SN/T 3930-2014 English PDFUS$319.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3930-2014: Determination of glycerole monocaprylin, glycerol monodecanoate and glycerol monolaurate in foods for export Status: Valid
Basic dataStandard ID: SN/T 3930-2014 (SN/T3930-2014)Description (Translated English): Determination of glycerole monocaprylin, glycerol monodecanoate and glycerol monolaurate in foods for export Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: X04 Classification of International Standard: 67.050 Word Count Estimation: 12,158 Date of Issue: 4/9/2014 Date of Implementation: 11/1/2014 Regulation (derived from): State inspection certification (2014) 210 Issuing agency(ies): General Administration of Customs Summary: This standard specifies the method for gas chromatography and gas chromatography-mass spectrometry of glyceryl monocaprylate, monoglycolate and glyceryl monolaurate in export food. This standard is applicable to the determination and confirmation of glyceryl monocaprylate, monoglycolate glyceride and glyceryl monolaurate in bread, milk powder, bean paste, beverage and sausage. SN/T 3930-2014: Determination of glycerole monocaprylin, glycerol monodecanoate and glycerol monolaurate in foods for export---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. (Food for export caprylic acid monoglyceride, triglyceride and determination monocaprate glyceryl monolaurate) People's Republic of China Entry-Exit Inspection and Quarantine Standards Glyceryl monocaprylate food for export, single capric glycerides Determination and glyceryl monolaurate Determinationofglycerolemonocaprylin, glycerolmonodecanoateandglycerol Issued on. 2014-04-09 2014-11-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Distribution of this document Institutions do not assume the responsibility to identify these patents. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard is drafted by. People's Republic of China Hebei Exit Inspection and Quarantine. The main drafters of this standard. Chenrui Chun, Mayu Song, Jia Haitao, Guo Chunhai. Glyceryl monocaprylate food for export, single capric glycerides Determination and glyceryl monolaurate1 ScopeThis standard specifies the export of food products of caprylic acid monoglyceride, capric acid glycerides and single glyceryl monolaurate of gas chromatography and gas chromatography - Mass spectrometry. This standard applies to bread, milk powder, bean paste, drinks and sausages in glycerol monocaprylate, single capric glycerides and glycerol monolaurate content Determination and confirmation. The first gas chromatography - mass spectrometry2 Method summaryThe analyte in the sample hexane dichloromethane (11) and the extracts back extracted with n-hexane saturated acetonitrile solution was concentrated, GC Mass spectrometry, external standard.3 Reagents and materialsUnless otherwise specified, reagents were of analytical grade. 3.1 acetone, pesticide grade. 3.2 acetonitrile, HPLC fractions. 3.3 methylene chloride, pesticide grade. 3.4 n-hexane, pesticide grade. 3.5 n-hexane saturated acetonitrile. Take acetonitrile (3.2) and n-hexane (3.4) in each 100mL separating funnel shaking, standing layer, the lower layer is n-hexyl Dioxane saturated acetonitrile. 3.6 hexane dichloromethane (11 volume fraction). amount of an equal volume of methylene chloride (3.3) and n-hexane (3.4) and mixed. 3.7 Standard. glyceryl monocaprylate (molecular formula. C11H22O4, CAS Number. 19670496) purity of greater than or equal to 98%; single-capric acid glycerol Ester (molecular formula. C13H26O4, CAS Number. 26402222) purity of greater than or equal to 98%; glycerol monolaurate (molecular formula. C15H30O4, CAS Number. 142187) purity of greater than or equal to 98%. 3.8 monocaprylate, glyceryl caprate single and glycerol monolaurate stock standard solution. Accurately weighed amount of standard product with acetone (3.1) Formulated into standard stock solution 10mg/mL of. 0 ℃ ~ 5 ℃ storage. 3.9 of caprylic acid monoglyceride, capric acid glycerides and single glyceryl monolaurate working standard solution. Pipette caprylic acid monoglyceride, capric acid alone Glycerides and glycerol monolaurate stock standard solution (3.8) 0.2mL, 0.5mL, 1.0mL, 2.0mL, 5.0mL, 10.0mL in 100mL flask, acetonitrile to volume, that is, for 20μg/mL, 50μg/mL, 100μg/mL, 200μg/mL, 500μg/mL, Working standard solutions 1000μg/mL of. 0 ℃ ~ 5 ℃ storage. 3.10 0.22μm membrane, organic.4 instruments and equipment4.1 Gas chromatography-mass spectrometry . 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