 Principle 1
5 Reagents and reference materials, instruments and apparatus volume 1
Qualitative analysis of 6
7 Quantitative Analysis
8 results of the evaluation 5
Appendix A (informative) external standard quantitation sample extraction operation parameters in Table 7
Appendix B (Informative Appendix) MDMA-related spectrum of 8
Foreword
This section drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
GA/T 1008 "Common drugs by gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts.
--- Part 1. opium, five-component;
--- Part 2. morphine;
--- Part 3. Cannabis three components;
--- Part 4. cocaine;
--- Part 5. Two-methylenedioxymethamphetamine amphetamine;
--- Part 6. methadone;
--- Part 7. methaqualone;
--- Part 8. triazolam;
--- Part 9. estazolam;
--- Part 10. diazepam;
--- Part 11. bromazepam;
--- Part 12. chlordiazepoxide.
This section GA/T 1008 Part 5.
This part of the National Standardization Technical Committee for Standardization of Poison Analyses for Criminal Technology Technical Committee (SAC/TC179/SC1) mention
And the focal point.
This section drafted by. Ministry of Public Security Evidence Identification Center.
The main drafters of this section. Gregory students, Chang Chun, Zheng Hui, Qian Zhenhua, Xu Peng, Huang Xing, Wang, Wang Wei Xin, Chang Ying, Liu Kelin.
Common drugs by gas chromatography, gas chromatography - mass spectrometry
Testing method
Part 5. Two-methylenedioxymethamphetamine amphetamine
1 Scope
GA/T 1008 provisions of this section two methylenedioxymethamphetamine amphetamine (MDMA) gas chromatography - mass spectrometry (GC-MS) Qualitative
Analysis and gas chromatography (GC) quantitative analysis.
Qualitative and quantitative examination and identification This section applies to drug cases solid samples of MDMA.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
GA/T 122 toxicological analysis Terminology
JJF1059-1999 Measurement Uncertainty and representation
3 Terms and Definitions
Terms and definitions GA/T 122 defined apply to this document.
Principle 4
This method uses the internal standard method or external standard method for quality control of solid samples of suspected drug MDMA organic solvent extraction,
By gas chromatography - mass spectrometry (GC-MS) qualitative analysis by gas chromatography - flame ionization detector (GC-FID) of MDMA into
Line quantitative analysis.
5 Reagents and reference materials, instruments and appliances volume
5.1 Reagents and Standards
The reagents used were of analytical grade.
a) methanol.
b) traceable reference materials. MDMA.
c) external standard quantitation using 1.0mg/mLMDMA standard stock solution. Weigh MDMA standard substance (according to the standard in terms of substance purity
After equal to 50.0mg of MDMA), placed in a 50mL volumetric flask, add 20mL of methanol shaking dissolved, diluted with methanol
To the mark, the preparation of 1.0mg/mLMDMA stock standard solution, home refrigerator freezer to save, save for 6 months.
d) external standard quantitation using 0.1mg/mLMDMA working standard solution. Pipette 1.0mg/mLMDMA standard solution 5mL added
To 50mL volumetric flask, diluted with methanol to the mark, formulated as 0.1mg/mLMDMA working standard solution, cooled in refrigerator
Tibetan save, save time of 3 months.
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