SN/T 2592.4-2011 English PDF

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SN/T 2592.4-2011: Determination of organotin compounds in electrical and electronic equipment. Part 4: High performance liquid chromatography-mass spectrometry
Status: Valid

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
SN/T 2592.4-2011	289	Add to Cart	3 days	Determination of organotin compounds in electrical and electronic equipment. Part 4: High performance liquid chromatography-mass spectrometry	Valid

Similar standards

GB/T 6113.102   GB/T 34986   GB/T 32910.3   SN/T 2592.6   SN/T 2592.5   SN/T 2592.1   

Basic data

Standard ID: SN/T 2592.4-2011 (SN/T2592.4-2011)
Description (Translated English): Determination of organotin compounds in electrical and electronic equipment. Part 4: High performance liquid chromatography-mass spectrometry
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: L04
Classification of International Standard: 31.020
Word Count Estimation: 11,117
Date of Issue: 2011-09-30
Date of Implementation: 2012-04-01
Quoted Standard: GB/T 6682
Regulation (derived from): National Quality Inspection (2011) 492; industry standard filing Notice 2012 No. 4 (No. 148 overall)
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the electrical and electronic products, plastic components of tributyltin (TBT), triphenyltin (TPhT) and tri- octyl tin (TOT) (see Appendix A) content of liquid chromatography mass spectrometry (LC-MS) method. This standard applies to electrical and electronic products, plastic components of tributyltin (TBT), triphenyltin (TPhT) and tri- octyl tin (TOT) content.

SN/T 2592.4-2011: Determination of organotin compounds in electrical and electronic equipment. Part 4: High performance liquid chromatography-mass spectrometry

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of organotin compounds in electrical and electronic equipment.Part 4. High performance liquid chromatography-mass spectrometry People's Republic of China Entry-Exit Inspection and Quarantine Standards Determination of organotin compounds in electrical and electronic products Part 4. Liquid Chromatography - Mass Spectrometry Part 4. Highperformanceliquidchromatography-massspectrometry Issued on. 2011-09-09 2012-04-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

"Determination of electrical and electronic products of organic tin compounds" SN/T 2592 series of standards is divided into six parts. --- Part 1. gas chromatography; --- Part 2. Fourier transform infrared spectroscopy screening method; --- Part 3. Inductively Coupled Plasma Mass screening; --- Part 4. Liquid chromatography - mass spectrometry; --- Part 5. gas chromatography - mass spectrometry; --- Part 6. Inductively coupled plasma atomic emission spectrometry. This section "Measurement of electrical and electronic products, organic tin compounds" SN/T 2592 series of standards - Part 4. This section drafted in accordance with GB/T 1.1-2009 given rules. This section proposed and managed by the National Certification and Accreditation Administration Committee. This section was drafted by. People's Republic of China Shandong Entry Inspection and Quarantine Bureau, People's Republic of China Guangdong Entry-Exit Inspection and Quarantine Bureau, the Shenzhen People's Republic of China Exit Inspection and Quarantine. The main drafters of this section. Xu Qin, cattle Zengyuan, Ye Xi Wen, Sun Yinfeng, Liu Yinfeng, Zouchun Hai. The first part of the Department of Inspection and Quarantine issued by industry standards. Determination of organotin compounds in electrical and electronic products Part 4. Liquid Chromatography - Mass Spectrometry

1 Scope

This section SN/T 2592 specifies the electrical and electronic products plastic parts tributyltin (TBT), triphenyltin (TPhT) and trioctyl Yl tin (TOT) (see Appendix A) content of liquid chromatography - mass spectrometry (LC-MS) spectrometry. This section applies to electrical and electronic products plastic parts tributyltin (TBT), triphenyltin (TPhT) and tri-octyl tin (TOT) containing Determination of the amount.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Method summary

The sample was dissolved in tetrahydrofuran, and after methanol precipitation of impurities, to LC-MS was measured and confirmed, external standard.

4 Reagents and materials

Unless otherwise specified, the reagents used were of analytical grade. Water should be consistent with GB/T 6682 water level. 4.1 Methanol. HPLC grade. 4.2 acetonitrile. HPLC grade. 4.3 THF. HPLC grade. 4.4 glacial acetic acid. 4.5 tributyltin, triphenyltin and tri-octyl tin Standard. Purity ≥98%, see Appendix A. 4.6 organotin standard stock solution. the standard concentration of the stock solution concentration of organotin cation. Accurately weighed amount of organotin standard Products, with a small amount of methanol dissolved and diluted to volume in a brown flask, the concentration of 1000μg/mL, method of preparation see Appendix B. 4.7 negative sample extract. with free samples of organic tin, different substrates prepared in accordance with 6.1 negative sample extract. 4.8 Matrix standard solution. apply diluted to concentrations of matrix standard as required by the negative sample extract (4.7) standard stock solution Working solution. Reference linear range. TBT, TPhT of 0.1μg/mL ~ 10.0μg/mL; TOT is 0.05μg/mL ~ 5.0μg/mL.

5 instruments and equipment

5.1 Liquid chromatography - mass spectrometry. with electrospray ionization (ESI). 5.2 Ultrasonic Extractor. 100W, operating frequency 40kHz. 5.3 liquid nitrogen freezer mill or similar equipment. ......

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