| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GA/T 1008.3-2013 | English | 519 |
Add to Cart
|
3 days [Need to translate]
|
GC and GC-MS examination methods for drugs-Part 3: Three components in cannabis
| Obsolete |
GA/T 1008.3-2013
|
PDF similar to GA/T 1008.3-2013
Basic data | Standard ID | GA/T 1008.3-2013 (GA/T1008.3-2013) | | Description (Translated English) | GC and GC-MS examination methods for drugs-Part 3: Three components in cannabis | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.130 | | Word Count Estimation | 13,152 | | Quoted Standard | GA/T 122; JJF 1059-1999 | | Regulation (derived from) | Industry standard filing notice 2014 No. 4 (total 172) | | Issuing agency(ies) | Ministry of Public Security | | Summary | This standard specifies the qualitative and quantitative analysis of active ingredients in cannabis by gas chromatography-mass spectrometry (GC-MS) and gas chromatography (GC). This standard is applicable to the qualitative examination and identification | GA/T 1008.3-2013: GC and GC-MS examination methods for drugs-Part 3: Three components in cannabis---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
GC and GC-MS examination methods for drugs-Part 3. Three components in cannabis
ICS 13.130
A92
People's Republic of China Public Security Industry Standards
Common drugs by gas chromatography, gas chromatography - mass spectrometry
Test methods - Part 3. three ingredients in marijuana
Part 3. Threecomponentsincannabis
Issued on. 2013-01-16
2013-03-01 implementation
People's Republic of China Ministry of Public Security
Table of Contents
Preface Ⅰ
1 Scope 1
2 Normative references 1
3 Terms and definitions
4 Principle 1
5 Reagents and reference materials, instruments and apparatus volume 1
Qualitative analysis of 6
7 Quantitative Analysis
8 results of the evaluation 5
Appendix A (informative) Preparation of the operating parameters of the standard solution of internal standard method selection table 7
Annex B (informative) external standard quantitation sample extraction operation parameters Table 8
Annex C (informative) marijuana-related spectrum of three active ingredients 9
Foreword
This section drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some content of this document may involve patents, the issuing authority of this document does not assume responsibility for the identification of these patents.
GA/T 1008 "Common drugs by gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts.
--- Part 1. opium, five-component;
--- Part 2. morphine;
--- Part 3. Cannabis three components;
--- Part 4. cocaine;
--- Part 5. Two-methylenedioxymethamphetamine amphetamine;
--- Part 6. methadone;
--- Part 7. methaqualone;
--- Part 8. triazolam;
--- Part 9. estazolam;
--- Part 10. diazepam;
--- Part 11. bromazepam;
--- Part 12. chlordiazepoxide.
This section GA/T 1008 Part 3.
This part of the National Standardization Technical Committee for Standardization of Poison Analyses for Criminal Technology Technical Committee (SAC/TC179/SC1) mention
And the focal point.
This section drafted by. Ministry of Public Security Evidence Identification Center.
The main drafters of this section. Gregory students, Zheng Hui, Chang Chun, Qian Zhenhua, Xu Peng, Huang Xing, Wang, Wang Wei Xin, Chang Ying, Liu Kelin.
Common drugs by gas chromatography, gas chromatography - mass spectrometry
Test methods - Part 3. three ingredients in marijuana
1 Scope
GA/T 1008 provisions of this part of the active ingredient in marijuana gas chromatography - mass spectrometry (GC-MS) and gas chromatography qualitative analysis
(GC) quantitative analysis.
This section applies to drug cases solid samples THC, THC and cannabidiol qualitative examination and identification, and tetrahydrocannabinol
Quantitative phenol inspection and appraisal.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
GA/T 122 toxicological analysis Terminology
JJF1059-1999 Measurement Uncertainty and representation
3 Terms and Definitions
Terms and definitions GA/T 122 defined apply to this document.
Principle 4
This method uses the internal standard method or external standard method for quality control, solid samples of suspected drug THC, cannabidiol, marijuana
Phenol organic solvent extraction, gas chromatography - mass spectrometry for qualitative analysis (GC-MS), gas chromatography - flame ionization detector
(GC-FID) of THC were quantitatively analyzed.
5 Reagents and reference materials, instruments and appliances volume
5.1 Reagents and Standards
The reagents used were of analytical grade.
a) methanol;
b) traceable reference materials. 0.1mg/mL THC stock standard solution;
c) traceable reference materials. 1mg/mL THC stock standard solution;
d) traceable reference materials. 1mg/mL cannabidiol standard solution;
e) quantified by external standard 0.05mg/mL THC standard working solution. Pipette 0.1mg/mL THC stock standard solution
1mL was added to 2mL volumetric flask, dilute to the mark with methanol to prepare a 0.05mg/mL THC Standard Operating
Liquid, frozen in refrigerator, storage time is one month;
|