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GC and GC-MS examination methods for drugs-Part 10: Diazepam
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GA/T 1008.10-2013
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Basic data | Standard ID | GA/T 1008.10-2013 (GA/T1008.10-2013) | | Description (Translated English) | GC and GC-MS examination methods for drugs-Part 10: Diazepam | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.130 | | Word Count Estimation | 11,197 | | Quoted Standard | GA/T 122; JJF 1059-1999 | | Regulation (derived from) | Industry standard filing notice 2015 No. 4 (total 184) | | Issuing agency(ies) | Ministry of Public Security | | Summary | This standard specifies the qualitative analysis of diazepam by gas chromatography-mass spectrometry (GC-MS) and quantitative analysis by gas chromatography (GC). This standard is applicable to qualitative and quantitative examination of diazepam in solid | GA/T 1008.10-2013: GC and GC-MS examination methods for drugs-Part 10: Diazepam---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
GC and GC-MS examination methods for drugs-Part 10. Diazepam
ICS 13.130
A92
People 's Republic of China Public Security Industry Standard
Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs
Testing method
Part 10. Diazepam
Part 10. Diazepam
2013-01-16 release
2013-03-01 implementation
Issued by the Ministry of Public Security of the People 's Republic of China
Directory
Preface III
1 Scope 1
2 normative reference document 1
3 Terms and definitions 1
Principle 1
5 reagents and reference materials, instruments and measuring instruments 1
Qualitative analysis
Quantitative analysis
8 Results 5
Appendix A (informative) External standard quantitative method Sample extraction operation parameter selection Table 7
Appendix B (informative) Diazepam Related Spectrum
Foreword
This part is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may relate to patents and that the issuer of this document does not assume responsibility for the identification of these patents.
GA/T 1008 "common drug gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts.
- Part 1. Five elements in opium;
- Part 2. morphine;
- Part 3. Three ingredients in cannabis;
- Part 4. Cocaine;
- Part 5. Dimethylenediamine Amphetamine;
- Part 6. methadone;
- Part 7. Ammonone;
- Part 8. Triazolam;
- Part 9. estazolam;
- Part 10. Diazepam;
- Part 11. Bromepam;
- Part 12. Chlorotiazole.
This section is part 10 of GA/T 1008.
This part of the National Criminal Technology Standardization Technical Committee of the Standardization Subcommittee on Poisons Analysis (SAC/TC179/SC1)
Out of charge.
This part of the drafting unit. the Ministry of Public Security evidence identification center.
The main drafters of this part. Gao Lisheng, Zhang Chunshui, Zheng Hui, Qian Zhenhua, Xu Peng, Huang Xing, Wang Yi, Wang Weixin, Chang Ying, Liu Keling.
Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs
Testing method
Part 10. Diazepam
1 Scope
This part of GA/T 1008 specifies the GC-MS qualitative analysis and gas chromatography (GC) quantification of diazepam
analysis.
This part is applicable to the qualitative and quantitative identification of diazepam in solid samples of drug cases.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Glossary of Terminology for Poison Analysis
Evaluation and Representation of Measurement Uncertainty JJF1059-1999
3 terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principle
This method uses internal standard or external standard method for quality control, the suspected drug samples of solid diazepam organic solvent extraction, with
Gas chromatography-mass spectrometry (GC-MS), and gas chromatography-hydrogen flame ionization detector (GC-FID) was used to determine diazepam
Quantitative analysis.
5 reagents and reference materials, instruments and measuring instruments
5.1 Reagents and standard substances
The reagents used were of analytical grade.
a) Methanol.
b) traceable standard substance. diazepam.
c) External standard with 1.0mg/mL diazepam standard stock solution. Weigh diazepam standard substance (according to the standard material purity after conversion
Equal to 50.0 mg of diazepam) was placed in a 50 mL volumetric flask, dissolved in 20 mL of methanol and dissolved in methanol
Scale, prepared into 1.0mg/mL diazepam standard stock solution, set the refrigerator frozen storage, save time of 6 months.
d) external standard quantitative 0.1mg/mL diazepam standard working solution. remove 1.0mg/mL diazepam standard stock solution 5mL added
To 50mL volumetric flask, diluted with methanol to the mark, prepared into 0.1mg/mL diazepam standard working fluid, set the refrigerator in the cold
Save, save time for 3 months.
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