| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GA/T 1008.1-2013 | English | 479 |
Add to Cart
|
3 days [Need to translate]
|
GC and GC-MS examination methods for drugs-Part 1: Five components in opium
| Obsolete |
GA/T 1008.1-2013
|
PDF similar to GA/T 1008.1-2013
Basic data | Standard ID | GA/T 1008.1-2013 (GA/T1008.1-2013) | | Description (Translated English) | GC and GC-MS examination methods for drugs-Part 1: Five components in opium | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.130 | | Word Count Estimation | 12,116 | | Quoted Standard | GA/T 122; JJF 1059-1999 | | Regulation (derived from) | Industry standard filing notice 2014 No. 4 (total 172) | | Issuing agency(ies) | Ministry of Public Security | | Summary | This standard specifies the qualitative analysis of morphine, codeine, phenobarbital, papaverine, naloxerine by gas chromatography-mass spectrometry (GC-MS) and gas chromatography (GC) quantitative analysis of morphine. This standard applies to morphine, | GA/T 1008.1-2013: GC and GC-MS examination methods for drugs-Part 1: Five components in opium---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
GC and GC-MS examination methods for drugs-Part 1. Five components in opium
ICS 13.130
A92
People 's Republic of China Public Security Industry Standard
Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs
Testing method
Part 1. Five Ingredients in Opium
Part 1. Fivecomponentsinopium
2013-01-16 release
2013-03-01 implementation
Issued by the Ministry of Public Security of the People 's Republic of China
Directory
Preface III
1 Scope 1
2 normative reference document 1
3 Terms and definitions 1
Principle 1
5 reagents and reference materials, instruments and measuring instruments 1
Qualitative analysis
Quantitative analysis
8 Results 5
Appendix A (informative) Related spectrum of active ingredients in opium 7
Foreword
This part is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may relate to patents and that the issuer of this document does not assume responsibility for the identification of these patents.
GA/T 1008 "common drug gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts.
- Part 1. Five elements in opium;
- Part 2. morphine;
- Part 3. Three ingredients in cannabis;
- Part 4. Cocaine;
- Part 5. Dimethylenediamine Amphetamine;
- Part 6. methadone;
- Part 7. Ammonone;
- Part 8. Triazolam;
- Part 9. estazolam;
- Part 10. Diazepam;
- Part 11. Bromepam;
- Part 12. Chlorotiazole.
This section is part 1 of GA/T 1008.
This part of the National Criminal Technology Standardization Technical Committee of the Standardization Subcommittee on Poisons Analysis (SAC/TC179/SC1)
Out of charge.
This part of the drafting unit. the Ministry of Public Security evidence identification center.
The main drafters of this part. Gao Lise, Zheng Hui, Zhang Chunshui, Qian Zhenhua, Xu Peng, Huang Xing, Wang Yi, Wang Weixin, Chang Ying, Liu Keling.
Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs
Testing method
Part 1. Five Ingredients in Opium
1 Scope
This section of GA/T 1008 specifies the gas chromatographic properties of opium in the active ingredient morphine, codeine, tibainine, papaverine,
(GC-MS) qualitative analysis and morphine gas chromatography (GC) quantitative analysis.
This part is applicable to the qualitative test of morphine, codeine, tibain, papaverine, and cacrine in solid samples.
Quantitative inspection and identification.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Glossary of Terminology for Poison Analysis
Evaluation and Representation of Measurement Uncertainty JJF1059-1999
3 terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principle
This method uses internal standard or external standard method for quality control, the suspected drug samples of solid morphine, codeine, babaine, poppy
(GC-MS), and gas chromatography-hydrogen flame ionization (GC-MS) was carried out by gas chromatography-mass spectrometry (GC-MS)
The detector (GC-FID) was used to quantitatively analyze morphine.
5 reagents and reference materials, instruments and measuring instruments
5.1 Reagents and standard substances
The reagents used were of analytical grade.
a) Methanol.
b) chloroform.
c) isopropanol.
d) 0.5% glacial acetic acid aqueous solution. take 0.5mL glacial acetic acid in 100mL volumetric flask, add water to the volume, the preparation of 0.5%
Glacial acetic acid aqueous solution.
e) 0.1M aqueous sodium hydroxide solution. take 0.46g sodium hydroxide solid in a 100mL volumetric flask, add water to the volume, the preparation
Into 0.1M aqueous sodium hydroxide solution.
|